• 한국산업융합학회 논문집
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• 제4권1호
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• pp.3-9
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• 2001

Many products related to automobile and airplane have been manufactured by semi-solid process. There are many parameters in semi-solid process such as punch velocity, die temperature, and solid fraction of material. Among these parameters, solid fraction of material is one of the most important factors to determine quality of product. To obtain solid fraction of a certain semi-solid product is very necessary and useful for inspecting and analyzing the product. In this paper, image analysis program for microstructure by semi-solid forming process has been developed with the simple apparatus such as a personal computer and scanner, instead of expensive image analyzer.

• 한국지반공학회:학술대회논문집
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• 한국지반공학회 1999년도 준설 및 환경매립에 관한 학술세미나
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• pp.15-31
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• 1999

The Pusan Clay is analyzed hereafter from a point of view of mineralogy and microstructure. Results indicate that the Pusan Clay is basically illitic in nature and that the soil microstructure reveals some characteristics which could be responsible for its brittle behavior as observed from sample disturbance. The overall analysis would tend to consider that the Pusan Clay profile analyzed here shows mechanical properties similar to well structured soils or so-called cemented soils.

• E2M - 전기 전자와 첨단 소재
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• 제8권5호
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• pp.544-550
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• 1995

In this paper, the anode for molten carbonate fuel cell have been prepared by doctor blade method and microstructure, pore distribution, sintering test of the electrode were investigated. Component analysis were done by Scanning Electron Micrograph, porosimeter and sintering test apparatus. As a result, median pore size was 11.mu.m order at the major specimen and porosity was about 70%. And thickness loss of the electrode was 1.5% at Ni-10Co anode after sintering test.

• 한국분말재료학회지
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• 제19권6호
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• pp.416-423
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• 2012

This paper introduces an effect of a preparing $ZrO_2$-Ag composite on its mechanical properties and microstructure. In present study, $ZrO_2$-Ag was prepared by reduction-deposition route and wetting dispersive milling method, respectively. Two type of Ag powders (nano Ag and micron Ag size, respectively) were dispersed into $ZrO_2$ powder during wetting dispersive milling in D.I. water. Each sample was sintered at $1450^{\circ}C$ for 2hr in atmosphere, and then several mechanical tests and analysis of microstructure were carried out by bending test, hardness, fracture toughness and fracture surface microstructure. As for microstructure, the Ag coated $ZrO_2$ showed homogeneously dispersed Ag in $ZrO_2$ in where pore defect did not appear. However, $ZrO_2$-nano Ag and $ZrO_2$-micro Ag composite appeared Ag aggregation and its pore defect, which carried out low mechanical property and wide error function value.

• 한국분말재료학회지
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• 제11권5호
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• pp.421-426
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• 2004

The microstructure and mechanical property of hot-pressed $Al_2O_3/Cu$ composites with a different temperature for atmosphere changing from H$_{2}$ to Ar have been studied. When atmosphere-changed from H$_{2}$ to Ar gas at 145$0^{\circ}C$, the hot-pressed composite was characterized by inhomogeneous microstructure and low fracture strength. On the contrary, when atmosphere-changed at low temperature of 110$0^{\circ}C$ the composite showed more homogeneous microstructure, higher fracture strength and smaller deviation in strength. Based on the thermodynamic consideration and microstructural analysis, it was interpreted that the Cu wetting behavior relating to the formation of CuAlO$_{2}$ is probably responsible for strong dependence of microstructure on atmosphere changing temperature. The reason for a strong sensitivity of fracture strength and especially of its deviation to atmosphere changing temperature was explained by the microstructural inhomogeneity and by the role of CuAlO$_{2}$ phase on the interfacial bonding strength.

• 열처리공학회지
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• 제34권1호
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• pp.17-24
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• 2021

In this study, Ti-X (X=Mn, Fe, Mo) powder alloys were designed and manufactured by both powder metallurgy (PM) and metal powder injection molding (MIM) process to improve strength and formability compared to CP-Ti powder materials. It was found that the lamellar microstructure consisted of α and β phases was formed in PM-processed alloys. However, MIM-processed alloys showed not the lamellar microstucture but the equiaxed α + β microstructure. It was also revealed that the contents of X component and feedstock were not affected to microstructure evolution. The reason why different microstructure was appeared between PM-processed and MIM-processed alloys is not clear yet, but supposed to be the effect of intersticial elements such as C, H and N derived from feedstock during debinding process of MIM.

