• Title/Summary/Keyword: hot-pressing temperature

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Thermoelectric Properties of the Hot-pressed n-Type $Bi_2({Te_{0.85}}{Se_{0.15}})_3$ Alloy Prepared by Mechanical Alloying (기계적 합금화 공정을 이용하여 제조한 n형 $Bi_2({Te_{0.85}}{Se_{0.15}})_3$ 가압소결체의 열전특성)

  • Kim, Hui-Jeong;O, Tae-Seong;Hyeon, Do-Bin
    • Korean Journal of Materials Research
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    • v.10 no.3
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    • pp.246-252
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    • 2000
  • Thermoelectric properties of the $Bi_2(Te_{0.85}Se_{0.15})_3$ alloy, prepared by mechanical alloying and hot pressing, were investigated with the variation of the hot-pressing temperature ranging from $300^{\circ}C$ to $550^{\circ}C$. Contrary to the p-type behavior of single crystal, the hot-pressed $Bi_2(Te_{0.85}Se_{0.15})_3$ alloy exhibited n-type conduction without addition of donor dopant. When the $Bi_2(Te_{0.85}Se_{0.15})_3$ powders were annealed in $(50{\%}\;H_2+50{\%}\;Ar)$ atmosphere, the hot-pressed specimens exhibited a positive Seebeck coefficient due to the reduction of the electron concentration by removal of the oxide layer on the powder surface and annealing-out of the excess Te vacancies. Figure-of-merit of the hot-pressed $Bi_2(Te_{0.85}Se_{0.15})_3$ alloy was improved by hot pressing at temperatures above $450^{\circ}C$, and the maximum value of $1.92{\times}10^{-3}/K$ was obtained for the specimen hot-pressed at $550^{\circ}C$.

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Microstructure and Elevated Temperature Strength of W-ZrC Composites with Micrometric and Nanosized ZrC Particles (서로 다른 입자크기의 ZrC가 첨가된 W-ZrC 복합체의 미세구조 및 고온강도에 관한 연구)

  • Han, Yoon Soo;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.21 no.6
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    • pp.415-421
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    • 2014
  • W-10vol.%ZrC composites reinforced by micrometric and nanosized ZrC particles were prepared by hot-pressing of 25 MPa for 2 h at $1900^{\circ}C$. The effect of ZrC particle size on microstructure and mechanical properties at room temperature and elevated temperatures was investigated by X-ray diffraction analysis, scanning electron microscope and transmission electron microscope observations and the flexural strength test of the W-ZrC composite. Microstructural analysis of the W-ZrC composite revealed that nanosized ZrC particles were homogeneously dispersed in the W matrix inhibiting W grain growth compared to W specimen with micrometric ZrC particle. As a result, its flexural strength was significantly improved. The flexural strength at room temperature for W-ZrC composite using nanosized ZrC particle being 740 MPa increased by around 2 times than that of specimen using micrometric ZrC particle which was 377 MPa. The maximum strength of 935 MPa was tested at $1200^{\circ}C$ on the W composite specimen containing nanosized ZrC particle.

Effects of Hot Isostatic Pressing on the Microstructure and High-Temperature Fatigue Life of the Ni-base Superalloy IN738LC (IN738LC 초내열합금에서 미세조직과 고온 피로수명에 미치는 고온등압압축(HIP) 공정의 영향)

  • Choi, Cheol;Kim, Doo-Soo;Lee, Young-Chan;Park, Young-Kyu;Kim, Gil-Moo;Kim, Jae-Cheol
    • Korean Journal of Materials Research
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    • v.10 no.2
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    • pp.128-137
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    • 2000
  • A study has been made to investigate the effects of hot isostatic pressing(HIPing) on the microstructure and high temperature fatigue lives of the IN738LC, Ni-base superalloy used in turbine blades, with emphasis on the elimination of casting microporosity and fatigue damage through HIP treatments. Microstructure was observed using OM, SEM and the fatigue life was investigated with rotate bending fatigue tester. The results show that the fatigue lives of properly HIP-processed specimens could be extended be extended by a factor of about sixty. In contrast, no comparable life improvement was achieved with heat treatment only. The repetitive HIP treatment was shown to be very effective as a means of rejuvenating the fatigue life of intentionally fatigue-damaged IN738LC by restoration of the initial alloy microstructure and additional removal of fine casting defects which remained in the HIP-processed material.

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Wear Properties of the Alumina Short Fiber Reinforced Tin-Bronze Matrix Composites manufactured by Hot Pressing (가압소결법으로 제조된 알루미나 단섬유 보강 청동기지 복합재의 마모특성)

  • Choi, Jun-Ho;Huh, Moo-Young
    • Transactions of Materials Processing
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    • v.4 no.4
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    • pp.398-409
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    • 1995
  • The wear properties of the alumina short fiber reinforced tin-bronze matrix composites manufactured by hot pressing was studied at the room temperature and $350^{\circ}C.$ The wear loss of various specimens having different constituent and different density was examined by a pin-on-disc type wear testing machine. The results were discussed by the observation of the worn surface morphology and the analysis of the composition on the worn surfaces. Since the reinforced effect of the alumina fiber on the wear resistance was dependent on the strength of alloy matrix, the pressureless sintered composites having a lower matrix strength showed a marked increase in wear resistance by the fiber reinforcement. As the wear condition became severe, the fiber reinforcement was more effective. The delamination on the wear surface was observed in the pressureless sintered specimens having pores which are related to the initiation and the propagation of cracks. However, the wear mechanism acting on a big failure area was not found on the wear surfaces of the hot pressed specimens having a few pores.

