• 레미콘
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• 10호통권69호
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• pp.2-11
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• 2001

This paper describes the feasiblity of recycling sewage dredged soils as fine affrefate. This paper describes the feasibility of recycling sewage dredged soils as fine aggregate. The specific gravity of the dredged soils was smaller than that of sand due to the effect of dredged sludge. However, the grain size distribution of the dredged soils is relative well graded, and the results of the heavy metal concentration from the leaching test of the dredged soils was significantly lower than the requirements of the allowable criteria. Therefore, the effect of recycling of dredged soils on environment the as fine aggregate was negligible. Also, the specific gravity of the dredged and washed soils was similar to that of sand, and the dredged and washed soils for the most part showed lower heavy metal leaching characteristics than those of dredged soils, Also, the results of the study for evaluation the recycling feasibility of dredged and washed soils as fine affrefate. The organic impurity content of the dredged and washed soils was lower than the requirements of the Korean industrial Standards, and the mortar compressive strength using the washdredged soils also met those of the Korean industrial Standards. And, the strengths of the dredged and washed soils were over 95% of those of the NaOH-treated samples. Therefore, it is expected that the dredged soils will be able to be an alternative for fine aggregate.

• 한국수소및신에너지학회논문집
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• 제22권2호
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• pp.257-264
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• 2011

This study discribes performance of DEFC (Direct Ethanol Fuel Cell) utilized bio-ethanol based on fruit wastes. To produce the bio-ethanol, fruit wastes were treated at temperature $120^{\circ}C$ and 90minutes in acid pre-treatment. After pre-treatment was done, alcohol fermentation process was running. Initial alcohol concentration was 5%. Using the multi coloumn distillation system, more than 95% ethanol was distilled and each component of bio-ethanol was analyzed. In DEFC performance test, it was revealed that cell performance was much higher than that of ethanol. Comparing ethanol with mixed fuel (bio-ethanol (10%) + ethanol (90%)), the performance of ethanol was higher than that of mixed fuel. Even though the bio-ethanol from the fruit wastes is corresponded with transport ethanol standards, it thought that organic matter in bio-ethanol could be negative effect on fuel cell.

• Korean Chemical Engineering Research
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• 제52권3호
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• pp.340-346
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• 2014

Continuous and dense ZIF-7 membranes were successfully synthesized on ${\alpha}-Al_2O_3$ porous substrate via two-step crystallization technique. ZIF-7 seeding layer was first deposited on porous ${\alpha}-Al_2O_3$ substrate by in-situ low temperature crystallization, and then ZIF-7 membrane layer can be grown through the secondary high-temperature crystallization. Two synthesis solutions with different concentration were used to prepare ZIF-7 seeding layer and membrane layer on porous ${\alpha}-Al_2O_3$ substrate, respectively. As a result, a continuous and defect-free ZIF-7 membrane layer can be prepared on porous ${\alpha}-Al_2O_3$ substrate, as confirmed by scanning electron microscope. XRD characterization shows that the resulting membrane layer is composed of pure ZIF-7 phase without any impurity. A single gas permeation test of $H_2$, $O_2$, $CH_4$ or $CO_2$ was conducted based on our prepared ZIF-7 membrane. The ZIF-7 membrane exhibited excellent H2 molecular sieving properties due to its suitable pore aperture and defect-free membrane layer.

• 대한금속재료학회지
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• 제49권1호
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• pp.73-78
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• 2011

Weldability, especially HAZ cold cracking, weld metal solidification cracking, and HAZ liquation cracking susceptibilities, of ASTM A356 CA6NM martensitic stainless steel casting was investigated and compared with that of 9-12% Cr ferritic steel castings. Irrespective of the Cr and Ni content in the castings, the HAZ maximum hardness increased with an increase of carbon content. CA6NM steel, which has the lowest carbon content, had the lowest HAZ hardness and showed no cold cracking in y-slit cracking tests. CA6NM steel, meanwhile, showed the largest weld metal solidification cracking susceptibility in varestraint tests because of its higher amount of impurity elements, phosphorus, and sulfur. All castings investigated had good high temperature ductility in hot ductility tests and showed little difference in liquation cracking susceptibility.

