• Title/Summary/Keyword: micro-crack development

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A development of fabrication processes of microstructure using SU-8 PR (SU-8 PR을 이용한 마이크로 구조물 제작 공정 개발)

  • 김창교;장석원;노일호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.2
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    • pp.68-72
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    • 2003
  • In this paper, we developed a new thick photoresist fabrication technology for 3-dimensional microstructures. In general, like as AZ photoresist was coated with thin film thickness about 1 $\mu\textrm{m}$ to 30 $\mu\textrm{m}$, but photoresist like SU-8 has thickness of several tens $\mu\textrm{m}$ or more and high aspect ratio. When we fabricate a microstructure using the thick photoresist like SU-8, cracks on the SU-8 thick photoresist are appeared by stress which was caused by sudden cooling down during bake of the thick photoresist spun on wafer. Thus, it was hard to fabricate the microstructure using the thick photoresist for electroplating. In this paper, we developed a new process to produce a 3-dimensional microstructure without the crack by stress through a suitable thick photoresist coating, time control of cool down and time control of PEB (Post Expose Bake).

Development and Assessment of Laboratory Testing Apparatus on Grouting Injection Performance (그라우팅 주입성능 실내실험 장비 개발 및 신뢰도 평가)

  • Jin, Hyunwoo;Ryu, Byunghyun;Lee, Jangguen
    • Journal of the Korean GEO-environmental Society
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    • v.17 no.10
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    • pp.23-31
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    • 2016
  • Grout is generally operated with low viscous material similar to water, but grout for micro crack with high viscous materials and high injection pressure is gradually increased under the development of underground and subsea space. In order to estimate grouting injection performance considering crack width, viscosity of grouting materials, and injection pressure, there should be a reliable standard laboratory testing method. In this paper, theoretical injection mechanisms of grouting materials are presented as radial and linear flows, and laboratory testing apparatus are introduced to simulate each flow case. Radial flow is simulated by using acrylic disk plates which are able to spread grouting material radially from the center of the disk plates, and linear flow is simulated by using stainless parallel plane plates which are able to spread grouting material linearly. Apparatus are consist of upper and lower plates and industrial films with different thickness are placed between plates in order to simulate various crack widths. Laboratory verification tests with these apparatus were conducted with tap water (1cP at $20^{\circ}C$) as an injection material. Through the laboratory testing results, the best laboratory testing method is recommended in order to estimate grouting injection performance.

A Numerical Model for the Freeze-Thaw Damages in Concrete Structures

  • Cho Tae-Jun
    • Journal of the Korea Concrete Institute
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    • v.17 no.5 s.89
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    • pp.857-868
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    • 2005
  • This paper deals with the accumulated damage in concrete structures due to the cyclic freeze-thaw as an environmental load. The cyclic ice body nucleation and growth processes in porous systems are affected by the thermo-physical and mass transport properties, and gradients of temperature and chemical potentials. Furthermore, the diffusivity of deicing chemicals shows significantly higher value under cyclic freeze-thaw conditions. Consequently, the disintegration of concrete structures is aggravated at marine environments, higher altitudes, and northern areas. However, the properties of cyclic freeze-thaw with crack growth and diffusion of chloride ion effects are hard to be identified in tests, and there has been no analytic model for the combined degradations. The main objective is to determine the driving force and evaluate the reduced strength and stiffness by freeze-thaw. For the development of computational model of those coupled deterioration, micro-pore structure characterization, pore pressure based on the thermodynamic equilibrium, time and temperature dependent super-cooling with or without deicing salts, nonlinear-fracture constitutive relation for the evaluation of internal damage, and the effect of entrained air pores (EA) has been modeled numerically. As a result, the amount of ice volume with temperature dependent surface tensions, freezing pressure and resulting deformations, and cycle and temperature dependent pore volume has been calculated and compared with available test results. The developed computational program can be combined with DuCOM, which can calculate the early aged strength, heat of hydration, micro-pore volume, shrinkage, transportation of free water in concrete. Therefore, the developed model can be applied to evaluate those various practical degradation cases as well.

