• Title/Summary/Keyword: high-purity

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Avoidance of Internal Resonances in Hemispherical Resonator Assemblies from Fused Quartz Connected by Indium Solder

  • Sarapuloff, Sergii A.;Rhee, Huinam;Park, Sang-Jin
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2013.04a
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    • pp.835-841
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    • 2013
  • Modern solid-state gyroscopes (HRG) with hemispherical resonators from high-purity quartz glass and special surface superfinishing and ultrathin gold coating become the best instruments for precise-grade inertial reference units (IRU) targeting long-term space missions. Designing of these sensors could be a notable contribution into development of Korea as a space nation. In participial, 40mm diameter thin-shell resonator from high-purity fused quartz, fabricated as a single-piece with its supporting stem has been designed, machined, etched, tuned, tested, and delivered by STM Co. (ATS of Ukraine) several years ago; an extremely-high Q-factor (upto 10~20 millions) has been shown. Understanding of the best way how to match such a unique sensor with inner glass assembly of the gyro means how to use the high potential in a maximal extent; and this has become the urgent task. Inner quartz glass assembly has a very thin indium (In) layer soldered the resonator and its silica base (case), but effects of internal resonances between operational modal pair of the shell-cup and its side (parasitic) modes can notable degrade the potential of the sensor as a whole, instead of so low level of resonator's intrinsic losses. Unfortunately, there are special combinations of dimensions of the parts (so-called, "resonant sizes"), when intensive losses of energy occurs. The authors proposed to use the length of stem's fixture as an additional design parameter to avoid such cases. So-called, a cyclic scheme of finite element method (FEM) and ANSYS software were employed to estimate different combinations of gyro assembly parameters. This variant has no mismatches of numerical origin due to FEM's discrete mesh. The optimum length and dangerous "resonant lengths" have been found. The special attention has been paid to analyses of 3D effects in a cup-stem transient zone, including determination of a difference between the positions of geometrical Pole of the resonant hemisphere and of its "dynamical Pole", i.e., its real zone of oscillation node. Boundary effects between the shell (cup) and 3D short "beams" (inner and outer stems) have been ranged. The results of the numerical experiments have been compared with the classic model of a quasi-hemispherical shell band with inextensional midsurface, and the solution using Rayleigh's functions of the $1^{st}$ and $2^{nd}$ kinds. To guarantee the truth of the recommended sizes to a designer of the real device, the analytical and FEM results have been compared with experimental data for a party of real resonators. The consistency of the results obtained by different means has been shown with errors less than 5%. The results notably differ from the data published earlier by different researchers.

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A Study on the Improvement of Gamma Ray Energy Spectrum Resolution through Electrical Noise Reduction of High Purity Ge Detector (고순도 Ge 검출기의 전기적 노이즈 감소를 통한 감마선 에너지 스펙트럼의 분해능 향상에 관한 연구)

  • Lee, Samyol
    • Journal of the Korean Society of Radiology
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    • v.14 no.7
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    • pp.849-856
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    • 2020
  • In the gamma-ray energy spectrum study, nuclide analysis through energy analysis is very important. High-purity Ge detectors, which are commonly used for gamma-ray energy measurements, are commonly used because of their high energy resolution and relatively high detection efficiency. However, in order to maintain a high energy resolution, the semiconductor detector has a problem in that it is difficult to maintain the original performance if the noise generated from the surrounding environment is not effectively blocked, and the effect of the expensive device is not achieved. Therefore, in this study, ground loop isolator (NEXT-001HDGL) was used to remove the electrical noise generated from the detector. In order to test the effect of improving energy resolution, HPGe detection device newly installed in the proton accelerator KOMAC was used. In the case of gamma-ray energy 2614 keV, the energy resolution was improved from (0.16 ± 0.02) % to (0.11 ± 0.01) %, and in the case of gamma-ray energy 662 keV of 137Cs isotope, the energy resolution was improved from (0.72 ± 0.07) % to (0.27 ± 0.03) %. This result is considered to be very useful for the gamma ray spectrum study using the HPGe detection equipment of KOMAC(Korea Multi-Purpose Accelerator Complex).

