• Title/Summary/Keyword: high curing temperature

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Improvement of Early Strength of Blast-Furnace Slag Blended Cement at Low Temperature (고로 슬래그 시멘트의 저온 조기 강도 증진)

  • 장복기;임용무;김윤주
    • Journal of the Korean Ceramic Society
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    • v.36 no.2
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    • pp.130-135
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    • 1999
  • The enhanced slag fineness and the batch water of low water-to-cement ratio(W/C) were employed in order to improve the early strength of blast-furnace slag blended cement at low temperature. A grinding aid was used to grind the blast-furnace slag into the fineness of 6,280$\textrm{cm}^2$/g (Blaine), and this fine slag was then homogeneously mixed with the ordinary Portland cement to produce the blast-furnace slag blended cement containing 40% slag by weight composition. On the other hand, the batch water could be reduced from W/C=0.50 (KS L 5105) to W/C=0.33 through a commercial, naphthalene type superplasticizer. Through the method mentioned above, the early strength of the blast-furnace slag blended cement at low temperature could be enhanced even somewhat higher than the Portland cement strength. And the microsturcture of the cement was studied by both the pore structure analysis and the A.C. impedance measurement.

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Application of Master Packaging System to Fresh Shiitake Mushroom Supply Chain on Semi-commercial Scale (생표고버섯에 대한 마스터 포장 시스템의 현장 적용)

  • An, Duck Soon;Lee, Ji Hye;Lee, Hye Lim;Lee, Dong Sun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.20 no.3
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    • pp.71-76
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    • 2014
  • Master packaging system is a technology combining primary and secondary packaging to preserve the fresh produce in the supply chain. Master packaging system with tailor-designed gas transfer and $CO_2$ absorber of $Ca(OH)_2$ was applied to fresh shiitake mushroom in its supply from farm to retail store. The temperature, humidity and package atmosphere were monitored through the distribution and/or storage until the packages were opened to measure the mushroom quality. Conventional perforated individual packages without secondary master pack were prepared and travelled the same path for comparison purpose. While high temperature history was observed in some initial period of actual practice of the mushroom transportation and storage unexpectedly, the package atmosphere around the produce in the master packaging system was maintained at modified atmosphere consisting of $O_2$ concentration of 0.4 to 4.2% and $CO_2$ concentration of 0.7 to 1.7%, which is known to be beneficial for the mushroom preservation. While curing the mushrooms with precooled drying was effective for quality preservation, positive effect of master packaging system could be apparent for the uncured mushroom. Harmonized combination of curing treatment, master packaging system and temperature management was suggested for the best quality preservation of the fresh shiitake mushroom.

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Flip Chip Assembly Using Anisotropic Conductive Adhesives with Enhanced Thermal Conductivity

  • Yim, Myung-Jin;Kim, Hyoung-Joon;Paik, Kyung-Wook
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.1 s.34
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    • pp.9-16
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    • 2005
  • This paper presents the development of new anisotropic conductive adhesives with enhanced thermal conductivity for the wide use of adhesive flip chip technology with improved reliability under high current density condition. The continuing downscaling of structural profiles and increase in inter-connection density in flip chip packaging using ACAs has given rise to reliability problem under high current density. In detail, as the bump size is reduced, the current density through bump is also increased. This increased current density also causes new failure mechanism such as interface degradation due to inter-metallic compound formation and adhesive swelling due to high current stressing, especially in high current density interconnection, in which high junction temperature enhances such failure mechanism. Therefore, it is necessary for the ACA to become thermal transfer medium to improve the lifetime of ACA flip chip joint under high current stressing condition. We developed thermally conductive ACA of 0.63 W/m$\cdot$K thermal conductivity using the formulation incorporating $5 {\mu}m$ Ni and $0.2{\mu}m$ SiC-filled epoxy-bated binder system to achieve acceptable viscosity, curing property, and other thermo-mechanical properties such as low CTE and high modulus. The current carrying capability of ACA flip chip joints was improved up to 6.7 A by use of thermally conductive ACA compared to conventional ACA. Electrical reliability of thermally conductive ACA flip chip joint under current stressing condition was also improved showing stable electrical conductivity of flip chip joints. The high current carrying capability and improved electrical reliability of thermally conductive ACA flip chip joint under current stressing test is mainly due to the effective heat dissipation by thermally conductive adhesive around Au stud bumps/ACA/PCB pads structure.

