• 제목/요약/키워드: microscopic analysis

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알칼리와 고온노출에 의한 GFRP 보강근 손상에 대한 현미경분석 연구 (Optical Microscopic Image Analysis for Damaged GFRP Rebar by Alkali and High Temperature Exposures)

  • 배정명;문도영;박철우;박영환
    • 한국구조물진단유지관리공학회 논문집
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    • 제21권2호
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    • pp.53-59
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    • 2017
  • 본 연구에서는 고온에 노출된 GFRP 보강근과 고온에 노출된 후 알칼리용액에 노출된 보강근의 단면을 현미경을 통해 관찰하고 발생된 손상의 특징을 고찰하였다. 또한, 각 시험체에 발생한 레진 균열과 공극에 대한 정량적 분석을 실시하였다. 알칼리로 인한 손상은 주로 표면에 집중되며 레진균열과 작은 공극을 발생시키는 것으로 확인되었다. 고온노출에 의한 손상은 레진균열과 공극을 발생시키는 것은 알칼리와 동일하지만 전단면에서 발생하며, 공극의 크기가 훨씬 크다. 또한 정량분석 결과, 동일한 알칼리 용액 노출조건에도 불구하고, $200^{\circ}C$ 이상의 고온에 노출된 시편에서 발견된 레진 균열과 공극이 고온노출이력이 전혀 없는 보강근에서 발견된 것 보다 1.5 및 1.4배 큰 것으로 확인되었다. 그러므로 동일한 알칼리 노출 조건이라 할지라도 $200^{\circ}C$ 이상의 고온에 노출된 보강근은 고온노출이력이 없는 보강근에 비하여 레진의 열화가 가속화 될 가능성이 있음을 알 수 있다.

저소성 세립분 함량이 카올리나이트-모래 혼합토의 공학적 특성에 미치는 영향 (Effect of Low-Plastic Fine Content on the Engineering Properties of Kaolinite-Sand Mixture)

  • 판야봇 카오톤;이수형;최영태;윤찬영
    • 한국지반공학회논문집
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    • 제37권7호
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    • pp.35-42
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    • 2021
  • 본 연구에서는 다양한 카올리나이트 혼합비에 따른 카올리나이트-모래 혼합토의 특성을 실험적으로 분석하였다. 이를 위하여 기본물성실험과 다짐시험을 실시하고 그 결과를 분석하였으며, 카올리나이트와 모래입자 간의 상호 구조를 더욱 자세히 분석하기 위하여 현미경 사진을 이용한 관측을 추가적으로 수행하였다. 실험결과, 카올리나이트 혼합비가 증가할수록 비표면적의 증가에 따른 함수비의 증가 및 모래입자와의 강한 결합구조를 형성하는 것으로 나타났으며, 최대 건조밀도는 감소하고 초기간극비는 증가하는 것으로 나타났다. 현미경 사진 분석 결과, 세립분 함량의 증가에 따라 모래의 특성이 지배적인 비율, 중간 비율, 세립분의 특성이 지배적인 비율을 확인할 수 있었으며, 세립분의 함량이 25-40% 정도인 경우에 입자간 상호작용이 잘 이루어지는 것을 관측할 수 있었다.

연속류 시설의 이동병목구간에서 지체산정방법 -모의실험을 통한 교통류의 평균지체분석- (The Analysis of Traffic Flow Characteristics on Moving Bottleneck)

  • 김원규;정명규;김병종;서은채;김송주
    • 정보통신설비학회논문지
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    • 제8권4호
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    • pp.170-181
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    • 2009
  • When a slow-moving vehicle occupies one of the lanes of a multi-lane highway, it often causes queuing behind, unlike one is caused by an actual stoppage on that lane. This happens when the traffic flow rate upstream from the slow vehicle exceeds a certain critical value. This phenomena is called as the Moving Bottleneck, defined by Gazis and Herman (1992), Newell (1998) [3], and Munoz and Daganzo (2002), who conducted the flow estimates of upstream and downstream and considered slow-moving vehicle speed and the flow ratio exceeding slow vehicle and the microscopic traffic flow characteristics of moving bottleneck. But, a study of delay on moving bottleneck was not conducted until now. So this study provides a average delay time model related to upstream flow and the speed of slow vehicle. We have chosen the two-lane highway and homogeneous traffic flow. A slow-moving vehicle occupies one of the two lanes. Average delay time value is a result of AIMSUN[9], the microscopic traffic flow simulator. We developed a multiple regression model based on that value. Average delay time has a high value when the speed of slow vehicle is decreased and traffic flow is increased. Conclusively, the model is formulated by the negative exponential function.