Preparation of Manganese Oxide Powders by Spray Pyrolysis and its Electrochemical Characterization (Spray Pyrolysis에 의한 Manganese Oxide 입자의 제조 및 전기화학적 특성)

  • Choi, Won-Chang;Byun, Dong-Jin;Lee, Jung-Kee;Park, Dal-Keun;Kim, Hyeon-Joong
    • Korean Journal of Materials Research
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    • v.11 no.11
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    • pp.936-940
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    • 2001
  • Spray pyrolysis is a favorable technique to form complex mixed-metal oxide powders with high purity in high temperature region. Manganese oxide powders were prepared by spray pyrolysis from an aqueous solution of $Mn(NO_3)_2$. Powders were formed in the temperature range of 500~$700^{\circ}C$ under the constant pressure of 300torr. All the powders have hydrous forms. When the temperature was increased, the size and the surface area of the particles decreased. An electrochemical capacitors were made with manganese oxide electrodes and KOH electrolyte. With the temperature decreased, capacitors showed high capacitance. Capacitor which was prepared with powders formed in the temperature $500^{\circ}C$ demonstrated specific capacitances as high as 83F/g.

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The Effect of Adittives on the Sintering Properties of Barium Titanate Powder Prepared by Self-propagating High-temperature Synthesis (자전연소합성법에 의해 제조된 BaTiO3 분말의 소결특성에 미치는 첨가제의 영향)

  • Lim Sung-Jae;Shin Chang-Yun;Won Hyung-Il;Won Chang-Whan
    • Journal of Powder Materials
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    • v.13 no.2 s.55
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    • pp.129-137
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    • 2006
  • In this study, high purity fine $BaTiO_3$ powders were prepared by SHS (Self-propagating High-temperature Synthesis). We would examinate the study of sintering properties and characteristics as a function of temperature with various additives (binder, sintering agent). In separately binder addition, the green and sintered density of specimen were increased as binder content increases. The increased porosity resulted in fine grain size due to the inhibition of grain boundary moving. The $Al_{2}O_{3},\;TiO_{2}$ and MgO playa role of increasing dielectric constants at room temperature. These values were decreased at curie temperature. In case of $SiO_2$, the Curie temperature was decreased. In this study, a high dielectric ceramic capacitor material with temperature stability was synthesized by using various additives.

Design of Adiabatic Demagnetization Refrigerator for Hydrogen Re-Liquefaction (수소 재액화용 단열 탈자 냉동기의 설계)

  • Park, Ji-Ho;Kim, Young-Kwon;Jeong, Sang-Kwon;Kim, Seok-Ho
    • Progress in Superconductivity and Cryogenics
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    • v.14 no.3
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    • pp.53-59
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    • 2012
  • Adiabatic demagnetization refrigerator (ADR) for hydrogen re-liquefaction operating between 24 K and 20 K has been designed. $Dy_{0.9}Gd_{0.1}Ni_2$, whose Curie temperature is 24 K, is selected as a magnetic refrigerant. The magnetic refrigerant powder is sintered with oxygen-free high purity copper (OFHC) powder to enhance its effective thermal conductivity as well as to achieve relatively high frequency. A perforated plate heat exchanger (PPHE) operated with forced convection is utilized as a heat switch. The forced convection heat switch is expected to have fast response relative to a conventional gas-gap heat switch. A conduction-cooled high Tc superconducting (HTS) magnet is employed to apply external magnetic field variation on a magnetic refrigerant. $2^{nd}$ generation GdBCO coated conductor HTS tape with Kapton$^{(R)}$ insulation (SUNAM Inc.) will be utilized for the HTS magnet. The magnetization and demagnetization processes are to be achieved by the AC operation of the HTS magnet. The designed magnetic field and target ramp rate of the HTS magnet are over 4 T with 180 A and 0.4 T/s, respectively. AC loss distribution on HTS magnet is theoretically estimated.

Engineering Properties of High Strength Concrete Using Lime Stone Recycling Fine Aggregate (석회암 순환잔골재를 사용한 고강도 콘크리트의 공학적 특성)

  • Han, Cheon-Goo;Kim, Hyun-Woo
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.3 no.1
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    • pp.72-79
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    • 2007
  • This study investigates the engineering properties of concrete incorporating lime stone crushed fine aggregate(Ls), which has been abandoned about 20% of total production due to the low purity. Test results showed that increase of Ls had favorable fluidity and slightly decreased air content. Bleeding capacity of all specimens was not appeared as those were high strength mixture proportion, but the specimens using more Ls accelerated initial and final setting. For the mechanical properties, specimens incorporating higher ratio of Ls, overall, resulted in increase of compressive strength, and exhibited very small inclined tendency in a dynamic elasticity modulus test In addition, for the durability properties, specimens incorporating higher Ls dramatically decreased a drying shrinkage and showed similar tendency in a frost & thaw test, as well as showing no more change in an accelerated neutralization test from the beginning. In conclusion, as it was confirmed in the experimental test, the high strength concrete applying Ls did not showed any problems in the aspects of engineering properties and mostly exhibited even more excellent quality than the specimens using natural fine aggregate.

