• Title/Summary/Keyword: microscopic analysis

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Observation by the Microscopic Analysis of Lacquer Layer for Identification of Lacquer-ware Function (칠 기법 규명을 위한 칠도막의 현미경 관찰)

  • Kim, Soo-Chul;Lee, Kwang-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.6
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    • pp.96-104
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    • 2008
  • In this study, the observation of test pieces with an optical microscope was carried out after fabricating 4 groups of standard lacquer, in order to inquire into the ancient lacquering techniques. Group I had transparent reddish brown color, and the part of layer was indefinite, and the layer polished was easily distinguished. Group II had mostly transparent yellowish brown color, and it was possibility distinguished the layers when they were varnished with mixed lacquer after prime coating, and when they were varnished with lacquer as the prime coating. Group III set up membrane in the hardening process of the lacquer, and the lacquer and the unsaturated fatty acid of internal part was dried, so the top layer and the lacquer layer were separated and observed. Group IV: When the lacquer coat film of Group IV test pieces were observed in polarized light, the ferrous components were seen as the black and red color were mixed, and the silica crystals of silty soil were distinguished by reflection of lights. And the colors were distinguished as the lacquer layer of ruddle had red color, and the mixed lacquer of reddish lacquer and ruddle had the deep red color at the top and the bottom, but the middle part had the bright red color.

A STUDY OF BONE APPOSITION AND MARGINAL ALVEOLAR BONE LOSS AROUND IMMEDIATE IMPLANSTS (발치 직후 매식 임프란트의 골침착과 변연골 상실에 대한 연구)

  • Jun, Chul-Oh;Vang, Mong-Sook
    • The Journal of Korean Academy of Prosthodontics
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    • v.35 no.1
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    • pp.165-180
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    • 1997
  • The purpose of this study was to observe bone apposition and marginal bone loss and to check the possibility of success on titanium implant, HA coated implant and the implant with natural coral that were place immediately after teeth extraction in dogs. Experimental subjects were divided into 4 groups ; the 1st group is the titanium implant, second the HA coated implant, third the implant with natural coral, and the last the control group that was prepared in the extraction sockets. After 12 weeks, the dogs were sacrificed for visual observation and microscopic examination approaching histologic and histomorphometric analysis. The results were as follows : 1. Neither the infection nor the exposure of implant was found at the sites of all implant. 2. In a histomorphometric analysis, mean percentage of direct bone contact with the titanium implant was 80.7% and the HA coated implant showed 81.5% apposition, but the implant with natural coral showed 64.9% apposition(P<0.05). 3. In a microscopic examination, mature lamellated bone was found around the immediate implants and control group, while unabsorbed natural coral around the immediate implants with natural coral was found. 4. All immediate implant groups showed the loss of marginal bone in order from implant with natural coral, titanium implant, and HA coated implant. 5. Implant with natural coral that was placed by the type I interface of the Barzilay's classification immediately after teeth extraction showed low percentage of direct bone contact area, low success rate and a lot of marginal bone loss. Above results suggested that the immediate implants are osseointegrated successfully, although slightly marginal bone was loss.

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Plasticity Model for Directionality of Concrete Crack Damages (콘크리트 균열 손상의 방향성을 고려한 다중파괴기준 소성 모델)

  • Kim, Jae-Yo;Park, Hong-Gun
    • Journal of the Korea Concrete Institute
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    • v.19 no.5
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    • pp.655-664
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    • 2007
  • The inherent characteristic of concrete tensile cracks, directional nonlocal crack damage, causes so-called rotating tensile crack damage and softening of compressive strength. In the present study, a plasticity model was developed to describe the behavior of reinforced concrete planar members In tension-compression. To describe the effect of directional nonlocal crack damage, the concept of microplane model was combined with the plasticity model. Unlike existing models, in the proposed model, softening of compressive strength as well as the tensile crack damage were defined by the directional nonlocal crack damage. Once a tensile cracking occurs, the microplanes of concrete are affected by the nonlocal crack damage. In the microplanes, microscopic tension and compression failure surfaces are calculated. By integrating the microscopic failure surfaces, the macroscopic failure surface is calculated. The proposed model was implemented to finite element analysis, and it was verified by comparisons with the results of existing shear panel tests.