• 한국산학기술학회논문지
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• 제13권6호
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• pp.2458-2464
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• 2012

최근 디스플레이용 부품소재는 국가 산업 경쟁력을 강화시킬 수 있는 고부가가치 산업분야로 발전하고 있다. 하지만 디스플레이용 부품소재 생산을 위한 시스템은 대부분 수입에 의존하며 개발이 미비한 상태이다. 그러므로 디스플레이용 부품소재인 스페이서 테이프 생산을 위한 엠보싱 처리 시스템의 국산화 및 생산성 증대를 위한 시스템 향상이 시급한 실정이다. 따라서 본 논문에서는 엠보싱처리 시스템의 국산화 및 생산성 증대를 위한 스페이서 테이프 생산을 위한 회전형 엠보싱 처리 시스템을 제안한다. 시스템은 권출부, 성형부, 권치부, 세정부, 검사부로 구성된다. 이 중, 성형부의 금형을 회전형 방식으로 설계하였고, 각 구성품들을 설계하고 시제작품을 제작하여 성능 실험을 하였다. 성능 실험은 삼차원 측정기를 통해 엠보싱 형상, 직경, 엠보싱 간격 및 반대편 엠보싱과의 거리를 측정하였다. 오염물 검출 실험을 하기 위해, 검사부를 통해 첫 번째 샘플과 반복 생산한 후의 샘플에 대해 이물질 레벨을 측정하였다. 그리고 샘플에 이물질을 부착한 후 세정부를 통해 샘플을 세정한 후의 이물질 개수를 측정하여 오염물 세정 실험을 하였다. 또한, 시제작품에 의해 생산되는 스페이서 테이프의 생산성을 측정하였다.

• 전기화학회지
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• 제11권1호
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• pp.42-46
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• 2008

연료전지는 수소를 직접 사용하는 것이 가장 효율이 높지만 가정이나 사무실에서는 수소 저장탱크를 사용하기보다는 도시가스(메탄가스)를 연료 source로 하여 수소를 생산하는 것이 유리하다. 연료전지에 사용하는 수소는 천연가스나 바이오가스, 탄화수소계열의 연료를 개질하여 생산하며 개질반응과정에서 필연적으로 여러 성분의 불순물이 포함되어 있다. CO, $CO_2$, $H_2S$, $NH_3$, $CH_4$등의 불순물이 포함된 수소연료가 PEM fuel cell에 공급되면 연료전지 성능에 영향을 준다고 보고되어 있다. 이러한 영향에는 전극 촉매의 피독에 의한 kinetic losses, 전해질막과 촉매이온층의 양이온 전도성 감소에 의한 ohmic losses 그리고 촉매층의 구조나 소수성 감소에 의한 mass transport losses가 있다. 개질기에서 생산된 수소연료는 약 73%의 $H_2$와 20% 이하의 $CO_2$, 5.8% 이하의 $N_2$, 2% 이하의 $CH_4$, 10ppm 이하의 CO로 최종 공급된다. 본 연구에서는 연료 중에 $CO_2$가 고분자전해질 연료전지 anode측 성능에 미치는 영향을 조사하였다. 실험은 연료전지에 공급되는 연료중에 $CO_2$농도를 10%, 20%, 30%로 전류와 전압의 성능곡선과 장시간(10시간)실험 그리고 임피던스를 측정하였다. 또한 가스크로마토그래피를 이용하여 순수한 수소와 $CO_2$가 함유된 수소의 혼합을 통해 나온 연료전지 inlet에서의 불순물의 농도를 검증하였다.

• 융합정보논문지
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• 제11권10호
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• pp.131-137
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• 2021

본 연구에서 진단, 과민반응 검사에 사용되며 의약품에 불순물로 포함되어 규제되는 histamine의 단독 및 병용 투여에서 조직/근육 선택적 장관 수축성 조절에 대한 실험을 하고자 하였다. Histamine은 muscarinic receptor 작용 외에 histamine H1 receptor에 대한 직접 작용으로 수축성을 증가시켰고 회장/결장 윤주근에서 수축성을 거의 증가시키지 않았다. 또한 M3 수용체에 선택적으로 작용하는 atropine의 병용 효과를 관찰하였는데 histamine과 병용된 atropine은 장관 중 회장의 종주근의 수축성을 거의 감소시키지 않았고 회장/결장의 윤주근의 수축성을 감소시키지 않았다. 따라서 적어도 회장의 종주근에서 histamine은 M3 수용체를 거의 경유하지 않고 작용하고 atropine은 항무스카린 효과 외에 histamine에 의한 조직 선택적 위장관 운동성을 거의 조절하지 않는 것으로 생각된다. 그리고 이러한 단순한 검색은 의약품 불순물 검사로 선호될 것으로 생각된다.