High Ductile Fiber Reinforced Concrete with Micro Fibers (마이크로 섬유를 혼입한 고인성 섬유 보강 콘크리트)

  • Shin, Kyung-Joon;Lee, Seong-Cheol;Kim, Yun-Yong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.2
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    • pp.92-98
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    • 2019
  • In general, high strength and high performance fiber reinforced cement composites exclude coarse aggregates basically in order to have homogeneous distributions of material properties. However, these fiber-reinforced cement mortar without coarse aggregate have a tenancy that the modulus of elasticity is low and the unit weight of cement is high, resulting in low economic efficiency. Therefore, in this study, the development of high ductile fiber - reinforced concrete was conducted, which has the adequate level of coarse aggregate but still retains the high flexural toughness and strength and also has the crack - distributing performance. Experimental study was carried out by using the amount of coarse aggregate as an experimental parameter. The results showed that the best flexural toughness and crack dispersion characteristics was obtained when the coarse aggregate was added at 25% by weight of the fine aggregate to the typical mixtures of high ductile cement mortar. PVA fiber was effective in crack distribution and ductility enhancement, and steel fiber was effective in strengthening flexural strength rather than crack distribution.

Development of the stone surface process equipment by Water Jet System (워터젯 시스템을 이용한 석재표면처리장치 개발)

  • 강지호;장명환
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.26 no.3
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    • pp.31-38
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    • 2003
  • There is boner process of stone manufacturing to become quality down of stone to consolidated micro crack appearance of stone surface and biotite by fire that is to be route process in stone surface by flame of LPG. And then, it is develop that stone surface process equipment by automation for the work method of boner process can be substitute work method by water jet To development of equipment, There is to be down noise and dust. According to remove calamity growth hazardous substance in the work environment, there is to solve workplace avoidance factor.

An Experimental Study on Development of Eco-Friendly Color Concrete Using Industrial Waste Red Mud (산업폐기물 레드머드를 사용한 친환경 칼라 콘크리트 개발에 관한 실험적 연구)

  • Jeong, Dong-Young;Choi, Kyoung-Rag;Kim, Moon-Hoon;Hong, Chong-Hyun
    • Journal of Environmental Science International
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    • v.16 no.8
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    • pp.929-939
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    • 2007
  • Red mud is a waste generated by the aluminium industry, and its disposal is a major problem for this industry. Red mud has a reddish-brown color and superfine particle characteristics. So, it can be a promising pigment admixture for concrete industry. An experimental study was conducted to investigate the potential use of red mud in color concrete. The micro structures of red mud and iron oxide pigment such as porosity, pore size distribution, diameter of particle were analyzed with the aid of SEM, X-ray diffraction(XRD), and the infrared absorbance. Tests on physical properties of color concrete, such as strength, slump, early shrinkage crack patterns, and color characteristics were carried out and the results were reported in this paper.

Micro-silica Mixed Aqua-epoxy for Concrete Module Connection in Water : Part 2 - Structural Application and Evaluation (해상 프리캐스트 콘크리트 부유체 모듈 가접합을 위한 마이크로 실리카 혼입 수중용 에폭시 접합 성능 검토 : Part 2 - 구조 접합 성능 평가)

  • Choi, Jin-Won;You, Young-Jun;Jeong, Youn-Ju;Kwon, Seung-Jun;Kim, Jang-Ho Jay
    • Journal of the Korea Concrete Institute
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    • v.27 no.1
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    • pp.29-35
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    • 2015
  • Recent studies to develop Very Large Floating Structure(VLFS) has shown that the construction procedure of the structure needs to acquire precast concrete module connection system using prestressing. However, the loads occurring on water are complex combinations of various condition, so the safe and stable performance of the module joints and bonding materials are key to the success of the construction. Therefore, micro-silica mixed aqua-epoxy development was introduced in Part 1 using a bonding material developed in this study. The performance of the micro-silica mixed aqua-epoxy(MSAE) applied joint of concrete module specimens connected by prestressing tendon was evaluated to verify the usability and safety of the material. RC beam, spliced beam connected by prestressing tendon and MSAE, and continuous prestressed concrete beam were tested for their initial cracking and maximum loads as well as cracking procedure and pattern. The results showed that the MSAE can control the stress concentration effect of the shear key and the crack propagation, and the maximum load capacity of MSAE joint specimens are only 5% less than that of continuous RC specimen. The details of the study are discussed in detail in the paper.