Chemistry and Cathodoluminescence Properties of the Carbonate Minerals From the Tertiary Marine Sediments, SE Korea (제3기 해성퇴적층에서 산출되는 탄산염광물의 화학적 및 음극선 발광 특성)

  • Son, Byeong-Kook;Kim, Hyun-Tae
    • Journal of the Mineralogical Society of Korea
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    • v.17 no.2
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    • pp.123-133
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    • 2004
  • Carbonate minerals are examined by cathodoluminescence microscopy and chemical analysis to characterize the carbonate materials occurring in the Tertiary marine basin. The microscopic technique with cathodoluminescence gives new informations that are not obtainable by conventional microscopic techniques. The carbonate cements in sandstones appear to be uniform with transmitted light or with crossed prisms. but the inspection with cathololuminescence reveals foraminiferal tests and rhomb crystals in the carbonate cements. The chemical analysis indicates that the intense luminescence depends mainly on the presence of$ Mn^{ 2+}$ and $Fe^{2+}$ as activator ions, but the $Fe^{2+}$ also acts as an important quencher ion when Fe concentration in dolomite is over 10,000 ppm. The dolomites, which are rich in calcium, are formed at the early stage of diagenesis at a temperature of about 60 ~ $70^{\circ}C$.

Analysis of Chemical Composition, Microstructure and Hydroxyapatite Structure for Mouse Teeth (생쥐 치아의 화학적 조성, 미세구조 및 Hydroxyapatite 구조 분석)

  • Kim, Eun-Kyung;Jeon, Tae-Hoon;Kim, Chang-Yeon;Nam, Seung-Won;Song, Kyung;Lee, Sang-Gil;Kim, Youn-Joong
    • Applied Microscopy
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    • v.40 no.3
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    • pp.147-154
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    • 2010
  • The aim of this study is to determine microstructure, chemical composition and crystal structure of hydroxyapatite for mouth teeth using optical microscopy and electron microscopy as well as electron probe micro-analysis (EPMA). Enamel, a protective cover to the teeth, consisted of rods oriented in regular and had relatively higher crystallinity and Ca component. In contrast, dentin showed a sponge-like microstructure with circular holes which were passages of dentinal tubules, and had higher Mg component than the enamel region due to its higher organic content. Hydroxyapatite crystals appeared as large rods in enamel, but as small needles in dentin. Their electron diffraction patterns were different by their crystallinity as well as by the organic content of the matrix.

A HISTOMORPHOMETRIC STUDY OF TWO DIFFERENT THREADED CP TITANIUM IMPLANTS (국내 제작 Avana 임프란트와 $Br{\aa}nemark$ 임프란트 주위 골조직에 대한 광학 및 형광 현미경학적 연구)

  • Han, Dong-Hoo;Jeon, Young-Sik;Kim, Jin;Kim, Seon-Jae
    • The Journal of Korean Academy of Prosthodontics
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    • v.37 no.4
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    • pp.531-541
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    • 1999
  • The purpose of this study was to compare surface roughness and bone formation around two types of threaded commercially pure titanium implants manufactured by two different companies. The test implants were manufactured by Sumin synthesis dental materials Co. (Avana, Busan, Korea), while the controls were manufactured by Nobel Biocare (MK II, Goteborg, Sweden). To compare bone formation adjacent to newly product implant with $Br{\aa}nemark$ MK II implant, surface roughness was measured by Accurate 1500M and histomorphometric analysis was done. The results were as follows: 1. Measurement of surface roughness showed that Avana implant had a slightly more irregular surface compared with $Br{\aa}nemark$ implant. 2. In the light microscopic studies, no infiltration of inflammatory cells nor the giant cells were observed on both groups. 3. In the light and fluorescent microscopic studies, the amount of osseointegration and the extent and the timing of bone formation were similar. 4. There were no statistically difference between two groups in the average bone to implant con-tacts. Branemark implant; 67% (SD 23%), Avana implant; 70% (SD 16%). Comparing with $Br{\aa}nemark$ implant, Avana implant made of CP grade II titanium showed similar good bone healing, formation and osseointegration.

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Anti-ulcerogenic activity of virgin coconut oil contribute to the stomach health of humankind

  • Selverajah, Malarvili;Zakaria, Zainul Amiruddin;Long, Kamariah;Ahmad, Zuraini;Yaacob, Azhar;Somchit, Muhammad Nazrul
    • CELLMED
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    • v.6 no.2
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    • pp.11.1-11.7
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    • 2016
  • The aimed of the presence study was to determine the antiulcer potential of virgin coconut oil (VCO), either extracted by wet process (VCOA) or fermentation process (VCOB), and to compare their effectiveness against the copra oil (CO) using the HCl/ethanol-induced gastric ulcer model. Earlier, the oils underwent chemical analysis to determine the free fatty acids composition, physicochemical properties and anti-oxidant capability. In the antiulcer study, rats (n=6) were pre-treated orally for 7 consecutive days with distilled water (vehicle), 100 mg/kg ranitidine (positive group) or the respective oils (10, 50, and 100% concentration). One hour after the last test solutions administration on Day 7th, the animals were subjected to the gastric ulcer assay. Macroscopic and microscopic analyses were performed on the collected rat's stomachs. From the results obtained, the chemical analysis revealed i) the presence of high content of lauric acid followed by myristic acid and palmitic acid in all oils and; ii) the significant (*p< 0.05) different in anisidine- and peroxide-value, percentage of free fatty acid, total phenolic content and total antioxidant activity among the oils. The animal study demonstrated that all oil possess significant (*p< 0.05) antiulcer activity with VCOB being the most effective oil followed by VCOA and CO. The macroscopic observations were supported by the microscopic findings. Interestingly, all oils were more effective than 100 mg/kg ranitidine (reference drug). In conclusion, coconut oils exert remarkable antiulcer activity depending on their methods of extraction, possibly via the modulation of its antioxidant and anti-inflammatory activity.