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Microstructure and Mechanical Properties of Cu-1.1wt% Al2O3 Alloy with Cu-1.1wt% Al2O3 Powders (Cu-1.1wt% Al2O3 합금의 미세 조직과 기계적 성질)

  • Kim, Kyeong Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.2
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    • pp.96-102
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    • 2001
  • $Al_2O_3$-copper alloy has been successfully made by gas atomization, mechanical alloying and hot pressing. In order to investigate microstructure and phase, it has been studied by using scanning electron microscope, transmission electron microscope and X-ray diffractometor. Mechanical properties have been examined using hardness tester and compressive tester according to annealing temperature. Although comparatively large Cu-Al powders are milled, the reaction between Cu-Al and $Cu_2O$ occurs and very fine $Al_2O_3$ particles in the matrix particles (5-10nm) are obtained. Compressive strength of this alloy is more than that of GlidCop Al60.

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Fast-Curing of Phenol·Formaldehyde Resin Adhesives for Plywood (합판용 페놀수지 접착제의 속경화)

  • Roh, Jeang-Kwan
    • Journal of the Korean Wood Science and Technology
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    • v.23 no.3
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    • pp.33-39
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    • 1995
  • To accelerate the cure of phenolic resin adhesives for plywood, the complexation with melamine resin and the addition of cure-accelerating agents were discussed. The hot-pressing temperature and time of phenol resin could be decreased by complexation with melamine resin. but the wet glue-joints strength of phenol melamine resin was lower than that of ordinary phenol resin in case of plywood using spruce veneer at core layer. Among the tested cure-accelerating agents. the sodium carbonate showed the greatest effect on shortening gelation time of phenolic resin. In addition, in the manufacturing scale test, the hot-pressing time of phenol resin with the addition of 5 parts sodium carbonate could be shortened about 20% compared with ordinary phenol resin which had same glue-joints properties.

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Characterization of Silicon-Zinc-Oxide films by thermal annealing methods (열처리 방식에 따른 실리콘 산화아연 박막의 물성 분석)

  • Lee, Sang-Hyuk;Jun, Hyun-Sik;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 2015.07a
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    • pp.1151-1152
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    • 2015
  • Silicon zinc oxide (SZO) thin films were deposited via co-sputtering. Two kinds of post-treatment, furnace annealing and hot pressing, were carried out on the deposited SZO films. The effects of the post-treatment on the chemical bond and surface roughness of the deposited SZO films were analyzed as functions of the post-treatment conditions that were used. It was observed from the X-ray photoelectron spectroscopy (XPS) results that the amount of Si-O bonds in the SZO film drastically increased after the low-temperature furnace annealing. The experiment results showed that the hot pressing method would be favorable as it could improve the electrical characteristics of the SZO-TFTs.

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Microstructure and Properties of High Tc Superconductor fabricated by Hot Isostatic Pressing (열간정수압소결(HIP) 시킨 고온초전도체의 조직과 특성)

  • Song, Jin-Tae;Akihama, Ryozo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1988.05a
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    • pp.17-19
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    • 1988
  • $YBa_2Cu_3O_{7-x}$ oxide superconductors were fabricated by the hot isostatic pressing (HIP). It was shown that their structures were orthorombic and constited of a single (123) phase. While as-sintered compacts had many pores, they were remarkably reduced by Hiping. The on-set and off set temperature of (123) compound sintered at $950^{\circ}C$ in oxygen and hiping at $880^{\circ}C$ were the highest and it showed 0 resistance at $90^{\circ}K$. The critical current density ($J_c$) of the above superconductor was $27A/cm^2$ and it also showed a number of twin structures, which are typical of high $T_c$ superconductor. It seemed that the low current density may be due to the many pores of starting-sintered compacts.

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Research on Two Sintered Techniques of Nanometer WC-Co Powder

  • Sun, Lan;Jia, Chengchang;Tang, Hua
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.529-530
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    • 2006
  • This paper concerned with SPS (spark plasma sintering), hot pressing of sinter nanometer WC-Co powder and discussed the density, hardness, microstructures and grain sizes of the alloys sintered. The results showed that the two sintered techniques could produce high density alloys and play well on the grain growth, but SPS could lower the sintering temperature and shorten sintering time. Besides, the hardness of the sintered cemented alloys that was dependent on the grain size and densification could also be improved.

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Development of Rice Hull Insulation Board using Urea Formaldehyde Resin (요소수지(尿素樹脂) 연질(軟質) 왕겨보드의 개발(開發))

  • Lee, Hwa-Hyoung;Kang, Chun-Won
    • Journal of the Korean Wood Science and Technology
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    • v.26 no.4
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    • pp.50-55
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    • 1998
  • This study was carried out to develop low density board made of rice hull which needs proper use. Urea formaldehyde adhesive(UF) was used. The raw materials were the mixtures of the rice hulls from IllFum, DongGin, ChuChong, etc. The physical and mechanical properties of rice hull insulation board were examined. The results are as follows : For the thickness of 15mm of the low density rice hull board bonded with UF resin, proper manufacturing conditions were $171^{\circ}C$ of hot pressing temperature with thickness bar for optimum density, 12 percent of resin solid contents of rice hull ovendry weight, and 20 minutes of hot pressing time. These conditions meet Korean standards(KS 3201-1982) in relation to free formaldehyde emission, bending strength, water absorption and heat resistance.

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