• Title/Summary/Keyword: large grains

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Precipitates Behavior and Microstructure of Friction Stir Welded 2519Al Alloy (마찰교반 용접한 2519Al 합금 용접부의 석출거동 및 미세조직)

  • Bae, Jong-Mo;Park, Tae-Won;Baik, Doo-Hyun;Kim, Hung-Ju;Chang, Woong-Seong
    • Proceedings of the KWS Conference
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    • 2006.10a
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    • pp.109-111
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    • 2006
  • In this study, microstructure and mechanical properties for the friction stir welded 2519Al-T87 alloy of the thickness of 38.8mm were studied using DSC, OM, SEM and micro hardness tester. DSC analysis show that GP Zone, ${\theta}'$ and $\theta$ phases in upper part and ${\theta}'$ and $\theta$ phase in lower part of the FSW zone. Recrystallized large grains are observed in HAZ, and elongated small and large grain in the TMAZ. In SZ, very small grains forms by high plastic deformation and heat from friction by tool and specimen.

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Formation of Ultrafine Grains in 5083 Al Alloy by Cryogenic Rolling Process (극저온 압연에 의한 초세립 5083 A1 Alloy 제조 연구)

  • 이영범;심혜정;남원종
    • Transactions of Materials Processing
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    • v.13 no.2
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    • pp.137-141
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    • 2004
  • The large deformation at cryogenic temperature is expected as one of the effective methods to produce large bulk ultrafine grained materials. The effects of annealing temperature, 150∼$300^{\circ}C$, on microstructures and mechanical properties of the sheets received 85% reduction at cryogenic temperature were investigated, in comparison with those at room temperature. Annealing of 5083 Al alloy deformed 85%, at $200^{\circ}C$ for an hour,. resulted in the considerable increase of tensile elongation without the great loss of strength and the occurrence of equiaxed grains less than 300nm in diameter.

Effect of Grain Specific Gravity on Seedling Growth and Vascular Bundle Development of Two Rice Cultivars (벼종자의 비중차이가 유묘생장 및 유관속 발달에 미치는 영향)

  • Chae, Je-Cheon;Lee, Dong-Jin
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.41 no.1
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    • pp.62-67
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    • 1996
  • High density (HD) grains is associated with seedling vigor. Studies were conducted on the relationship of different grain densities and vascular bundle(VB) development and seedling growth. IR58 (indica type) and Unbong 7 (japonica type) were used in this experiment. HD grains had more and bigger VB in the leaf blade and sheath than poor density grain at seedling stage. IR58 had more large VB at the leaf compared with Unbong 7. Higher development of VB in seedling of HD grains can increase transport of assimilate and growth rate. Plant height, leaf number, root growth and dry weight increased with increasing grain density from poor to high. The total area of large VB in the leaf blade and sheath was highly correlated with the dry weight. Higher number and larger area of VB and dry weight can be obtained by using HD grains and these initial advantages can contribute to high yield potential.

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Preparation of Self-reinforced Silicon Carbide Ceramics by Hot Pressing (가압소결에 의한 자체강화 탄화규소 세라믹스의 제조)

  • Park, Jong-Gon;Lee, Jong-Kook;Seo, Dong-Seok;Kim, Min-Jeong;Lee, Eun-Gu;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.36 no.12
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    • pp.1356-1363
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    • 1999
  • Self-reinforced silicon carbide was prepared by hot pressing and the control of starting phases of raw materials and its microstructural characteristics was investigated. The specimens with self-reinforced microstructure were obtained from the compacts with mixed compositions of ${\alpha}$-and ${\beta}$-SiC powders. Self-reinforced microstructure which is composed of large dispersed grains with rod-like shape and matrix with small equiaxed grains was formed by the transformation to the ${\alpha}$-SiC with 4H polytype for ${\beta}$-SiC and anisotropic grain growth during the heat treatment. Of all speimens the values of volume fraction maximum length and aspect ratio for large grains with rode-like types were the highest at the specimen with 50 vol% ${\beta}$-SiC in the starting SiC powder and therefore this specimen showed the highest fracture toughness due to the crack deflection by rod-like grains during crack propagation.