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Synthesis and Properties of Mullite from Kaolin by Boehmite Gel Coating (Boehmite Gel Coating법에 의한 Kaolin으로부터 Mullite의 합성 및 그 특성)

  • 임병수;김인섭
    • Korean Journal of Crystallography
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    • v.8 no.2
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    • pp.89-96
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    • 1997
  • In order to apply synthesis technique of the high purity ceramic powder to the traditional ceramic powder, mullite powder which is widly used for refractory materials was synthesized. Boehmite and Hadong kaolin with high alumina content were used as starting materials and gel coating method was tried to produce the mullite powder. As a result, the mullite powder of high quality was successfully obtained at 1350℃. The unreacted silica and cornudum were not observed in the synthesized mullite powder, mullite content was more than 80% when the starting materials were sintered at 1700℃. Their properties showed bulk specific gravity of 2.56, water absorption of 1.9%, and 3-point flexual strength of 169 MPa. It is thought that that their good properties are applicable to refractory materials of high quality.

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Ultra-fine Grained Aluminum Alloy Sheets fabricated by Roll Bonding Process

  • Kim, Hyeong-Uk;Tsuji, Nobuhiro
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.6.2-6.2
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    • 2009
  • Ultra-fine grained (UFG) Al alloys, which have submicron grain structures, are expected to show outstanding high strength at ambient temperature and excellent superplastic deformation at elevated temperatures and high strain rate. In order to get the UFG microstructure, various kind of severe plastic deformation (SPD) processes have been developed. Among these processes, accumulative roll bonding (ARB) process is a promising process to make bulky Al sheets with ultrafine grained structure continuously. The purpose of the present study is to clarify the grain refinement mechanism during the ARB process and to investigate on the effects of ultra-fine grained structure on the mechanical properties. In addition, UFG AA8011 alloy (Al-0.72wt%Fe-0.63wt%Si) manufactured by the ARB had fairly large tensile elongation, keeping on the strength. In order to clarify the reason for the increase of elongation in the UFG AA8011 alloy, detailed microstructural and crystallographic analysis was performed by TEM/Kikuchi-line and SEM/EBSP method. The unique tensile properties of the UFG AA8011 alloy could be explained by enhanced dynamic recovery at ambient temperature, owing to the large number of high angle boundaries and the Al matrix with high purity.

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A Study on the Characteristics of the High Concentration Ozone Generator for the Semiconductor Wafer Cleaning with the Ozone Dissolved De-ionized Water (반도체 웨이퍼의 오존 수(水) 세정을 위한 고농도 오존발생장치 특성 연구)

  • 손영수;함상용;문세호
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.52 no.12
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    • pp.579-585
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    • 2003
  • Recently the utilization of the ozone dissolved de-ionized water(DI-O3 water) in semiconductor wet cleaning process to replace the conventional RCA methods has been studied. In this paper, we propose the water-electrode type ozone generator which has the ozone gas characteristics of the high concentration and high purity to produce the high concentration DI-O3 water for the silicon wafer surface cleaning process. The ozone generator has the dual dielectric tube structure of silent discharge type and the water is both used to electrode and cooling water. We investigate the performance of the proposed ozone generator which has the design goal of the concentration of 7[wt%] and ozone generation quantity of 6[g/hr] at flow rate of 1[$\ell$/min). The experiment results show that the water electrode type ozone generator has the characteristics of 8.48[wt%] of concentration, 8.08[g/hr] of generation quantity and 76.2[g/kWh] of yield and it's possible to use the proposed ozone generator for the DI-O3 water cleaning process of silicon wafer surface.

Vapor Deposition Techniques for Synthesis of Two-Dimensional Transition Metal Dichalcogenides

  • Song, Jeong-Gyu;Park, Kyunam;Park, Jusang;Kim, Hyungjun
    • Applied Microscopy
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    • v.45 no.3
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    • pp.119-125
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    • 2015
  • Two-dimensional (2D) transition metal dichalcogenides (TMDCs) have attracted significant attention due to their unique and exotic properties attributed to their low dimensionality. In particular, semiconducting 2D TMDCs such as $MoS_2$, $WS_2$, $MoSe_2$, and $WSe_2$ have been demonstrated to be feasible for various advanced electronic and optical applications. In these regards, process to synthesize high quality 2D TMDCs layers with high reliability, wafer-scale uniformity, controllable layer number and excellent electronic properties is essential in order to use 2D TMDCs in practical applications. Vapor deposition techniques, such as physical vapor deposition, chemical vapor deposition and atomic layer deposition, could be promising processes to produce high quality 2D TMDCs due to high purity, thickness controllability and thickness uniformity. In this article, we briefly review recent research trend on vapor deposition techniques to synthesize 2D TMDCs.