• Title/Summary/Keyword: low temperature firing

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Preparation and properties of BaO-ZnO-$B_2O_3-V_2O_5$ glass for PDP dielectric paste (PDP 유전체용 BaO-ZnO-$B_2O_3-V_2O_5$ 유리의 제조 및 특성 변화)

  • Son, Myung-Mo;Lee, Sang-Geun;Park, Hee-Chan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05c
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    • pp.295-298
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    • 2003
  • The principal problems in development of dielectric paste materials for PDP(plasma display panel)are PbO free paste and low melting temperature. We prepared PbO free paste from glasses in the system BaO-ZnO-$B_2O_3-V_2O_5$. DTA, XRD and SEM were used to study and characterize BaO-ZnO-$B_2O_3-V_2O_5$ glasses. PbO free paste developed at this paper has thermal expansion of $74{\times}10^{-7}/^{\circ}C$, DTA transformation point of $460^{\circ}C$, and firing condition of $560^{\circ}C$, 10min.

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Preparation and properties of PbO Free for PDP Rib Paste (PDP용 무연프리트 유리의 제조 및 특성)

  • Son, Myung-Mo;Lee, Heon-Soo;Lee, Chang-Hee;Lee, Sang-Geun;Park, Hee-Chan
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.524-525
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    • 2005
  • The principal problems in development of dielectric paste materials for PDP(plasma display panel)are PbO free paste and low melting temperature. We prepared PbO free paste from glasses in the system $ZnO-B_2O_3-Bi_2O_3-SiO_2$, DTA, and XRD were used to characterize $ZnO-B_2O_3-Bi_2O_3-SiO$ glasses. In this present study, PbO free paste had thermal expansion of $74\times10^{-7}/^{\circ}C$, DTA transformation point of $470^{\circ}C$, and firing condition of $540^{\circ}C$, 20min.

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Synthesis of Mesoporous Hollow Silica Sphere Using Water Glass: Filler for Weight Reduction of Rubber

  • Mun, Hanjun;Bae, Jae Young
    • Elastomers and Composites
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    • v.55 no.4
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    • pp.277-280
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    • 2020
  • In this study, mesoporous hollow silica spheres were synthesized using a polystyrene core and cetyltriammonium chloride (CTACl) as a pore template, and a low-cost water glass instead of expensive tetraethyl orthosilicate (TEOS) as a precursor. In addition, the material was synthesized by varying the concentration of polystyrene. Later, the polystyrene core and CTACl were removed by firing in a high-temperature heat-treatment process. The synthesized product was analyzed by various methods, such as scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffractometry (XRD), and N2-sorption analysis. It was confirmed that the hollow silica sphere had a hexagonal structure with a Brunauer-Emmett-Teller (BET) specific area of 1623 ㎡/g.

Resonance Mode Anlaysis in a Single Can-type Combustor through 3D Thermo-acoustic Analysis based on Helmholtz Solver (헬름홀츠 솔버 기반의 3차원 열음향해석을 통한 발전용 단일 캔 연소기에서의 공진 모드 분석)

  • Junwoo Jung;Daesik Kim
    • Journal of ILASS-Korea
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    • v.29 no.1
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    • pp.23-31
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    • 2024
  • This study conducted a 3D thermo-acoustic analysis based on the helmholtz solver to analyze the major resonance modes causing combustion instability in a single-can combustor. The experimental investigations were carried out on a test rig designed by the Korea Institute of Machinery & Materials (KIMM) under various conditions of hydrogen co-firing and fuel staging. Through these experiments, two primary unstable frequencies were identified. To determine the resonance modes of these frequencies, a 3D thermo-acoustic analysis was conducted using temperature information from the test rig. The results confirmed that the unstable frequencies observed in the experiments were all longitudinal modes. Additionally, the mode shapes identified in the analysis facilitated a simplification of the exit geometry for the low-order network model, confirming that this did not significantly affect the fundamental resonance modes.

TRANSFER ORBIT THERMAL ANALYSIS FOR COMS (통신해양기상위성의 전이궤도 열해석)

  • Jun, Hyoung-Yoll;Kim, Jung-Hoon;Kim, Sung-Hoon;Yang, Koon-Ho
    • Journal of computational fluids engineering
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    • v.13 no.2
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    • pp.48-54
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    • 2008
  • COMS (Communication, Ocean and Meteorological Satellite) is a geostationary satellite and has been developing by KARI for communication, ocean and meteorological observations. It will be launched by ARIANE 5. Ka-band components are installed on South panel, where single solar array wing is mounted. Radiators, embedded heat pipes, external heat pipe, insulation blankets and heaters are utilized for the thermal control of the satellite. The Ka-band payload section is divided several areas based on unit operating temperature in order to optimize radiator area and maximize heat rejection capability. Other equipment for sensors and bus are installed on North panel. The ocean and meteorological sensors are installed on optical benches on the top floor to decouple thermally from the satellite. During the transfer orbit operation, satellite will be under severe thermal environments due to low dissipation of components, satellite attitudes and LAE(Liquid Apogee Engine) firing. This paper presents temperature and heater power prediction and validation of thermal control design during transfer orbit operation.

Characterization of Embedded Thick Film Capacitor in LTCC Substrate (유전체 Paste를 이용한 LTCC 내장형 후막 Capacitor 제작 및 평가)

  • Cho, Hyun-Min;Yoo, Myung-Jae;Park, Sung-Dae;Lee, Woo-Sung;Kang, Nam-Kee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.760-763
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    • 2003
  • Low Temperature Cofired Ceramics (LTCC) technology is a promising technology to integrate many devices in a module by embedding passive components. For the module substrate, most LTCC structures have dielectric constants below 10 to reduce signal delay time. Some components, which need high dielectric constants, have not been yet embedded in LTCC module. So, embedding capacitor with high capacitance by applying another dielectrics with high dielectric constants in LTCC is an important issue to maximize circuit density in LTCC module. In this study, electrical properties of embedded capacitor fabricated by dielectric paste of high dielectric constants (K-100) and co-firing behavior with LTCC were investigated. To prevent camber development of co-fired structure, constrained sintering process was tested. Dielectric properties of embedded capacitors were calculated from their capacitance and impedance value. Temperature coefficient of capacitance were also measured.