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Effects of Storage Conditions on Rancidity of Perilla and Sesame Seed Oils (저장조건(貯藏條件)이 들깨유(油) 및 참깨유(油)의 산패도(酸敗度)에 미치는 영향(影響))

  • Kim, Hye-Kyung;Lee, Yang-Cha;Lee, Ki-Yull
    • Journal of Nutrition and Health
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    • v.12 no.1
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    • pp.51-58
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    • 1979
  • It is a general trend everywhere that the uses of vegetable oils are increasing due to the fact that they are effective in curing and preventing symptoms of high blood pressure and various heart failure conditions. At the same time the concept that oxidative rancidity is caused by the oxidation of unsaturated fatty acid moieties whose subsequent decomposition gives rise to various undesirable, sometimes toxic compounds is now well accepted. Linolenic acid (C, 18:3) is one of highly unsaturated and readily oxidizable fatty acid. The content of this essential polyunsaturated fatty acid in perilla seed oil (PSO) was found to be as high as 48% while only 1.5% in sesame seed oil (SSO). In this experiment the oxidative stability of PSO was compared with that of SSO. The experimental test group were as follows: A) Stored at different temperatures, namely $4^{\circ}C,\;30^{\circ}C,$ and $60^{\circ}C,$ B) Stored at room temperature $(20{\pm}5^{\circ}C)$ ; a. protected from sunlight and air, b. exposed to air without sunlight c. exposed to sunlight but protected front air, d. completely exposed to both air and sunlight. The following results were obtained; 1) It was found to be most stable against oxidation to store both PSO and SSO under the low temperature $(4^{\circ}C)$ condition. According to P.V. measurements it was found to be safe to keep both oils up to $30^{\circ}C$ for at least 8 weeks. When exposed to air, sunlight and high temperature $(60^{\circ}C)$, P.V. of PSO reached there peak values, which were much higher than those of SSO. This explains much of its instability as compared to SSO against oxidation. 2) The effect of high temperature $(60^{\circ}C)$ on A.V. was found to be more striking than those of all the other storage conditions. The condition of refrigeration was most effective in keeping A.V. low for both oils as was the case in P.V. 3) For both oils, I.V. decreased throughout the experimental period (8 weeks). The range of decrement was larger for PSO than SSO. 4) There was no significant change in the compositions of fatty acids of SSO caused by various experimental storage conditions. But for PSO the compositions of stearic, oleic and linoleic acid were decreased, whereas linolenic acid was increased proportionally.

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Investigation on Factors Influencing Creep Prediction and Proposal of Creep Prediction Model Considering Concrete Mixture in the Domestic Construction Field (크리프 예측 영향요인 검토 및 국내 건설현장 콘크리트 배합을 고려한 크리프 예측 모델식 제안)

  • Moon, Hyung-Jae;Seok, Won-Kyun;Koo, Kyung-Mo;Lee, Sang-Kyu;Hwang, Eui-Chul;Kim, Gyu-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.19 no.6
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    • pp.503-510
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    • 2019
  • Recently, construction technology of RC structures must be examined for creep in concrete. The factors affecting the creep prediction of concrete and the results of creep in domestic construction field were reviewed. The longer the creep test period and the higher the compressive strength, the higher the creep prediction accuracy. The higher the curing temperature, the higher the initial strength development of the concrete, but the difference in the creep coefficients increased over time. Based on the results of creep evaluation in the domestic construction field and lab. tests, a modified predictive model that complements the ACI-209 model was proposed. In the creep prediction of real members using general to high strength concrete, the test period and temperature should be considered precisely.

