• 제목/요약/키워드: melting time

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국산 가래나무 간벌재활용을 위한 금속주입목재의 제조 및 특성 (Properties and Manufacturing of Low Melting Alloy Impregnated Wood Composites for using Domestic Thinned Logs of Juglans mandshurica)

  • 박계신;이화형
    • 농업과학연구
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    • 제37권3호
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    • pp.457-464
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    • 2010
  • The low melting alloy impregnated wood composites with natural grain of thinned Juglans mandshurica was made and evaluated in this study. And the proper manufacturing conditions was also investigated in this study. The low melting alloy with bismuth(Bi) and tin(Sn) which are harmless to humans, was applied for this novel composites, which showed not only no defects of discoloration, delamination, swelling, and cracking, because of high dimensional stability and low thickness swelling, but also much improved performance such as high bending strength, high hardness, low abrasion, high thermal conductivity as floor materials. This study also suggested the proper impregnating condition, such as 10 minutes of the preliminary vacuum time, $187^{\circ}C$ of the heating temperature and 10 minutes of the maintaining pressure time at the pressure of 30kgf/$cm^2$. The produced composites showed 9 times higher density for small specimen, 6.6 times for actual size sample and great increase in bending strength from 102.05N/$mm^2$ to 189.47N/$mm^2$ for small size sample and to 205.4N/$mm^2$ for actual size sample, also great increase in hardness from 15.1N/$mm^2$ to 73.38N/$mm^2$ for small size sample and 64.87N/$mm^2$ for actual size sample. And the composites demonstrated great decrease in abrasion depth and in water absorption.

폴록사머를 이용한 디클로페낙 고형 좌제의 개발 (Development of Poloxamer-Based Solid Suppository Containing Diclofenac Sodium)

  • 용철순;오유경;김정애;김용일;박상만;양준호;이종달;최한곤
    • Journal of Pharmaceutical Investigation
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    • 제34권2호
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    • pp.91-94
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    • 2004
  • To develop a poloxamer-based solid suppository with poloxamer mixtures, the melting points of various formulations composed of P 124 and P 188 were investigated. To investigate the effect of poloxamer to the dissolution ad dissolution mechanism of diclofenac sodium from the suppository the dissolution of diclofenac sodium delivered by the poloxamer-based suppository was performed. Furthermore, to investigate the mucoadhesive property of the poloxamer-based sold suppository, the identification test in the rectum was carried out after its rectal administration in rats. The poloxamer mixtures composed of P 124 and P 188 were homogeneous. Ver small amounts of P 188 affected the melting points of poloxamer mixtures. In particular, the poloxamer mixture [P 124/P 188 (97/3%)] with the melting point of about $32^{\circ}C$ was a sold for at room temperature and instantly melted at physiological temperature. Furthermore, very small amounts of P 188 in the poloxamer-based suppository hardly affected the dissolution rates of diclofenac sodium from the suppository. Dissolution mechanism analysis showed the dissolution of diclofenac sodium was proportional to the time. At 4 h after administration, the blue colo of poloxamer-based suppository [diclofenac sodium/poloxamer mixture (2.5/97.5%)] with the P 124/ P 188 ratio of (97/3%) and blue lake in the rectum was faded. However, the position of suppository in the rectum did not significantly change with time. Thus, it retained in thε rectum for at least 4 h. Our results indicated that the poloxamer-based sold suppository with P 124 and P 188 would be a candidate of rectal dosage form for diclofenac sodium.

적시 생산 방식에서의 주조공정 스케줄링 (Scheduling of a Casting Sequence Under Just-In-Time (JIT) Production)

  • 박용국;양정민
    • 산업경영시스템학회지
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    • 제32권3호
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    • pp.40-48
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    • 2009
  • In this article, scheduling of a casting sequence is studied in a casting foundry which must deliver products according to the Just-in-time(JIT) production policy of a customer. When a foundry manufactures a variety of casts with an identical alloy simultaneously, it frequently faces the task of production scheduling. An optimal casting schedule should be emphasized in order to maximize the production rate and raw material efficiency under the constraints of limited resources; melting furnaces and operation time for a casting machine. To solve this practical problem-fulfilling the objectives of casting the assigned mixed orders for the highest raw material efficiency in a way specified by the customer's JIT schedule, we implement simple integer programming. A simulation to solve a real production problem in a typical casting plant proves that the proposed method provides a feasible solution with a high accuracy for a complex, multi-variable and multi-constraint optimization problem. Employing this simple methodology, a casting foundry having an automated casting machine can produce a mixed order of casts with a maximum furnace utilization within the due date, and provide them according to their customer's JIT inventory policy.

