• Title/Summary/Keyword: magnetic separation

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Thermal Decomposition of Arsenopyrite by Microwave Heating and the Effect of Removal Arsenic with Wet-magnetic separation (마이크로웨이브 가열에 의한 황비철석의 열분해와 습식-자력선별에 의한 비소 제거 효과)

  • On, Hyun-Sung;Kim, Hyun-Soo;Myung, Eun-Ji;Lim, Dae-Hack;Park, Cheon-Young
    • Journal of the Mineralogical Society of Korea
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    • v.30 no.3
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    • pp.103-112
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    • 2017
  • In order to transform arsenopyrite into pyrrhotite and to decrease As content by less than 2,000 mg/kg, pulp sample and non-magnetic pulp sample were heated in a microwave oven at different heating times and were separated through wet-magnetic separation. As the microwave heating time increased, the phase of pyrrhotite was extended to become arsenopyrite entirely. The melting pores and micro-cracks occurred on the pyrrhotite due to hot spot phenomenon with microwave heating. The heated raw pulp sample (As content : 19,970.13 mg/kg) and non-magnetic pulp sample (As content : 19,970.13 mg/kg) which were heated in a microwave oven for 10 minutes were separated through wet-magnetic separation and magnetic fraction containing less than 2,000 mg/kg of As content was recovered only from the heated sample of magnetic separation. It was discovered that for the sulfide complex ore with As penalty imposed on, if microwave heating and wet-magnetic separation are effectively utilized, magnetic fraction. We expect to be able to obtain ore minerals with an arsenic content below the penalty charge.

Concentration of As Component in Pb Dross by Magnetic Separation (자력선별에 의한 납드로스 중 비소성분의 농축)

  • Choi, Sanghyeon;Na, Hyunjin;Yoo, Kyoungkeun
    • Resources Recycling
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    • v.28 no.3
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    • pp.53-58
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    • 2019
  • Pb dross has been generated from recycling processes of waste acid lead batteries, and proper treatment of Pb dross was required because it contains As component, which has been found to be toxic. This study is aimed at concentrating As component by magnetic separation of ground product obtained from ball and mixer milling of Pb dross. No arsenic component was detected in the non-magnetic product of 10000 G magnetic separation using ground product with $-150{\mu}m$ by ball milling, and As could be concentrated upto 18.87 % by further 2000 G magnetic separation. The ball mill ground product with over $300{\mu}m$ was ground again by mixer mill to less than $150{\mu}m$, and then magnetic-separated by 4000 G followed by 2000 G magnet. The As component was concentrated upto 21.021 % in the magnetic fraction of 2000 G. It was confirmed that As component exsit as $Fe_2As$ by XRD measrument. These results indicate that As component could be concentrated from 0.6 % in the Pb dross to 21.021 % in the magnetic fraction by milling followed by magnetic separation.

The review of IFMFC (International Forum on Magnetic Force Control) -The accumulated knowledge and experience of the magnetic force control with IFMFC

  • Watanabe, Tsuneo
    • Progress in Superconductivity and Cryogenics
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    • v.20 no.2
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    • pp.20-23
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    • 2018
  • The practical use of superconducting magnets is limited to medical equipment, energy equipment and the like. Therefore, it does not fully utilize the superior features of superconducting magnet or magnetic force. In order to overcome this blockage condition, The international Forum on Magnetic Force Control (IFMFC) was launched in Tokyo in 2010 by the magnetic separation researchers in Japan, Korea and China. The policy is to hold around the country every year, to apply the application to the engineering field of magnetic force utilization and information exchange about the development of applied science to mutual visit of researchers and to develop the application field of superconducting magnets in particular. The main object is to review the field of application of magnetic force with respect to published papers at 8 IFMFCs, and to introduce the trend of research forum utilizing strong magnetic force which is rare in the world. The United Nations is asking each country to achieve Corporate Social Responsibility (CSR) targets for 2030. This IFMFC review will be utilized in this field.

Removal of Iron Bearing Minerals from Illite (일라이트에 함유된 Fe 불순물 제거)

  • Kim, Yun-Jong;Cho, Sung-Baek;Park, Hyun-Hae;Kim, Sang-Bae
    • Korean Journal of Materials Research
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    • v.16 no.8
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    • pp.497-502
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    • 2006
  • Recently, many attention have been focused on illite as a material for the well-being industry. Illite contains various kinds of iron bearing materials and they restrict their usage. In this study, Fe impurities in the illite produced in Yeongdong-gun, Chungcheongbuk-do were characterized and their removal experiments were performed. According to the characterization of illite raw ore, it contained 1.54 wt.%$Fe_2O_3$ due to the existence of iron oxide($Fe_2O_3$) and pyrite($FeS_2$). The raw ore was crushed into 3 mm or less using cone crusher and then ground by rod mill for the liberation of impurity mineral. For the removal of iron bearing minerals, an acid treatment, a flotation, a magnetic separation, and a flotation combined with magnetic separator were performed respectively. When the illite raw ore was treated with magnetic separation and various kinds of acid, 1.54wt.%. $Fe_2O_3$ content was reduced to 0.78 and 1.0 wt.%, respectively. On the other hand $Fe_2O_3$ content was reduced to be 0.52 wt.% after flotation. These results indicate that iron bearing minerals cannot be reduced below 0.3wt.%$Fe_2O_3$. However, combination of magnetic separation and flotation enable us to get 0.24wt.% of illite concentrate. It is concluded that, for the refinement of illite from Yeongdong-gun, the flotation combined with magnetic separation is good for high purity illite.