Development of Lecithin Organogel to Improve Solubility of Genistein (레시틴 오가노겔을 이용한 난용성 제니스테인의 용해도 향상)

  • Lee, Su Jin;Kim, Jung A;Kang, Nae Gyu;Park, Sun Gyoo;Lee, Cheon Koo
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.41 no.3
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    • pp.201-208
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    • 2015
  • Organogels are semi-solid systems that consist of an apolar solvent as the liquid phase within a three-dimensional networked structure. In this study, we developed a stable and skin penetration-enhanced Lecithin Organogel (LO) containing genistein, which is one of the poorly soluble active ingredients in both polar and apolar phase. After screening of various components (type of gelators, organic and aqueous phase), hydrogenated lecithin (HL), sunflower oil (SO), dipropylene glycol (DPG), and polyethylene glycol (PEG) were mainly used in this formulation. Phase ternary diagram was employed for optimization of the composition in the LO. The formulated LO were evaluated for its organoleptic characteristics, stability, pH, rheology, phase transition temperatures, microscopic analysis and skin penetration. The optimized stable LO system can be utilized as an effective and stable cosmetic formulation that can carry poorly soluble active ingredients at high concentration for topical dermal delivery.

Microscopic Evaluation and Analysis on the Tensile Strength of Hybridized Reinforcement Filament Yarns by the Commingling Process

  • Herath, Chathura Nalendra;Kang, Bok-Choon;Hwang, Beong-Bok;Min, Kyung-Ho;Seo, Jung-Min;Lee, In-Chul;Ruchiranga, Jayasekara Vishara;Lim, Joong-Yeon
    • Advanced Composite Materials
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    • v.17 no.3
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    • pp.225-233
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    • 2008
  • The analysis in this paper is focused on the pattern of mixing of filaments over a cross-section of hybrid yarns according to different combinations of reinforcement and matrix filament yarns through microscopic view. The volume content of filament in hybrid yarn cross-section was maintained at 50% for both reinforcement and matrix, and the hybrid yarns count at 600 tex throughout the experiments. It was observed from the experiments that diameters of reinforcement and matrix filaments have strong effects particularly on the pattern of mixing of filaments over a cross-section of hybrid yarns such that the hybrid yarns with more or less equal diameters of reinforcement and matrix filaments showed considerably even distributions over the hybrid yarn cross-section. This paper also investigates the possibility of hybridizing carbon/aramid, carbon/glass and aramid/glass matrices through the commingling process. In the experiment, several process parameters were selected and they include pressure, yarn oversupply-rate and different nozzle types. As a result of these experiments, it was concluded that the hybridized materials show better performance than individual reinforced filament yarns in terms of mechanical properties. For small tensile forces, the carbon/glass/matrix combination turned out to be good enough for general purpose applications.

Mechanical Anisotropy Dependent on the Rock Fabric in the Pocheon Granite and its Relationship With Microcracks (포천화강암내에 발달한 결의 역학적 이방성과 미세균열의 상관성)

  • 장보안;오선환
    • The Journal of Engineering Geology
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    • v.11 no.2
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    • pp.191-203
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    • 2001
  • We investigate mechanical anisotropy dependent of rock fabric and its relationship with microcracks in the Pocheon Granite. Uniaxial compressive strengths range from 177MPa to 212MPa and the elastic constants are 48GPa-62GPa. The tensile strengths are 6.9MPa~8.5MPa and ultrasonic wave velocities range between 3,200m/sec and 3,700m/sec, indicating that mechanical anisotropy is strongly dependent of rock fabric. The minimum anisotropy ratio is 14% and the maximum is 24%, depend on the mechanical properties. The preferred orientations of microcracks are closely related with the directions of rock fabric. The preferred orientations of microcracks in feldspar are governed by the direction of mineralogical axis and are different from the directions of rock fabric. However, microcracks in quartz grains are very long and parallel to the directions of rock fabric, indicating that directions of rock fabric may be governed by the preferred orientations of microcracks in quartz grains. The preferred orientations of microcracks measured by differential strain analysis and microscopic observation are slightly different. That may be caused by different methodology. Lengths and numbers of microcrack are measured by microscopic observation. However, differential strain analysis measures the widths of microcracks.

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