• 한국재료학회지
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• 제28권12호
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• pp.738-747
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• 2018

For the aerospace structural application of high-strength 2xxx series aluminum alloys, stress corrosion cracking(SCC) behavior in aggressive environments needs to be well understood. In this study, the SCC sensitivities of 2024-T62, 2124-T851 and 2050-T84 alloys in a 3.5 % NaCl solution are measured using a constant load testing method without polarization and a slow strain rate test(SSRT) method at a strain rate of 10-6 /sec under a cathodic applied potential. When the specimens are exposed to a 3.5 % NaCl solution under a constant load for 10 days, the decrease in tensile ductility is negligible for 2124-T851 and 2050-T84 specimens, proving that T8 heat treatment is beneficial in improving the SCC resistance of 2xxx series aluminum alloys. The specimens are also susceptible to SCC in a hydrogen-generating environment at a slow strain rate of $10^{-6}/sec$ in a 3.5 % NaCl solution under a cathodic applied potential. Regardless of the test method, low impurity 2124-T851 and high Cu/Mg ratio 2050-T84 alloys are found to have relatively lower SCC sensitivity than 2024-T62. The SCC behavior of 2xxx series aluminum alloys in the 3.5 % NaCl solution is discussed based on fractographic and micrographic observations.

• Journal of Pharmaceutical Investigation
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• 제38권3호
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• pp.157-162
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• 2008

The aim of the study was to formulate the stable amlodipine maleate tablet by selecting and combining of suitable ingredients. Amlodipine tablets were designed by using different manufacturing methods or formulations. Dissolution rate at 30 min of newly formulated tablets was over 98% in 0.1 M HCl medium. After 4 months storage under accelerated condition, the changes of appearance, loss on drying, content and total impurity were investigated. For long-term stability tests, two formulations of K017 (direct compressed tablets consisting of microcrystalline cellulose and pregelatinized starch) and K018 (wet granulated tablets by OpadryAMB) were stored under $25^{\circ}C$, 60% RH for 24 months. Under the accelerated condition, moisture content in K017 formulation was increased as 5.96% for 4 months, while other formulations with anhydrous monobasic phosphoric potassium or by wet granulation showed higher increase in moisture content compared to K017. In addition, K017 formulation showed a low decrease in contents and total relative substance as 0.8% and 0.7%, respectively. Similar stability of amlodipine in K017 was obtained under the long-term stability test. These results indicate that the K017 combined with microcrystalline cellulose and pregelatinized starch as ingredients is very stable formulation to protect active substance from moisture contact and sustain stability. Therefore, suitable combination of ingredients such as microcrystalline cellulose and pregelatinized starch could attribute to enhance the stability of moisture-labile drug such as amlodipine maleate.

• 한국반도체및디스플레이장비학회:학술대회논문집
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• 한국반도체및디스플레이장비학회 2007년도 춘계학술대회
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• pp.193-198
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• 2007

The NiSi is very promising candidate for the metallization in 60nm CMOS process such as FUSI(fully silicided) gate and source/drain contact because it exhibits non-size dependent resistance, low silicon consumption and mid-gap workfunction. Ni film was first deposited by using ALD (atomic layer deposition) technique with Bis-Ni precursor and $H_2$ reactant gas at $220^{\circ}C$ with deposition rate of $1.25{\AA}/cycle$. The as-deposited Ni film exhibited a sheet resistance of $5{\Omega}/{\square}$. RTP (repaid thermal process) was then performed by varying temperature from $400^{\circ}C$ to $900^{\circ}C$ in $N_2$ ambient for the formation of NiSi. The process window temperature for the formation of low-resistance NiSi was estimated from $600^{\circ}C$ to $800^{\circ}C$ and from $700^{\circ}C$ to $800^{\circ}C$ with and without Ti capping layer. The respective sheet resistance of the films was changed to $2.5{\Omega}/{\square}$ and $3{\Omega}/{\square}$ after silicidation. This is because Ti capping layer increases reaction between Ni and Si and suppresses the oxidation and impurity incorporation into Ni film during silicidation process. The NiSi films were treated by additional thermal stress in a resistively heated furnace for test of thermal stability, showing that the film heat-treated at $800^{\circ}C$ was more stable than that at $700^{\circ}C$ due to better crystallinity.