Development of SiC Composite Solder with Low CTE as Filling Material for Molten Metal TSV Filling (용융 금속 TSV 충전을 위한 저열팽창계수 SiC 복합 충전 솔더의 개발)

  • Ko, Young-Ki;Ko, Yong-Ho;Bang, Jung-Hwan;Lee, Chang-Woo
    • Journal of Welding and Joining
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    • v.32 no.3
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    • pp.68-73
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    • 2014
  • Among through silicon via (TSV) technologies, for replacing Cu filling method, the method of molten solder filling has been proposed to reduce filling cost and filling time. However, because Sn alloy which has a high coefficient of thermal expansion (CTE) than Cu, CTE mismatch between Si and molten solder induced higher thermal stress than Cu filling method. This thermal stress can deteriorate reliability of TSV by forming defects like void, crack and so on. Therefore, we fabricated SiC composite filling material which had a low CTE for reducing thermal stress in TSV. To add SiC nano particles to molten solder, ball-typed SiC clusters, which were formed with Sn powders and SiC nano particles by ball mill process, put into molten Sn and then, nano particle-dispersed SiC composite filling material was produced. In the case of 1 wt.% of SiC particle, the CTE showed a lowest value which was a $14.8ppm/^{\circ}C$ and this value was lower than CTE of Cu. Up to 1 wt.% of SiC particle, Young's modulus increased as wt.% of SiC particle increased. And also, we observed cross-sectioned TSV which was filled with 1 wt.% of SiC particle and we confirmed a possibility of SiC composite material as a TSV filling material.

Temperature Effect on Tensile Strength of Filled Natural Rubber Vulcanizates (가황 천연고무의 인장강도에 미치는 온도의 영향)

  • Ko, Young-Chon;Park, Byung-Ho
    • Elastomers and Composites
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    • v.36 no.4
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    • pp.255-261
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    • 2001
  • This study was related with the effect of elevated temperature on the tensile strength of edge-cut samples. There was a different tensile strength behavior of uncut samples and pre-cut samples under different test temperatures. Tensile strength of uncut sample decreases with increasing test temperature. When pro-cut size(C) is larger than critical cut size($C_{cr}$), tensile strength or pre-cut specimen at $80^{\circ}C$ is higher than that of pre-cut specimen at room temperature (RT). Test specimens under $80^{\circ}C$ condition exhibited more secondary cracks at the crack tip region compared to room temperature conditions. However, secondary cracks of pre-cut specimens are not clearly developed at $110^{\circ}C$. Differences in tensile strength induced by different test temperature seem to be responsible for the strain-induced crystallization and micro-cracking patterns.

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Mechanical Property and Microstructure of the Annealed Fe-Si Alloy Manufactured by Laser-Powder Bed Fusion (L-PBF 공정 처리된 Fe-Si 합금의 열처리 조건에 따른 미세조직 및 기계적 특성)

  • J. Y. Park;M. S. Gwak;S. G. Jeong;H. S. Kim;J. G. Kim
    • Transactions of Materials Processing
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    • v.32 no.2
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    • pp.67-73
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    • 2023
  • To overcome a climate change, manufacturing complex-shaped electric mobility parts becomes one of the important issues for enhancing a performance of motor with reducing their weight. Therefore, development of laser-based additive manufacturing shed on light due to their flexible manufacturing capacity that can be suitable to solve the poor formability of Fe-Si alloys for electric mobility parts. Although there are several studies existed to optimize the performance of additively manufactured Fe-Si alloys, the post-annealing effect was not well investigated yet though this is important to control the texture and mechanical properties of additively manufactured parts. In the present work, annealing effect on the mechanical property and microstructure of additively manufactured Fe-4.5Si alloy was investigated. Because of the ordered phase initiation after annealing, the hardness of additively manufactured Fe-4.5Si alloy increased up to 1173 K while a hardness drop occurs at the 1273 K condition due to the micro-crack initiation. The response surface methodology result represents the 1173 K-5 h sample is an optimal condition to maximize the mechanical property of additively manufactured alloy without micro-cracks.