• 제목/요약/키워드: interfacial analysis

검색결과 634건 처리시간 0.026초

마이크로 유체 원심분리기의 챔버 크기에 따른 회전 유동 가시화 (Visualization of Rotational Flow for Chamber Size of a 2×2 Microfluidic Centrifuge)

  • 전형진;권봉현;김대일;고정상
    • 한국가시화정보학회지
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    • 제10권3호
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    • pp.25-29
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    • 2012
  • This paper introduces a new parameter to design the $2{\times}2$ microfluidic centrifuge with single flow rotation positioned at the center of microchamber. The dimensional centrifugal acceleration momentum flux which is defined as the interfacial momentum flux divided by distance from the center of the chamber explains the flow rotation and its threshold provides a reference to expect single flow rotation. Through the numerical and experimental visualization of the flow rotation, the number and position of flow rotation in the $2{\times}2$ microfluidic centrifuge were examined. At a channel width of $50{\mu}m$ and chamber width of $250{\mu}m$, single flow rotation was obtained over at a Reynolds number of 300, while at a channel width of $100{\mu}m$ and chamber width of $500{\mu}m$, single flow rotation did not appear. The numerical analysis showed that the threshold centrifugal acceleration momentum flux to obtain single flow rotation was $3500kg/m{\cdot}s^2$.

보스-리브 시험 시 마찰보정선도에 대한 펀치형상 및 유동응력의 영향 (Effect of Punch Design and Flow Stress on Frictional Calibration Curve in Boss and Rib Test)

  • 윤여웅;강성훈;이영선;김병민
    • 소성∙가공
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    • 제18권8호
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    • pp.640-645
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    • 2009
  • Recently, boss and rib test based on backward extrusion process was proposed to quantitatively evaluate the interfacial friction condition in bulk forming process. In this test, the tube-shaped punch with hole pressurizes the workpiece so that the boss and rib are formed along the hole and outer surface of the punch. It was experimentally and numerically revealed that the height of boss is higher than that of the rib under the severe friction condition. This work is focused on the effect of the punch design and flow stress on deformation pattern in boss and rib test. From the boss and rib test simulations, it was found that there is slight variation in both the heights of boss and rib according to the length of punch land, nose radius, and face angle. However the hole diameter of the punch and the clearance between the punch and die have a significant influence on the calibration curves showing the heights of the boss and rib. In addition, the effect of flow stress on the calibration curves was investigated through FE simulations. It was found that there is no effect of strength coefficient of the workpiece on the calibration curves for estimation of friction condition. On the other hand, the strain-hardening exponent of the workpiece has a significant influence on the calibration curve.

Zeta 전위에 의한 도핑되지 않은 다결정 Si 및 GaAs 반도체 계면의 표면준위에 관한 정성적 해석 (A Qualitative Analysis on the Surface States at the Undoped Polycrystalline Si and GaAs Semiconductor Interfaces Using the Zeta Potential)

  • Chun, Jang-Ho
    • 대한전자공학회논문지
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    • 제24권4호
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    • pp.640-645
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    • 1987
  • Surface states and interfacial phenomena at the undoped polycrystalline semiconductor particale-electrolyte interfaces were qualitatively analyzed based on the zeta potentials which were measured with microelectrophoresis measurements. The suspensions were composed of the undoped polycrystaline silicon(Si) or gallium arsenide (GaAs) semiconductor particles stalline Si and GaAs particles in the KCl electrolytes was 3.73~6.2x10**-4 cm\ulcornerV.sec and -2.3~1.4x10**-4cm\ulcornerV.sec at the same conditions, respectively. The range of zeta potentials corresponding to the electrophoretic mobilities is 47.8~80.1mV and -30.1~17.9mV, respectively. The variation of the zeta potentials of the undoped polycrystalline Si was similar to the doped crystalline Si. On the other hand, two points of zeta potential reversal occurred at the undoped polycrystalline GaAs-KCl electrolyte interfaces. The surface states of the undoped polycrystalline Si and GaAs were dominated by positively charged donor surface states. These surface states are attributed to adsorbed ion surface states (slow states) at the semiconductor oxide layer-electrolyte interfaces.

