• Title/Summary/Keyword: microcracks

Search Result 270, Processing Time 0.029 seconds

Fabrication of oxide buffer layers for coated conductors (MOD 공정에 의한 산화물 완충층 제조)

  • Km Young-Kuk;Yoo Jai-Moo;Ko Jae-Woong;Chung Kuk-Chae
    • Progress in Superconductivity and Cryogenics
    • /
    • v.8 no.3
    • /
    • pp.37-40
    • /
    • 2006
  • Oxide buffer layers for YBCO coated conductors were fabricated using MOD processing and development of microstructure and texture were investigated. A $CeO_2$ buffer layers were formed on RABiTS tape. Acetate-based precursor solution was employed to synthesize the precursor solution. Subsequently, the precursor solution was stabilized and modified with triethanolamine. $CeO_2$ precursor gel film was coated and annealed in $Ar/H_2$ atmosphere at high temperature. An annealed $CeO_2$ film shows mixed orientation with high (001) texturing. It was shown that (111) texture of $CeO_2$ layers were enhanced by multiple coating. This degradation was attributed to development of microcracks in the multiply coated $CeO_2$ films. Also discussed are the synthesis and the characterization of $La_2Zr_2O_7$ (LZO) buffer layers on RABiTS tape. A biaxially textured LZO buffer layer was fabricated with MOD processing method using metal alkoxide based precursor solution. It was shown that the LZO film were epitaxially grown on RABiTS tape and crack-free & uniform surface was obtained after annealing in $Ar/H_2$ atmosphere.

Study of strength and microstructure of a new sustainable concrete incorporating pozzolanic materials

  • Grzegorz Ludwik Golewski
    • Structural Engineering and Mechanics
    • /
    • v.86 no.4
    • /
    • pp.431-441
    • /
    • 2023
  • The aim of this paper is to present a new sustainable ternary and quaternary binder by partially replacing ordinary Portland cement (OPC) with different percentages of supplementary cementitious materials. The motivation is to reduce our dependency on OPC to reduce CO2 emission and carbon foot print. As the main substitute for the OPC, siliceous fly ash was used. Moreover, silica fume and nanosilica were also used. During examinations the main mechanical parameters of concrete composites, i.e., compressive strength (fcm) and splitting tensile strength (fctm) were assed. The microstructure of these materials was also analysed. It was found that the concrete incorporating pozzolanic materials is characterized by a well-developed structure and has high values of mechanical parameters. The quaternary concrete containing: 80% OPC, 5% FA, 10% SF, and 5% nS have shown the best results in terms of good strength parameters as well as the most favourable microstructure, whereas the worst mechanical parameters with microstructure containing microcracks at phase interfaces were characterized by concrete with more content of FA additive in the concrete mix, i.e., 15%. Nevertheless, all concretes made on quaternary binders had better parameters than the reference one. It can be stated that sustainable concrete incorporating pozzolanic materials could be good substitute of ordinary concretes.

Effect of Adhesion Strength Between Flexible Substrates and Electrodes on the Durability of Electrodes (유연 기판과 전극 사이의 접합력이 전극의 내구성에 미치는 영향)

  • Doyeon Im;Byoung-Joon Kim;Geon Hwee Kim;Taechang An
    • Journal of Sensor Science and Technology
    • /
    • v.33 no.2
    • /
    • pp.86-92
    • /
    • 2024
  • Flexible electronic devices are exposed to repeated mechanical deformation; therefore, electrode performance is an important element. Recently, a new technology has been developed to improve the adhesion strength between polymer substrates and metal thin films through the cross-linking reaction of bovine serum albumin (BSA) bioconjugation proteins; however, additional performance evaluation as an electrode is necessary. Therefore, in this study, we investigated the effect of adhesive strength between a flexible substrate and a metal thin film on the performance of a flexible electrode. Cracks and changes in the electrical resistance of the electrode surface were observed through outer bending fatigue tests and tensile tests. As a result of a bending fatigue test of 50,000 cycles and a tensile test at 10% strain, the change in the electrical resistance of the flexible electrode with a high adhesion strength was less than 40%, and only a few microcracks were formed on the surface; thus, the electrical performance did not significantly deteriorate. Through this study, the relationship between the adhesion strength and electrical performance was identified. This study will provide useful information for analyzing the performance of flexible electrodes in the commercialization of flexible electronic devices in the future.