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Numerical Simulation of Mechanical Behavior of Composite Structures by Supercomputing Technology

  • Kim, Seung-Jo;Ji, Kuk-Hyun;Paik, Seung-Hoon
    • Advanced Composite Materials
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    • 제17권4호
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    • pp.373-407
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    • 2008
  • This paper will examine the possibilities of the virtual tests of composite structures by simulating mechanical behaviors by using supercomputing technologies, which have now become easily available and powerful but relatively inexpensive. We will describe mainly the applications of large-scale finite element analysis using the direct numerical simulation (DNS), which describes composite material properties considering individual constituent properties. DNS approach is based on the full microscopic concepts, which can provide detailed information about the local interaction between the constituents and micro-failure mechanisms by separate modeling of each constituent. Various composite materials such as metal matrix composites (MMCs), active fiber composites (AFCs), boron/epoxy cross-ply laminates and 3-D orthogonal woven composites are selected as verification examples of DNS. The effective elastic moduli and impact structural characteristics of the composites are determined using the DNS models. These DNS models can also give the global and local information about deformations and influences of high local in-plane and interlaminar stresses induced by transverse impact loading at a microscopic level inside the materials. Furthermore, the multi-scale models based on DNS concepts considering microscopic and macroscopic structures simultaneously are also developed and a numerical low-velocity impact simulation is performed using these multi-scale DNS models. Through these various applications of DNS models, it can be shown that the DNS approach can provide insights of various structural behaviors of composite structures.

서울시 홍대상권 내 업종변화 필지의 공간적 특성 분석 - 상업 젠트리피케이션의 관점에서 - (Analysis of Spatial Characteristics of Business-Type-Changed Parcel in Hongik-University Commercial Area, Seoul - Focused on the View Point of Commercial Gentrification -)

  • 김동준;김기중;이승일
    • 국토계획
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    • 제54권2호
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    • pp.5-16
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    • 2019
  • The purpose of this study is to analyze the spatial characteristics of business-type-changed parcel in the Hongik-University commercial area, from the view point of commercial gentrification. A commercial gentrification occurs through a business-type-change in a spatial basic unit (microscopic spatial unit such as parcel) of an area which has not been considered in relavent policies and research. So, this study analyzed the spatial characteristics of business-type-changed parcels using the Cox's proportional hazard regression model. The main results of this study are as follows. First, as new developments in the adjacent area occur, the business-type-change probability increases. Second, by the commercial area division, the business-type-change probability is different. Finally, the accessibility is better, the probability is higher. These results could suggest that a consideration of the spatial characteristics form microscopic viewpoint is necessary to understand the commercial gentrification. And these could be used as basic data for a gentrification diagnostic and management system, which can predict gentrification from the view point of business-type-change on the basis of a parcel.

대용량 모빌리티 궤적 자료를 이용한 과속 위험노출도 분석 방법론 (Analysis Method for Speeding Risk Exposure using Mobility Trajectory Big Data)

  • 이숭봉;장현호;강태석
    • 한국재난정보학회 논문집
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    • 제17권3호
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    • pp.655-666
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    • 2021
  • 연구목적:본 연구는 대용량 차량궤적 자료를 이용하여 동적 과속 위험성을 측정하기 위한 방법론을 개발하고, 개발된 과속 지표의 적용성을 증명하는데 있다. 연구방법: 개별 차량 궤적을 이용하여 차량의 속도 변화를 미시적 시공간으로 분석하고, 사고 위험성 관점에서 과속의 경계(즉, 경계속도)를 결정하였다. 결정된 경계속도를 이용하여 미시적 시공간 기반 과속 노출도 지표를 개발하였다. 연구결과: 검증 연구는 대용량 차량 GPS 궤적 자료와 실제 교통사고 자료를 이용하여 수행되었다. 분석결과, 개발된 과속 노출도 지표는 고속도로 교통사고에 대해 우수한 설명력 (R2=0.7)을 보였다. 이는 미시적 시공간 차원에서 과속이 분석되어야 함을 직접적으로 의미한다. 결론:차량 속도 상태의 시공간적 변화는 매우 가변적이다. 따라서 본 연구에서 제시된 방법론은 차량 궤적 자료를 이용한 미시적인 공간기반 교통사고 요인 및 사고 위험 노출도 분석에 효과적으로 활용될 수 있을 것으로 판단된다.

부고환 생검이 부고환의 폐색에 미치는 실험적 연구 (An Experimental Study on the Effect of the Epididymal Biopsy on the Obstruction of the Epididymal Ducts)

  • 김두천;김세철
    • Clinical and Experimental Reproductive Medicine
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    • 제11권2호
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    • pp.77-81
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    • 1984
  • Epididymal biopsy has been performed without consideration of the possibility of epididymal ductal severance and obstruction which result in obstructive azoospermia. An attempt was made to study the effect of the epididymal biopsy on the obstruction of the epididymal ducts. Bilateral epididymal biopsies were done in 8 healthy rabbits (New Zealand White strain) weighing over 3 kg, and then ejaculated semens have been analyzed 5 times every other week from 1 month after biopsies. Microscopic examination of the biopsied epididymides was also done after the 5th semen analysis. The results were as follows. 1. Semen analysis: 6 out of 8 rabbits showed azoospermia from the 4th semen analysis and 2 cases showed normal number of the sperms in the 5th semen analysis. 2, Microscopic examination: 6 cases of azoospermia showed complete obstruction of the biopsied sites of the epididymides, and abscence of sperms in epididymal ducts distal to the biopsied sites of the epididymides. However, recanalization of the epididymal ducts was noted in 2 cases showing normal sperm count. Therefore, it is concluded that the epididymal biopsy should be avoided in patients who want to be fertile, because it may cause the epididymal severance and obstruction of the epididymal ducts.