A Study on the Evaluating Shrinkage Cracking Properties of Concrete by Size of Specimen of Plat-Ring Restrained Test Method (판상-링형 구속시험방법의 시험체 치수에 따른 콘크리트 수축균열 특성 평가에 관한 연구)

  • Choi, Hyeong-Gil;Nam, Jeong-Soo;Na, Chul-Sung;Back, Yong-Kwan;Kim, Gyu-Yong;Kim, Moo-Han
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.581-584
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    • 2008
  • In this study, it is willing to present that fundamental data for proposing quantitatively shrinkage cracking evaluation method such as plat-ring type restrained test method. To examine suitable size of specimen of plat-ring type restrained test method, Evaluated concrete about restrained shrinkage crack properties of numerical analysis of 3D solid element using the MIDAS program, drying shrinkage deformation, restrained shrinkage stress, crack area and crack point with inside ring diameter of specimen in 100mm, 150mm, 200mm and high of Specimen in 30mm, 50mm after curing in condition of constant temperature and usual habit of temperature 20${\pm}$3$^{\circ}$C, humidity 60${\pm}$5%. As a result, it was available about suitable estimation with inside ring diameter of specimen in more than 150mm and high of Specimen in 50mm. Hereafter, it is considered that the study concerning environmental condition and mixing factor in plat-ring type restrained test method is need.

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Adhesive bonding using thick polymer film of SU-8 photoresist for wafer level package

  • Na, Kyoung-Hwan;Kim, Ill-Hwan;Lee, Eun-Sung;Kim, Hyeon-Cheol;Chun, Kuk-Jin
    • Journal of Sensor Science and Technology
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    • v.16 no.5
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    • pp.325-330
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    • 2007
  • For the application to optic devices, wafer level package including spacer with particular thickness according to optical design could be required. In these cases, the uniformity of spacer thickness is important for bonding strength and optical performance. Packaging process has to be performed at low temperature in order to prevent damage to devices fabricated before packaging. And if photosensitive material is used as spacer layer, size and shape of pattern and thickness of spacer can be easily controlled. This paper presents polymer bonding using thick, uniform and patterned spacing layer of SU-8 2100 photoresist for wafer level package. SU-8, negative photoresist, can be coated uniformly by spin coater and it is cured at $95^{\circ}C$ and bonded well near the temperature. It can be bonded to silicon well, patterned with high aspect ratio and easy to form thick layer due to its high viscosity. It is also mechanically strong, chemically resistive and thermally stable. But adhesion of SU-8 to glass is poor, and in the case of forming thick layer, SU-8 layer leans from the perpendicular due to imbalance to gravity. To solve leaning problem, the wafer rotating system was introduced. Imbalance to gravity of thick layer was cancelled out through rotating wafer during curing time. And depositing additional layer of gold onto glass could improve adhesion strength of SU-8 to glass. Conclusively, we established the coating condition for forming patterned SU-8 layer with $400{\mu}m$ of thickness and 3.25 % of uniformity through single coating. Also we improved tensile strength from hundreds kPa to maximum 9.43 MPa through depositing gold layer onto glass substrate.

New Approach to Chuncheon Dakgalbi Processing by Various Chicken Materials, Seasoning and Cooking Methods