스컬용융법에 의한 패각을 이용한 큐빅지르코니아 단결정 성장 (Cubic zirconia single crystal growth using shell by skull melting method)

  • 정진화;연석주;석정원
    • 한국결정성장학회지
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    • 제23권3호
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    • pp.124-128
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    • 2013
  • 본 연구에서는 안정화제로, 패각으로부터 정제한 CaO를 사용하여 Skull melting법으로 큐빅 지르코니아를 성장시켰다. 꼬막 패각을 HCl을 0.1~1 mol%로 1차 처리한 후 수화반응을 거쳐 최적의 처리시간과 농도를 검토하였다. HCl을 1 mol%의 농도로 처리했을 때 가장 순도가 높았으며 수화반응시 $45^{\circ}C$의 온도로 24시간 동안 반응시킬 때 완전한 $Ca(OH)_2$ 를 얻을 수 있었다. $Ca(OH)_2$$1200^{\circ}C$에서 5시간 처리하였을 때 CaO의 순도가 가장 높게 측정되었다. 패각으로부터 얻어진 CaO를 $ZrO_2$에 첨가하여 함량을 10~30 mol% 로 변화시켜 Skull melting법으로 단결정을 성장시켰다. Skull melting법에 사용된 고주파 발진기의 주파수는 약 3.4 MHz이며 단결정의 하강속도는 시간당 3 mm로 4 cm 길이로 성장시켰다. 실험결과 CaO의 함량이 15 mol% 일 때 결정성이 가장 우수했다.

수평식 셸-튜브형 잠열축열조의 축열 및 방열특성에 관한 실험적 연구 (An Experimental Study on Heat Storage and Heat Recovery Characteristics of a Latent Heat Storage Tank with Horizontal Shell and Tube Type)

  • 권영만;서해성;모정하
    • 대한기계학회논문집B
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    • 제24권1호
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    • pp.50-59
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    • 2000
  • An experimental study has been carried out in order to investigate the heat storage characteristics for a latent heat storage tank with horizontal shell and tube type. The heat exchanger consisted of horizontal cylindrical capsules with a staggered tube bank layout. Based on the obtained data, the effects of flow rate and inlet fluid temperature on the melting time and heat storage rates were examined. It is found that the melting time decreased with increase of the flow rate and the inlet temperature. Results also show that at the initial stage of heat transfer the heat storage rate represents the maximum value and rapidly decreases.

Shape-Stabilized Phase Change Materals : Frozen Gel from Polypropylene and n-Octadecane For Latent Heat Storage

  • Son, Tae-Won;Kim, Tae-Hun;Kim, Bong-Shik;Kim, Byung-Giu
    • 한국고분자학회:학술대회논문집
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    • 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
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    • pp.375-375
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    • 2006
  • The preparation methods are to be used as "melting method" and "absorption method", respectively. The reaction mixture in the reaction container was heating up the reaction mixture to $200^{\circ}C$ for 2 hour. The mixing time of lab scale preparation should be provided quit long, instead of the short working time in a compounder vessel. And The PP-PCM mixture in the reaction container was heating up the mixture around $60-80^{\circ}C$ for 2 hour. A melting method of frozen gel with 50/50 weight ratio of polypropylene-normal octadecane was prepared by adding PP chip and normal octadecane. An absorption method of frozen gel with 70/30 weight ratio of PP 4.8-normal n-octadecane was prepared by adding PP powder and normal octadecnae.