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Development of Multi-sample Loading Device for TEM Characterization of Hydroxyapatite Nanopowder

  • Lee, Jong-Moon;Kim, Jung-Kyun;Jeong, Jong-Man;Kim, Jin-Gyu;Lee, Eunji;Kim, Youn-Joong
    • Bulletin of the Korean Chemical Society
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    • 제34권3호
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    • pp.788-792
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    • 2013
  • A shortcoming of using transmission electron microscopy (TEM) for structural analysis via electron diffraction is the relatively large error of the measurements as compared to X-ray diffraction. To reduce these errors, various internal standard methods from earlier studies have been widely used. We developed a new device to facilitate the application of internal standard methods in preparation of TEM grids used for nanopowder analysis. Through the application of a partial mask on the TEM grid, both the internal standards and the research materials can be loaded on the same grid. Through this process, we conducted a TEM analysis that compared synthetic hydroxyapatite (HAp) nanopowder to bone apatite from a bovine femur. We determined that the accuracy of the d-spacing measurements of the HAp and bone powders could be improved to better than 1% after statistical treatments of the experimental data. By applying a quarter mask, we loaded four different nanoparticles on a single TEM grid, with one section designated for the internal standard.

Determination of Absorbed Dose for Gafchromic EBT3 Film Using Texture Analysis of Scanning Electron Microscopy Images: A Feasibility Study

  • So-Yeon Park
    • 한국의학물리학회지:의학물리
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    • 제33권4호
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    • pp.158-163
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    • 2022
  • Purpose: We subjected scanning electron microscopic (SEM) images of the active layer of EBT3 film to texture analysis to determine the dose-response curve. Methods: Uncoated Gafchromic EBT3 films were prepared for direct surface SEM scanning. Absorbed doses of 0-20 Gy were delivered to the film's surface using a 6 MV TrueBeam STx photon beam. The film's surface was scanned using a SEM under 100× and 3,000× magnification. Four textural features (Homogeneity, Correlation, Contrast, and Energy) were calculated based on the gray level co-occurrence matrix (GLCM) using the SEM images corresponding to each dose. We used R-square to evaluate the linear relationship between delivered doses and textural features of the film's surface. Results: Correlation resulted in higher linearity and dose-response curve sensitivity than Homogeneity, Contrast, or Energy. The R-square value was 0.964 for correlation using 3,000× magnified SEM images with 9-pixel offsets. Dose verification was used to determine the difference between the prescribed and measured doses for 0, 5, 10, 15, and 20 Gy as 0.09, 1.96, -2.29, 0.17, and 0.08 Gy, respectively. Conclusions: Texture analysis can be used to accurately convert microscopic structural changes to the EBT3 film's surface into absorbed doses. Our proposed method is feasible and may improve the accuracy of film dosimetry used to protect patients from excess radiation exposure.

The Identification of Aucklandiae Radix, Inulae Radix, Vladimiriae Radix and Aristolochiae Radix, Using Macroscopic, Microscopic and Physicochemical Methods

  • Yoon, Jee-Hyun;Park, Ha-Yeong;Kim, Tae-Ju;Lee, Seung-Ho;Kim, Jung-Hoon;Lee, Guem-San;Kim, Hong-Jun;Ju, Young-Sung
    • 대한한의학회지
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    • 제35권4호
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    • pp.83-97
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    • 2014
  • Objectives: This study aimed for establishing the discriminative criteria for Aucklandiae Radix, Inulae Radix, Vladimiriae Radix and Aristolochiae Radix, which can be confused as 'Mokhyang', because of similar appearances and synonyms. Methods: Morphological characteristics of dried herbal medicines were compared by macroscopic observation. To examine microscopic features of 'Mokhyang', paraffin embedding and the staining by using Ju's method were conducted. Physicochemical experiments were performed using HPLC analysis and antioxidant assay. Results: The types of stem, phyllotaxy and leaf shape were chosen as macroscopic criteria and the size, oil spots, color and root top as well as phloem and central cylinder were compared using microscopic features. The HPLC results showed different amounts of costunolide and dehydrocostuslactone among Aucklandiae Radix, Inulae Radix and Vladimiriae Radix. However, Aristolochiae Radix only contained aristolochic acid. The antioxidant assays also showed that Vladimiriae Radix exhibited strongest antioxidant activity followed by Aucklandiae Radix, Inulae Radix and Aristolochiae Radix. Conclusions: These results demonstrate that macroscopic, microscopic and physicochemical methods would be useful tools for the discrimination of 4 kinds of 'Mokhyang'.