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재생시멘트의 품질향상을 위한 제조방법에 관한 연구 (An Experimental Study of the Recycled Cement Manufacturing Method for Improving the Material Quality)

  • 오상균
    • 한국건축시공학회지
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    • 제4권2호
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    • pp.143-149
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    • 2004
  • The recycle of domestic waste concrete is, however, still in an early stage, and it has been only partially being used for the road fillers. As a counter-plan of activating recycled concrete, we have confirmed the hydration possibility of the waste concrete powder from the experiment on recycling the aggregate powder since 2000. Though that study, we have known that the strength is increasing when the baking time is longer, and baking temperature maintain in $700^{\circ}C$. Also, the quality is lowered because of the fine aggregate powder which has a bad influence on flowability & compression strength by adhesion of mortar on the aggregate face. Therefore, mortar and interfacial separation of aggregate are large in proper quality for concrete recycling is expected that affect. The purpose of this study is to investigate effective aggregate separation and to determine the most suitable production method controlling the duration of baking time for recycled cement from the compressive strength, X-ray diffraction and ingredient analysis test.

복합재료 접착체를 가지는 튜브형 접합부의 토크전달능력 예측 (Prediction of the Torque Capacity for Tubular Adhesive Joints with Composite Adherends)

  • 오제훈
    • 대한기계학회논문집A
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    • 제30권12호
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    • pp.1543-1550
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    • 2006
  • Since the performance of joints usually determines the structural efficiency of composite structures, an extensive knowledge of the behavior of adhesive joints and the related effect on joint strength is essential for design purposes. In this study, the torque capacity of adhesive joints was predicted using the combined thermal and mechanical analyses when the adherend was a composite tube. A finite element analysis was performed to evaluate residual thermal stresses developed in the joint, and mechanical s stresses in the adhesive were calculated including both the nonlinear adhesive behavior and the behavior of composite tubes. Three different joint failure modes were considered to predict joint failure: interfacial failure, adhesive bulk failure, and adherend failure. The influence of the composite adherend stacking angle on the residual thermal stresses was investigated, and how the residual thermal stresses affect the joint strength was also discussed. Finally, the predicted results were compared with experimental results available in literature.

고속 화염 용사를 통하여 형성된 다중벽 탄소 나노튜브 알루미늄 복합소재 코팅의 특성 평가 (Property Evaluation of HVOF Sprayed Multi-walled Carbon Nanotube Aluminum Composite Coatings)

  • 강기철;박형권;이창희
    • 한국표면공학회지
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    • 제45권1호
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    • pp.1-7
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    • 2012
  • Multi-walled carbon nanotube (MWCNT) aluminum composite powders were deposited to form coatings using a high velocity oxygen fuel (HVOF) spraying process. High thermal energy and contact with atmospheric oxygen were supplied as the MWCNT aluminum composite particles were exposed to a gas flow field at high temperature (${\sim}3.0{\times}10^3$ K) during HVOF spraying. As a result, the particles underwent full or partial melting and rapid solidification due to the high thermal energy, and the exposure to oxygen induced the interfacial reaction of MWCNTs within the particle. The electrical and mechanical properties of MWCNT aluminum composite coatings were evaluated based on microstructure analysis. Electrical resistivity, elastic modulus, and micro-hardness, of the MWCNT aluminum composite coatings were higher than those of pure aluminum coating. The contribution of MWCNTs to the aluminum matrix can be attributed to their high electrical conductivity, dispersion hardening and anchoring effects. The relationship among the properties and the interaction of the MWCNTs with the aluminum matrix is discussed.

분무성형법에 의해 제조된 $Al-SiC)_p$ 금속기 복합재료의 미세조직과 성질에 관한 연구 (A Study on the Microstructures and Properties of $Al-SiC)_p$ Metal Matrix Composites Fabricated by Spray Forming Process)

  • 김춘근
    • 한국분말재료학회지
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    • 제1권1호
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    • pp.42-51
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    • 1994
  • 6061Al-SiCP metal matrix composite materials(MMCs) were fabricated by injecting SiCP particles directly into the atomized spray. The main attraction of this technique is the rapid fabrication of semi-finished, composite products in a combined atomization, particulate injection(10 $\mu\textrm{m}$, 40 $\mu\textrm{m}$, SiCP) and deposition operation. Conclusions obtained are as follows; The microstructure of the unreinforced spray formed 6061Al alloy consisted of relatively fine(50 $\mu\textrm{m}$) equiaxed grains. By comparision, the microstructure of the I/M materials was segregated and consisted of relatively coarse(150 $\mu\textrm{m}$) grains. The probability of clustering of SiCP particles in co-sprayed metal matrix composites increased it ceramic particle size(SiCP) was reduced and the volume fraction was held constant. Analysis of overspray powders collected from the spray atomization and deposition experiments indicated that morphology of powders were nearly spherical and degree of powders sphercity was deviated due to composite with SiCp particles. Interfacial bonding between matrix and ceramics was improved by heat treatment and addition of alloying elements(Mg). Maximum hardness values [Hv: 165 kg/mm2 for Al-10 $\mu\textrm{m}$ SiCp Hv--159 kg/mm2 for Al-40 $\mu\textrm{m}$SiCp] were obtained through the solution heat treatment at $530^{\circ}C$ for 2 hrs and aging at $178^{\circ}C$, and there by the resistance were improved.