  • Muhlisin, Muhlisin;Kang, Sun Moon;Choi, Won Hee;Kim, Cheon-Jei;An, Byoung Ki;Kang, Chang Won;Lee, Sung Ki
    • Food Science of Animal Resources
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    • v.32 no.6
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    • pp.740-748
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    • 2012
  • This research was conducted to develop a new approach to Chuncheon Dakgalbi processing by various chicken materials, seasoning (conventional sauce/CS and new approach of seasoning by adding the curing mixture/CSA), and cooking methods. Three chicken breeds (broiler, old broiler and spent laying hen) were divided into five experimental groups: broiler-CS, old broiler-CS, old broiler-CSA, spent laying hen-CS, and spent laying hen-CSA. All samples were stored at $5^{\circ}C$ for 12 d. For sensory evaluation, all samples were cooked with conventional cooking (pan grilling) or high temperature and pressure cooking (at $121^{\circ}C$ with pressure 1.5 $Kg_f/cm^2$ for 30 min). The chicken material analysis showed that the moisture and crude protein content, cooking loss and shear-force of the old broiler and spent laying hen were higher (p<0.05) than those of the current broiler, but the crude ash, crude lipid and WHC were lower (p<0.05). The addition of CSA increased the pH value and reduced the lipid oxidation at the end of storage regardless of chicken breeds (p<0.05). The high temperature and pressure cooking method seemed to increase the taste, smell and overall-acceptability scores of the old broiler and spent laying hen Chuncheon Dakgalbi regardless of the implementation of new approach of seasoning (CSA). In conclusion, an old broiler and spent laying hen can be used as material of Chuncheon Dakgalbi by the application of a new approach of seasoning and cooking method.

The Preparation and Characteristics of High Solids Acrylic/Polyisocyanate Coatings (하이솔리드 아크릴/폴리이소시아네이트 도료의 제조와 도막 특성)

  • 김대원;황규현;정충호;우종표;박홍수
    • Polymer(Korea)
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    • v.24 no.4
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    • pp.520-528
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    • 2000
  • New high solid acrylic resins (BMHA) containing 70% of solids content have been synthesized. The environmental friendly high solid coatings (BNHS) were prepared by using these acrylic resins and polyisocyanates. The BMHA was obtained by introducing a new functional group, acetoacetoxyethyl methacrylate (AAEM), in the copolymerization of n-butyl acrylate, methyl methacrylate, and 2-hydroxyethyl acrylate. Lowering T$_{g}$ and increasing the AAEM amount in the BMHA resulted in a high value of conversion. There was no difference in conversion with the variations of OH values. In the next step, high solid BNHS coatings were prepared by the curing reaction between BMHA and polyisocyanate at room temperature. The properties of these coatings were evaluated especially for the application of automotive top-coating materials. The introduction of AAEM in the BNHS enhanced the abrasion resistance and solvent resistance of the coatings, which indicated the possible use of BNHS coatings for top-coating materials of automobile..

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An Experimental Study on Strength Properties of Concrete Using Blast-Furnace Slag Subjected to Freezing at Early Age (초기재령에서 동결을 받은 고로슬래그 콘크리트의 강도발현특성에 관한 실험적 연구)

  • Choi, Sung-Woo;Ban, Seong-Soo;Ryu, Deuk-Hyun;Choi, Bong-Joo
    • Journal of the Korea Concrete Institute
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    • v.15 no.1
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    • pp.43-51
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    • 2003
  • Recently, to consider financial and constructive aspect usage of Admixture such as Blast-Furnace Slag and Fly-Ash, are increased. Also the use of cold-weather-concrete is increased. Blast-Furnace Slag, a by-product of steel industry, have many advantage to reduce the heat of hydration, increase in ultimate strength and etc. But it also reduces early-age strength, so it is prevented from using of Blast-Furnace Slag at cold-weather-concrete. In this study, for the purpose of increasing usage of Blast-Furnace Slag at cold-weather-concrete, it is investigated the strength properties of concrete subjected to frost damage for the cause of early age curing. The factors of this experience to give early frost damaged were Freezing temperature(-1, -10, $-15^{\circ}C$), Early curing age(0, 12, 24, 48hour), Freezing times(0, 12, 24, 48hour). According to this study, if early curing is carried out before haying frost damage, the strength of concrete used admixture, subjected to frost damage, is recovered. And that properties are considered, the effect of using admixture like blast-furnace-slag, is very high