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Ni/B/Ni 액상확산접합계의 액상폭에 관한 연구 (A Study on the Width of Liquid Layer of Ni/B/Ni Diffusion Bonding System)

  • 정재필;강춘식
    • Journal of Welding and Joining
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    • 제13권4호
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    • pp.147-154
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    • 1995
  • In order to study the bonding mechanism of Ni/B/Ni transient liquid phase bonding system, width of liquid layers were calculated, where in this system melting point of insert material(B) is higher than bonding temperature and melting point of base metal(Ni). Caclulated values were compared with experimental ones which were measured by bonding Ni/B/Ni system at 1433-1474K under vacuum atmosphere. As results, the width of initial liquid layer of Ni/B/Ni system was calculated as $W_{IL}$ = $W_{o}$[1 + {2.100..rho.$_{S/}$ ( $X_{3}$ + $X_{4}$)..rho.$_{Ni}$ }-.rho.$_{S/}$.rho. Ni/], and it was nearly same with experimental values. Maximum width of liquid layer, width of liquid layer during isothermal solidification and isothermal solidification time were calculated also.o.o.o.

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용융법에 의한 수용성 유리의 제조 및 특성 (I) : 용해 특성, 살균 효과 및 세포 독성 (Preparation and Characterization of Water-Soluble Glass through Melting Process (I) : Dissolution Characteristics, Bactericidal Effects and Cytotoxicity)

  • 조종호;이용근;최세영;신철수;김경남
    • 한국세라믹학회지
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    • 제32권10호
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    • pp.1093-1102
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    • 1995
  • Water-soluble phosphate glasses containing Ag or Cu ion were prepared through melting process. Then the powdered glass samples were dissolved in D.I. water at room temperature with changing the dissolution time. In terms with the glass composition, dissolution characteristics, bactericidal effects and cytotoxicities were investigated. Dissolved amounts increased uniformly with dissolution time, and the dissolution rate was higher for ternary glass than for binary glass and with less metal oxide amount. And the dissolution rate of the glass with Ag ion was higher than that with Cu ion, and the bactericidal effect of the glass with Ag ion was also greater. Solution with more than 25 ppm of Ag was observed to have strong cytotoxicity to L929, and solutions of lower Ag concentration or with Cu seemed to have little cytotoxicity.

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동결과정을 포함한 다공층에서 자연대류에 대한 유한요소 해석 (Finite element solutions of natural convection in porous media under the freezing process)

  • 이문희;최종욱;서석진;박찬국
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 춘계학술대회논문집B
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    • pp.51-56
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    • 2000
  • The Finite Element Solutions Is reported on solid-liquid phase change in porous media with natural convection including freezing. The model is based on volume averaged transport equations, while phase change is assumed to occur over a small temperature range. The FEM (Finite Element Method) algorithm used in this study is 3-step time-splitting method which requires much less execution time and computer storage the velocity-pressure integrated method and the penalty method. And the explicit Lax-Wendroff scheme is applied to nonlinear convective term in the energy equation. For natural convection including melting and solidification the numerical results show reasonable agreement with FDM (Finite Difference Method) results.

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Competition between Phase Separation and Crystallization in a PCL/PEG Polymer Blend Captured by Synchronized SAXS, WAXS, and DSC

  • Chuang Wei-Tsung;Jeng U-Ser;Sheu Hwo-Shuenn;Hong Po-Da
    • Macromolecular Research
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    • 제14권1호
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    • pp.45-51
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    • 2006
  • We conducted simultaneous, small-angle, X-ray scattering/differential scanning calorimetry (SAXS/DSC) and simultaneous, wide-angle, X-ray scattering (WAXS)/DSC measurements for a polymer blend of poly($\varepsilon$-caprolactone)/poly(ethylene glycol)(PCL/PEG). The time-dependent SAXS/DSC and WAXS/DSC results, measured while the system was quenched below the melting temperature of PCL from a melting state, revealed the competitive behavior between liquid-liquid phase separation and crystallization in the polymer blend. The time-dependent structural evolution extracted from the SAXS/WAXS/DSC results can be characterized by the following four stages in the PCL crystallization process: the induction (I), nucleation (II), growth (III), and late (IV) stages. The influence of the liquid-liquid phase separation on the crystallization of PCL was also observed by phase-contrast microscope and polarized microscope with 1/4$\lambda$ compensator.