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유변학적 성질 측정으로 측정한 고분자 계면에서의 반응 kinetics와 morphology 변화 (Reaction Kinetics and Morphological Changes at Polymer-polymer Interface measured by Rheological Properties)

  • Kim, Hwang-Yong;Unyong Jeong;Kim, Jin-Kon
    • 한국유변학회:학술대회논문집
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    • 한국유변학회 2002년도 춘계 학술발표회 논문집
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    • pp.25-27
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    • 2002
  • In this study we investigated the reaction kinetics by a convenient but useful method-rheology to characterize the interface between two immiscible blends with a Reactive compatibilizer. Also, we made an attempt to correlate changes of interface roughness with rheological properties. The blend systems employed in this study was mono-carboxylated polystyrene (PS-mCOOH) and an poly(methyl methacrylate-ran-glycidylmethacrylate) (PMMA-GMA). PS-mCOOH was synthesized by an anionic polymerization and PMMA-GMA by a free radical polymerization. We prepared two plates of each polymer using compression molding with a smooth surface molder, then put one upon another. As soon as these two plates welds together inside a rheometer under nitrogen environment, the torque and moduli were obtained with reaction time at different temperatures. Through the analysis of this modulus change with reaction time, we estimated interfacial reaction and roughening. The increment of modulus in initial state can be correlated to the extent of reaction. We obtained the reaction kinetic constant by fitting appropriate kinetic equation into experimental data. We also showed that increment of modulus in later state was due to by roughened interface.

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코발트 산화물 전극의 수퍼커페시터 성질에 미치는 니켈 폼 집전체 효과 (Effect of Nickel Foam Current Collector on the Supercapacitive Properties of Cobalt Oxide Electrode)

  • 윤여일;김광만;고장면
    • 한국세라믹학회지
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    • 제45권6호
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    • pp.368-373
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    • 2008
  • An electrode for supercapacitor using 3-dimensional porous nickel foam as a current collector and cobalt oxide as an active material was prepared and characterized in terms of morphology observation, crystalline property analysis, and the investigation of electrochemical property. The electrode surface showed that the cobalt oxide was homogeneously coated as the crystalline phase of $Co_3O_4$. Cyclic voltammetry for the $Co_3O_4$/nickel foam electrode exhibited higher specific capacitance values (445 F/g at 10 mV/s and 350 F/g at 200 mV/s) and excellent capacitance retention ratio (99% after $10^4$ cycles). It was proved that the nickel foam substrate played the roles in reducing the interfacial resistance with cobalt oxide and in improving the electrode density by embedding greater amount of cobalt oxide within it.

$(Sr_{0.85}-Ca_{0.15})$$TiO_3$ 입계층 세라믹의 열자력전류 특성에 관한 연구 (A study on the properties of thermally stimulated current of $(Sr_{0.85}-Ca_{0.15})$$TiO_3$ grain boundary layer ceramic)

  • 김진사;김성열;유영각;최운식;이준웅
    • E2M - 전기 전자와 첨단 소재
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    • 제9권4호
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    • pp.396-403
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    • 1996
  • In this paper, the (S $r_{0.85}$.C $a_{0.15}$)Ti $O_{3}$ of paraelectric grain boundary layer (GBL) ceramics were fabricated, and the analysis of microstructuye and the thermally stimulated current(TSC) were investigated for understanding effects of GBL's interfacial phenomenon on variations of electrical properties. As a result, the three peaks of .alpha., .alpha. and .betha. were obtained at the temperature of -20 [.deg. C], 20[.deg. C] and 80[.deg. C], respectively. The origins of these peaks are that the .alpha. peak observed at -20[.deg. C] looks like to be ascribed to the ionization excitation from donor level in the grain, and the .alpha.' peak observed at 20[.deg. C] appears to show up by detrap of the trapped carrier of border between the oxidation layer and the grain, and the .betha. peak observed at 80[.deg. C] seems to be resulted from hopping conduction of existing carrier in the trap site of the border between the oxidation and second phase. and second phase.

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