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TRANSFER ORBIT THERMAL ANALYSIS FOR SATELLITE (위성의 전이궤도 열해석)

  • Jun, Hyoung-Yoll;Kim, Jung-Hoon;Kim, Sung-Hoon;Yang, Koon-Ho
    • 한국전산유체공학회:학술대회논문집
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    • 2007.10a
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    • pp.227-231
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    • 2007
  • COMS (Communication, Ocean and Meteorological Satellite) is a geostationary satellite and has been developing by KARI for communication and ocean and meteorological observations. It will be launched by ARIANE 5. Ka-band components are installed on South panel, where single solar array wing is mounted. Radiators, embedded heat pipes, external heat pipe, insulation blankets and heaters are utilized for the thermal control of the satellite. The Ka-band payload section is divided several areas based on unit operating temperature in order to optimize radiator area and maximize heat rejection capability. Other equipment for sensors and bus are installed on North panel. The ocean and meteorological sensors are installed on optical benches on the top floor to decouple thermally from the satellite. During the transfer orbit operation, satellite will be under severe thermal environments due to low dissipation of components, satellite attitudes and LAE(Liquid Apogee Engine) firing. This paper presents temperature and heater power prediction and validation of thermal control design during transfer orbit operation.

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Flexural performance of RC beams incorporating Zinc-rich and epoxy bonding coating layers exposed to fire

  • Tobbala, Dina E.;Rashed, Ahmed S.;Tayeh, Bassam A.
    • Structural Engineering and Mechanics
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    • v.82 no.2
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    • pp.163-172
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    • 2022
  • Zinc-rich epoxy (ZRE) is used to overcome corrosion problems in reinforced concrete (RC) beams and coat steel rebars to protect them from humidity and chlorides. An extra coating layer of Sikadur-31 epoxy (SDE) is utilised to increase bond strength because the use of ZRE reduces the bond strength between concrete and steel rebars. However, the low melting point of SDE indicates that concrete specimens are vulnerable to fire. An experimental investigation on flexural performance of RC beams incorporating ZRE-SDE coating of steel rebars that were destroyed by fire is performed in this study. Twenty beams of five concrete mixes with different cementitious contents were tested to compare fire exposure for coated and uncoated rebars of the same beams at room temperature and determine the optimal cementitious content. Scanning electron microscopy (SEM) was also applied to investigate characteristics of fired mixture samples. Results showed that the use of SDE-ZRE at room temperature improves flexural strengths of the five mixes compared with uncoated rebars with percentages ranging from 8.5% to 12.3%. All beams with SDE-ZRE lost approximately 50% of their flexural strength due to firing. Moreover, the mix incorporating SF (silica fume) of 15% and cement content of 400 kg/m3 introduces optimum behaviour compared with other mixes. All results were supported and verified by the SEM analysis and compressive strength of cubic specimens of the same mixes.

A Study on Changes in High-Temperature Microstructure of Coal Ash Applied as Cement Clinker Raw Material (시멘트 클링커 원료로서 적용한 석탄재의 고온 미세구조 변화 고찰)

  • Yoo, Dong-Woo;Im, Young-Jin;Kwon, Sung-Ku;Lee, Seok-Je
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.3
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    • pp.211-218
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    • 2022
  • Coal ash is being considered as a source of silica and alumina for cement clinker. The purpose of this study was to investigate the effect on cement clinker sintering by confirming the high-temperature microstructural change according to the firing temperature in the cement clinker sintering process of coal ash. In the coal ash used as a raw material for cement clinker, the shape change of the particle surface was confirmed from the sintering tem perature of 950 ℃. The shape of the coal ash disappeared from the sintering temperature higher than 1250 ℃. It was confirmed that the Al and Fe components of the coal ash were converted to the cement interstitial phase at a temperature higher than 1350 ℃. In addition, the clinker using a large amount of coal ash as a raw material showed a low content of Lime and a high content of Belite in the sintering tem perature range of 1150~1200 ℃. From this, it was confirmed that the formation of calcium silicate mineral proceeds more easily at the initial sintering temperature by the application of coal ash.

Degradation and Failure Analysis of Lead-free Silver Electrodes with Thermal Cycling (무연계 Ag 외부전극재의 열충격에 따른 열화특성과 고장해석)

  • Kim, Jung-Woo;Yoon, Dong-Chul;Lee, Hee-Soo;Jeon, Min-Seok;Song, Jun-Kwang
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.434-439
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    • 2008
  • Silver pastes as the outer electrodes have been prepared using Pb-free glass frits with different content of $Bi_2O_3$ and the effects of glass composition on the degradation behaviors of the Ag electrodes were investigated using the change of adhesion between Ag electrode and alumina substrate with thermal cycle stress. Low adhesion and high surface resistance were observed in Ag electrode using glass frit with a $Bi_2O_3$ content of 60 wt%, owing to the open microstructure formed at the firing temperature of $600^{\circ}C$. When the $Bi_2O_3$ was increased to 80 wt% in the glass frit, the Ag electrodes had a dense microstructure with high adhesion and a low surface resistance. Delamination of the Ag electrodes was a major failure mode under thermal cycle stress and this was attributed to residual stress due to the thermal expansion mismatch between the Ag electrode and the alumina substrate.