• 한국전산구조공학회논문집
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• 제30권1호
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• pp.23-30
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• 2017

입자 복합재료는 입자의 형상, 크기 그리고 분포의 산포특성으로 인해 물성치의 편차가 존재하고, 입자 복합재료를 사용한 시스템의 거동 또한 산포가 존재한다. 하지만 입자의 산포특성을 고려하기 어려우므로 균질화법을 사용하여 시스템의 거동을 해석하거나 국부영역에서 미세구조를 적용하여 해석한다. 본 연구에서는 입자의 랜덤적 산포특성을 고려하기 위해 RMDFs(random morphology description functions)를 사용하여 랜덤 미세구조를 생성하였고, 단면 1차 모멘트를 사용하여 가우시안 함수의 수(N)와 입자의 산포특성의 관계를 분석하였다. 그리고 랜덤 미세구조 구조물의 거동을 분석하기 위하여 랜덤 미세구조를 전체에 반영한 외팔보에 multi-scale 해석을 수행하였다. 그 결과 입자의 산포특성과 외팔보의 처짐의 편차는 N의 증가에 따라 감소하고 N=200에서 수렴하는 것을 확인하였다.

• Carbon letters
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• 제15권1호
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• pp.25-31
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• 2014

A microstructure analysis is carried out to optimize the process parameters of a randomly oriented discrete length hybrid carbon fiber reinforced carbon matrix composite. The composite is fabricated by moulding of a slurry into a preform, followed by hot-pressing and carbonization. Heating rates of 0.1, 0.2, 0.3, 0.5, 1, and $3.3^{\circ}C/min$ and pressures of 5, 10, 15, and 20 MPa are applied during hot-pressing. Matrix precursor to reinforcement weight ratios of 70:30, 50:50, and 30:70 are also considered. A microstructure analysis of the carbon/carbon compacts is performed for each variant. Higher heating rates give bloated compacts whereas low heating rates give bloating-free, fine microstructure compacts. The compacts fabricated at higher pressure have displayed side oozing of molten pitch and discrete length carbon fibers. The microstructure of the compacts fabricated at low pressure shows a lack of densification. The compacts with low matrix precursor to reinforcement weight ratios have insufficient bonding agent to bind the reinforcement whereas the higher matrix precursor to reinforcement weight ratio results in a plaster-like structure. Based on the microstructure analysis, a heating rate of $0.2^{\circ}C/min$, pressure of 15 MPa, and a matrix precursor to reinforcement ratio of 50:50 are found to be optimum w.r.t attaining bloating-free densification and processing time.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2005년도 춘계학술발표대회 개요집
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• pp.144-146
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• 2005

Measurements of Thermoelectric power (TEP) were used to evaluate microstructural analysis in HSLA steel weldments. The measurements of TEP for weld microstructure across weldment have shown good correlation with hardness profile. The different TEP values indicated that changes in weld microstructure can be correlated with TEP values measured.

• 보존과학회지
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• 제37권4호
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• pp.340-356
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• 2021

We have tried the experimental research of lost-wax casting to reconstruct Gilt-Bronze Pensive Bodhisattva; preliminary and reconstruction experiment based on ancient texts. Main object to reconstruct is Korean National Treasure No.83, Gilt-Bronze Pensive Bodhisattva (Maitreya), then we measure alloy ratio and casting method based on the scientific analysis. Other impurities were removed from the base metal components(copper : tin : lead) and their ratio was set to 95.5 : 6.5 : 3 where the ratios for tin and lead were increased by 2.5% each. The piece-mold casting method was used, and piece-mold casting experiments were carried out twice in this study but supplementary research on piece-mold casting was necessary. The microstructure was confirmed to be typical cast microstructure and the component analysis result was similar to that of the prior study. Analysis of the chemical composition is confirmed to copper, tin, lead, and zinc, and the chemical composition of the matrix was 87.8%Cu-7.5%Sn-2.7%Pb-2.1%Zn, and similar to previous experimental research. Also resulted in the detection of small impurity in Zn. Analysis of the mould revealed that the mould was fabricated by adding quartz and organic matter for structural stability, fire resistance, and air permeability. We expect that our research will contribute to provide base data for advanced researches in future.