An Experimental Study on the Dryness Judgement Criterion for Water-cooled Generator Stator Windings (수냉각 발전기 고정자의 권선 내부 건조 판정 기준 설정에 관한 실험적 연구)

  • Kim, Hee-Soo;Bae, Yong-Chae;Lee, Wook-Ryun;Lee, Doo-Young
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.34 no.2
    • /
    • pp.137-143
    • /
    • 2010
  • Complete dryness inside the stator is a necessary and sufficient condition for the leak test. Microcracks caused by high cycle fatigue due to operation are generated in stator windings, and they are interrupted by water molecules during the leak test. For this reason, during leak test, the wrong value is indicated when there are no leaks in stator windings. Generator manufacturers presents unique dryness judgment criteria for the leak test, but there is no actual criterion that accurately indicates the dryness point for the leak test. The reason is because stator winding has a complex structure and the absence of effective dryness equipment in power plants. This paper proposes a dryness judgment criterion to evaluate if inside the stator winding is dried completely and presents experimental results.

Variation of Physical and Microstructural Properties of Limestone caused by Artificial Freezing and Thawing (인공 동결-융해 풍화에 따른 석회암의 물성 및 미세구조 변화 분석)

  • Park, Jihwan;Park, Hyeong-Dong
    • Tunnel and Underground Space
    • /
    • v.25 no.5
    • /
    • pp.435-449
    • /
    • 2015
  • Physical and microstructural properties of Pungchon and Maggol limestone were investigated quantitatively during 50 cycles of artificial freezing and thawing test. There were decrease in dry weight and P,S-wave velocity, and increase in absorption rate in both rock types. Porosity, pore volume, equivalent diameter, throat thickness and pore orientation were analyzed using X-ray computed tomography images. Porosity increased, and initiation and expansion of pores were investigated as weathering progresses. Physical and microstructural variation in Maggol limestone was larger than that of Pungchon limestone because Maggol limestone has more pores and microcracks at initial state. As this study analyzes physical and microstructural properties of rock specimens comprehensively, it can be applied to further rock weathering study and can be used as fundamental data of construction and resource development in cold regions.

Interaction of cracks and precipitate particles on the REBCO superconducting layers of practical CC tapes through fractographic observations

  • de Leon, Michael;Diaz, Mark A.;Shin, Hyung-Seop
    • Progress in Superconductivity and Cryogenics
    • /
    • v.22 no.3
    • /
    • pp.7-12
    • /
    • 2020
  • Electromechanical properties of REBCO CC tapes are known to be limited by defects (cracks) that form in the brittle REBCO layer. These defects could be inherently acquired during the CC tapes' manufacturing process, such as slitting, and which can be initiated at the CC tapes' edges. If propagated and long enough, they are believed to cause critical current degradation and can substantially decrease the delamination strength of CC tapes. Currently, commercially available CC tapes from various manufacturers utilize different growth techniques for depositing the REBCO layers on the substrates in their CC tapes preparation. Their epitaxial techniques, unfortunately, cannot perfectly avoid the formation of particles, in which sometimes acts as current blocking defects, known as outgrowths. Collective research regarding the composition, size, and formation of these particles for various CC tapes with different deposition techniques are particularly uncommon in a single study. Most importantly, these particles might interact in one way or another to the existing cracks. Therefore, systematic investigation on the interactions between the cracks' development mechanism and particles on the REBCO superconducting layers of practical CC tapes are of great importance, especially in the design of superconducting devices. Here, a proper etching process was employed for the CC tapes to expose and observe the REBCO layers, clearly. The scanning electron microscope, field emission scanning microscope, and energy-dispersive x-ray spectroscopy were utilized to observe the interactions between cracks and particles in various practical CC tapes. Particle compositions were identified whether as non-superconducting or superconducting and in what manner it interacts with the cracks were studied.

Accelerated Ultrasonic Fatigue Testing Applications and Research Trends (초음파 가속피로시험 적용 사례 및 연구 동향)

  • Cho, In-Sik;Shin, Choong-Shig;Kim, Jong-Yup;Jeon, Yong-Ho
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.36 no.6
    • /
    • pp.707-712
    • /
    • 2012
  • Very high cycle fatigue (VHCF) behavior of aerospace components has emerged much attention due to their long service life. In this study, a piezoelectric ultrasonic fatigue testing (UFT) system has been developed by Mbrosiatec Co., Ltd. to study the high cycle fatigue (HCF) strength of Ti-6Al-4V alloy. Hourglass-shaped specimens have been investigated in the range from $10^6$ to $10^9$ cycles at room temperature under completely reversed R = -1 loading conditions,. Scanning electron microscopy (SEM) analysis revealed that failures occurred in the entire range up to the gigacycle regime, and the fractures have beenfound to be initiated from the surface, unlike in steels. However, it was found from the SEM microgprahs that microcracks transformed into intergranular fractures. Thus, it can be concluded from according to the results that this test method can be applicable to commercialized automotive and railroad parts that require high cycle fatigue strength.