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Discovery of a New Mechanism to Release Complex Molecules from Icy Grain Mantles around Young Stellar Objects

  • Hoang, Thiem;Tram, Le Ngoc
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.1
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    • pp.70.4-70.4
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    • 2019
  • Complex organic molecules (COMs) are increasingly observed in the environs of young stellar objects (YSOs), including hot cores/corinos around high-mass/low-mass protostars and protoplanetary disks. It is widely believed that COMs are first formed in the ice mantle of dust grains and subsequently released to the gas by thermal sublimation at high temperatures (T>100 K) in strong stellar radiation fields. In this paper, we report a new mechanism that can desorb COMs from icy grain mantles at low temperatures (T<100K), which is termed rotational desorption. The rotational desorption process of COMs comprises two stages: (1) ice mantles on suprathermally rotating grains spun-up by radiative torques (RATs) are first disrupted into small fragments by centrifugal stress, and (2) COMs and water ice then evaporate rapidly from the tiny fragments (i.e., radius a <1nm) due to thermal spikes or enhanced thermal sublimation due to increased grain temperature for larger fragments (a>1 nm). We discuss the implications of rotational desorption for releasing COMs and water ice in the inner region of protostellar envelopes (hot cores and corinos), photodissociation regions, and protoplanetary disks (PPDs). In shocked regions of stellar outflows, we find that nanoparticles can be spun-up to suprathermal rotation due to supersonic drift of neutral gas, such that centrifugal force can be sufficient to directly eject some molecules from the grain surface, provided that nanoparticles are made of strong material. Finally, we find that large aggregates (a~ 1-100 micron) exposed to strong stellar radiations can be disrupted into individual icy grains via RAdiative Torque Disruption (RATD) mechanism, which is followed by rotational desorption of ice mantles and evaporation of COMs. In the RATD picture, we expect some correlation between the enhancement of COMs and the depletion of large dust grains in not very dense regions of YSOs.

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$Y_BaCuO_5$ Distribution within $YBa_2Cu_3O_{7-x}$ Grains of Melt Infiltration Processed YBCO Oxides (융융체 침투법으로 제조한 YBCO 산화물에서 $YBa_2Cu_3O_{7-x}$ 결정립 내 $Y_BaCuO_5$ 입자분포)

  • 김찬중;이동만;지영아;박해웅;홍계원
    • Journal of Powder Materials
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    • v.7 no.4
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    • pp.205-211
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    • 2000
  • Distribution of $Y_2BaCuO_5$ (211) Particles within $YBa_2Cu_3O_{7-x}/$ (123) grains of melt infiltration processed YBCO oxides was investigated. Processing parameters were a temperature, atmosphere (air and $O_2$) and initial 211 size. The 211 particles were distributed randomly within the 123 grains when the initial 211 size was large, while they made x-like pattern and/or butterfly-like patterns when the 211 size was small. The 211 patterns were more clearly observed in the samples prepared at higher temperatures and under $O_2$ atmosphere. The 211 distribution was explained in terms of the interfacial energy relationship among the solid, particle and melt.

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X-X: Single-Crystalline Si TFTs Fabricated with ${\mu}-Czochralski$ (grain-filter) process

  • Ishihara, R.;Dijk, B.D.van;Wilt, P.Ch. van der;Metselaar, J.W.;Beenakker, C.I.M.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.159-162
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    • 2002
  • This paper reviews an advanced excimer-laser crystallization technique enabling precise location-control of the individual grains. With the developed ${\mu}$-Czochralski (grain-filter) process, the large grains having a diameter of 6 ${\mu}m$ can be set precisely at predetermined positions. We will also discuss the performance of the single-crystalline Si TFTs that are formed within the location-controlled Si grains. The field-effect mobility for electrons is 430 $cm^2/Vs$ on average, which is well comparable to that of TFTs made with silicon-on-insulator wafers.