Concentrating Effect of Heavy Metals from Heavy Metal Contaminated Soil by Magnetic Separation (중금속오염 토양의 자기분리에 의한 오염농축효과)

  • Kim, Jee-Eun;Kim, Jeong-Jin;Kim, Young-Hun
    • Journal of the Mineralogical Society of Korea
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    • v.27 no.4
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    • pp.311-320
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    • 2014
  • A magnetic separation study was conducted for a soil sampled from a landfill site where steel slag had been dumped for a long time. Heavy metal concentrating effect was evaluated by analyzing heavy metal content of magnetically separated soil and passed through soil. The effect was compared between soil after soil-washing process and original landfill soil and the effect was also tested between wet condition-magnetic separation and dry condition-magnetic separation. Separated ratio was relatively higher in non-soil washed sample. The water content has no significant effect on the separation rate. The concentrating effect of Fe, Pb, Cu, and Cd were 3.2, 2.1, 12.1, 2.5, 1.5 and 17.4, 7.0, 15.7, 9.6, 7.0 respectively for non-soil washed sample and soil washed sample. We can expect a bigger volume reduction effect from soil-washed samples. The volume reduction effect was obtained from the separation in dry condition. However, when the separation ratio is too high the volume reduction effect decreases. The magnetic separation leads to a volume reduction and concentration of heavy metals into a portion of soil in case of paramagnetic particles contained soil.

Design simulation of magnetic separator for purification of silica sand (자력선별방식을 이용한 고순도 실리카 정제 최적화를 위한 전산모사)

  • Choi, Hyun-Jin;Jo, Young Min;Lee, Jun Yub;Kim, Sang Bum
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.1
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    • pp.181-187
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    • 2016
  • Silica is an essential material in the electronics industries of LCDs and OLEDs, which particularly require high purity. This study attempted to find the optimal design of a magnetic separator for silica sand containing iron compounds using CFD simulation. Three designs of magnetic separation were prepared and their efficiency was examined. As a result of the evaluation, the sufficient contact of particulate silica with the surface of magnetic emitters improved the magnetic separation effects. In addition, the loss of $SiO_2$ and the removal rate of $Fe_2O_3$ depended strongly on the particle size, flow rate and magnetic flux density. In addition, magnetic separation is quite effective for a particle size of $10{\mu}m$ with a 0.2 m/s flow rate.

High Throughput Magnetic Separation for Human DNA by Aminosilanized Iron Oxide Nanoparticles (아미노실란화 철산화물 나노입자를 이용한 Human DNA의 초고속 자성분리)

  • Kang, Ki-Ho;Chang, Jeong-Ho
    • Journal of the Korean Ceramic Society
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    • v.45 no.10
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    • pp.605-609
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    • 2008
  • This work describes the preparation of functionalized magnetic nanoparticles(MNPs) and their bioapplication to human DNA separation. Silica coated MNPs were prepared by changing the volume ratio of tetraethyl orthosilicate(TEOS) for controlled coating thickness on the original nanoparticle of MNPs. The sol-gel process in silica coating on MNPs surface was adapted for relatively mild reaction condition, low-cost, and surfactant-free. And then amino functionalized magnetic nanoparticles were synthesized using amine groups as surface modifiers. The result of adsorption efficiency for human DNA with amino-functionalized silica coated MNPs was calculated as a function of the number of amine groups.

The optimized recover process of heavy minerals from Korean beach-sand

  • Shin, Hee-Young;Jeon, Ho-Soek;Baik, Seung-Woo;Kim, Wan-Tae;Lee, Jae-Chun
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.648-653
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    • 2003
  • Optimized recovery of heavy minerals from the near shore sands of Korean Yellow Sea was investigated using physical processing technologies such as gravity concentration and magnetic separation. The head samples were subjected to the three stages effective separation; Head sample was first treated by a spiral separator to recover rough heavy mineral concentrates, which are contained minerals like ilmenite, zircon and rare earth minerals. Much higher beneficiation processes were subsequently taken by wilfley table and magnetic separation according to their magnetic field responses. Heavy minerals were effectively recovered by wilfley table and subsequent recleaning of heavy minerals by magnetic separations was conducted. Qualitative and relative-quantitative analyses of their constituent elements were doing using XRD and XRF.

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Selective leaching of valuable metals (Au, Ag etc.) from waste printed circuit boards (PCB)

  • Oh, Chi-Jung;Lee, Sung-Oh;Song, Jin-Kon;Kook, Nam-Pyo;Kim, Myong-Jun
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.193-197
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    • 2001
  • This study was carried out to recover gold, silver and other valuable metals from the printed circuit boards (PCB) of waste computers. PCB samples were crushed to under 1mm by a shredder and initially separated into 30% conducting and 70% non-conducting materials by an electrostatic separator. The conducting materials, which contained the valuable metals, were then used as the feed material for magnetic separation where it was found that 42% was magnetic and 58% non- magnetic. The non-magnetic materials contained 0.227mg/g Au and 0.697mg/g Ag. Further leaching of the non-magnetic component using 2.0M sulfuric acid and 0.2M hydrogen peroxide at 85$^{\circ}C$ extracted more than 95% copper, iron, zinc, nickel and aluminium. Au and Ag were not extracted in this solution, however, more than 95% of Au and 100% of Ag were selectively leached with a mixed solvent (0.2M ammonium thiosulfate, 0.02M copper sulfate, 0.4M ammonium hydroxide). Finally, the residues were reacted with a NaCl solution to leach out Pb while sulfuric acid was used to leach out Sn. Recoveries reached 95% and 98% in solution, respectively.

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