Field Tests of Hydraulic Rock Splitting Technique Using Arrays of Injection Holes with Guide Slots (유도슬롯과 주입공 배열을 이용한 수압암반절개 현장 실험)

  • Park, Jong Oh;Woo, Ik
    • The Journal of Engineering Geology
    • /
    • v.29 no.4
    • /
    • pp.405-415
    • /
    • 2019
  • The cracks induced by hydraulic rock splitting technique are formed in the direction parallel to the free plane, which is perpendicular to the minimum principal stress of the ground, or is affected by the pre-existing microcracks. In this study, the hydraulic rock splitting experiments were conducted in which the guide slot was engraved in the direction parallel to the borehole axis on the biotite granite slope, and the hydraulic pressure was injected through the double packer pressure and interval section. The test results show that the cracks along with the guide slots were induced either by the double packer pressurization or the injection of hydraulic pressure into interval section, some cracks extended across the boreholes. Therefore, the hydraulic rock splitting test is expected to control efficiently the induced cracks if the guide slots are engraved in the direction of splitting and a big flow rate is applied.

A Study on the Measurement of Acoustic Emission and Deformation Behaviors of Rock and Concrete under Compression (암석 및 콘크리트의 압축변형거동과 미소파괴음 측정에 관한 연구)

  • 심현진;이정인
    • Tunnel and Underground Space
    • /
    • v.10 no.1
    • /
    • pp.59-69
    • /
    • 2000
  • Acoustic emission is n burst of microseismic waves generated by microscopic failure due to deformation in materials. The study on the detection of initiation and propagation of microcracks from acoustic emission measurement is very important for the evaluation of the stability of underground rock structures by the nondestructive letting method. In this study, acoustic emission was measured under uniaxial stiffness loading test used to obtain the complete stress-strain curves of marble and concrete used as reinforced materials of rock structures. The analysis of acoustic emission parameters and source location were performed to discuss the characteristics of the deformation and failure behavior of rock and concrete. And acoustic emission was measured under cyclic loading test to verify the Kaiser effect associated with the damage of materials, in situ stress of rock, and stress history of concrete structure.

  • PDF

Physical Properties of Rocks according to Heating Treatment (열충격 시험에 의한 암석의 물성변화)

  • Kim, Jae-Hwan;Lee, Myeong-Seong;Lee, Jae-Man;Lee, Mi-Hye;Park, Sung-Mi
    • 보존과학연구
    • /
    • s.31
    • /
    • pp.31-42
    • /
    • 2010
  • This study were performed thermal shock test for four kind of different rocks (Iksan granite, Namsan granite, Jeongseon marble, Yeongyang sandstone), and according to heating temperature($400^{\circ}C$, $600^{\circ}C$) on samples were investigated physical properties such as specify gravity, porosity, p-wave velocity. As a result, the tendency was appeared that porosity increased, and specific gravity and p-wave velocity decreased at a more higher temperature. But, the situation of change appeared characteristic according to temperature and rock types. In the case of Yeongyang sandstone, it appeared in especially porosity increasing at $400^{\circ}C$. The specific gravity was little change in the all the rock at $400^{\circ}C$ but the decreased at $600^{\circ}C$. Therefore the specific gravity in the temperature range is due to the relatively small impact on the change is expected. Porosity of the granite at $400^{\circ}C$ changes little. but marble in the rate of change is large. Conversely, the sandstone porosity decreased. At $600^{\circ}C$ increased porosity in all of rocks. particularly sandstone the smallest increase in porosity. Experiments showed that p-wave velocity measured through dry rocks was sensitive to quantify the thermal damage. The p-wave velocity of all rocks decreased with increasing temperature. In the relation between porosity and p-wave velocity, p-wave velocity decreased with increasing porosity. On the other hand, in case of Yeongyang sandstone p-wave velocity decreased with decreasing porosity. thus, development of microcracks more affects p-wave velocity than porosity. In this study, damage intensity was well explained with porosity and p-wave velocity values depending on temperature increase.

  • PDF