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Effect of SiC Particle Size on the Microstructure and Mechanical Properties Of Al2O3-SiC Composite (Al2O3-SiC 복합재료의 미세조직 및 기계적 물성에 미치는 SiC 원료분말의 크기 영향)

  • 채기웅
    • Journal of the Korean Ceramic Society
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    • v.41 no.2
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    • pp.125-130
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    • 2004
  • The effect of SiC particle size on the microstructures and mechanical properties of A1$_2$O$_3$-SiC composite was investigated. Two types of SiC powders having average particle sizes of 0.15 ${\mu}{\textrm}{m}$ and 3 ${\mu}{\textrm}{m}$ were used. The grain growth in the specimen containing 0.15 ${\mu}{\textrm}{m}$ SiC was effectively inhibited due to the fine SiC particles. However, after the formation of some abnormal grains, fast and exaggerated grain growth occurred which led to the microstructure of large grains with irregular shape. Fracture strength decreased due to the abnormal large grains. On the other hand, for specimen containing 3 ${\mu}{\textrm}{m}$ SiC showed normal grain growth behavior from initial sintering stage. Large SiC particles, however, effectively inhibited exaggerated grain growth after nucleation of a few abnormal grains. As a consequence, microstructure consisted of homogeneous elongated grains. In the A1$_2$O$_3$-2.5SiC(0.15 ${\mu}{\textrm}{m}$)-2.5SIC(3 ${\mu}{\textrm}{m}$) composite fabricated by mixing the two types of SiC powder, abnormal grain growth occurred. However, the good fracture strength was maintained regardless of microstructural changes in this specimen.

Effects of Heat Treatment on the Microstructure and Whisker Growth Propensity of Matte Tin Finish

  • Kim, K.S.
    • Journal of the Microelectronics and Packaging Society
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    • v.17 no.2
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    • pp.11-20
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    • 2010
  • The effects of heat treatment on matte pure tin-plated Cu leadframes at high temperature and humidity conditions were investigated. After 1800 hrs of storage at $55^{\circ}C/85%$ RH, approximately 14.5 ${\mu}m$ long striation-shaped whiskers were observed on the surface of the without postbake treatment (WOPB) samples, while no whiskers were found in with postbake treatment (WPB) samples. The preferred orientations of Sn grains in WOPB and WPB sample did not change after the postbake treatment at $125^{\circ}C$ for 1 hr. However, both changed from (112) to (321) and (101), respectively, after 1800 hrs of storage at $55^{\circ}C/85%$ RH. The tensile stress of 8 MPa generated in as-plated sample was changed to a compression stress of 17 MPa after 2 days in room temperature storage. Due to the grain growth during postbake treatment, the WPB samples have more regular grains than the WOPB samples. In the as-plated sample, 0.32 ${\mu}m$ thickness of planar intermetallic compound (IMC) was observed. The IMCs in the WOPB and WPB samples had two distinct layers with large grains of $Cu_6Sn_5$ and with small grains of ${\eta}-Cu_{6.26}Sn_5$.

Abnormal grain growth of ZnO ceramics (ZnO 세라믹스 거대입성장)

  • Kim, Young Jung
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.29 no.6
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    • pp.251-256
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    • 2019
  • In the process of ZnO ceramic sintering at a temperature of 1385℃, higher than the normal sintering temperature, some grains were growth up to mm scale. When sintered at 1400℃ for 8 hours, the size of the grains that are not involved in the abnormal growth is as large as 30~40 ㎛, but the size of the abnormal grown grain reaches 1,000 ㎛, which is more than 10,000 times bigger in volume than the normal one within 8 hr growth. As a cause of rapid and abnormal grain growth, primary particle size distribution, compaction density variation within sample and doping of impurities could be considered. The primary particle size distribution could be considered main reason for abnormal grain growth but no solid evidence was obtained. Through the observation of the microstructure, it is presumed that the giant grains grow absorbing the neighbor grains through a grain rotation process.