• 한국식품영양과학회지
• /
• 제35권10호
• /
• pp.1420-1426
• /
• 2006

여러 유도체 형태로 존재하는 대두 isoflavone을 산 가수 분해 방법 및 시간을 달리하면서 isoflavone 배당체의 aglycone으로의 전환율 및 aglycone의 분해여부를 실험하였다. 산 가수분해시 가열처리 조건을 $105^{\circ}C$ 항온기, $95^{\circ}C$ 수욕조, $120^{\circ}C$ heating block 및 hot plate로 달리한 결과 환류냉각장치를 이용하고 heating block에서 가수분해시키는 방법이 가장 적절한 가수분해 방법인 것으로 나타났다. 가수분해 시간 동안 aglycone의 안정성을 검토한 결과 적정 가수분해 시간인 60분 동안에는 genistein, daidzein 및 glycitein 모두 큰 함량변화가 없었다. 가수분해하는 시료의 양과 산의 비율은 시료 $10\sim30mg$당 1 N HCl 용액 1 mL의 비율이 적정하였다. 이상의 결과로부터 정량법은 0.5 g의 대두 시료에 1 N HCl용액 15 mL를 첨가하고 $120^{\circ}C$의 heating block에서 60분간 가수분해시킨 후 methanol로 50 mL로 정용하고 HPLC로 분석하도록 확립하였다. 이에 따라 대두 가공부산물의 iosflavone을 분석한 결과 착유 및 착유 후 hexane 제거를 위한 열처리 공정에서 isoflavone의 손실은 적은 것으로 나타났다.

• 분석과학
• /
• 제26권4호
• /
• pp.256-261
• /
• 2013

고춧가루의 매운맛을 나타내는 capsaicinoids인 capsaicin과 dihydrocapsaicin을 초고속액체 크로마토그래피로 간편하게 측정하기 위하여 고춧가루의 입도, 추출시간에 따른 추출율 비교하고 환류추출법과 가열블록법을 비교하였다. 환류추출법의 경우 3 시간 추출하는 것이 효율적이었으며 capsaicinoids 추출율은 덜 매운 고춧가루의 경우 입도가 고울수록 높았으나 매운 청량고추의 경우는 추출율이 입도에 영향을 덜 받았다. 시료량을 달리한 경우 용매의 사용을 동일하게하면 시료를 적게 사용하는 것이 추출율이 높았다. 환류추출법으로 3시간 추출한 것은 가열블록법으로 1 시간 추출한 것에 비하여 추출효율이 3-9% 높았으나 품질관리의 목적인 경우 신속간편 방법인 가열블록법으로 고춧가루의 capsaicinoids를 측정하는 것이 가능하였다.

• 한국해양공학회지
• /
• 제31권6호
• /
• pp.425-430
• /
• 2017

In order to reduce the cost of corrections and time needed for the block assembly process, the reverse setting method is applied for a back-heated block to neutralize deck deformation. The proper reverse setting shape for a back-heated block to correct deformation improved the deck flatness, but an excessive amount of reverse setting could inversely affect the flatness of the block. A prediction method was developed for the proper reverse setting shape using a back-heated block, considering the complex geometry of blocks, thickness of the deck plate, and thermal loading conditions such as welding and back-heating. The prediction method was developed by combining the re-meshing technique and inherent strain-based deformation analysis using the finite element method. Because the flatness deviation was decreased until the lower critical point and thereafter it tended to increase again, the optimum value for which the flatness was the best case was selected by repeatedly calculating the predefined reverse setting values. Based on this analysis and the study of the back-heating deformation of large assembly blocks, including the reverse setting shape, the mechanism for selecting the optimum reverse setting value was identified. The developed method was applied to the actual blocks of a ship, and it was confirmed that the flatness of the block was improved. It is concluded that the developed prediction method can be used to predict the optimum reverse setting shape value of a ship's block, which will reduce the cost of corrections in the construction stage.

• 한국융합학회논문지
• /
• 제8권4호
• /
• pp.199-205
• /
• 2017

이 연구에서는 3D 프린터 히팅 블록의 발열로 인해 가이드로 열이 전달되어 필라멘트가 녹는 문제점을 개선하기 위해 설계 해석과 폭발압접을 융합한 방법으로 클래드 판재를 만들었다. 클래드 판재에 대한 전단 강도시험을 하였으며, 히팅 블록으로 가공한 다음 열 해석, 열전도도, 열화상 측정 결과 다음과 같은 결론을 얻었다. 구리와 타이타늄 클래드 판재로 만든 히팅 블록에 대하여 3D 모델링 열 해석 한 결과 필라멘트 가이드 부위의 표면온도가 히팅 블록 표면온도 보다 낮은 온도가 예측되었다. 구리와 타이타늄 클래드 판재로 만든 다음 전단 강도를 측정한 결과 평균 195.6MPa 값을 얻었다. 구리와 타이타늄 클래드 판재로 만든 히팅 블록에 대하여 열전도도를 3회 측정한 결과 평균 $62.52W/m{\cdot}K$값을 나타내었다. 구리와 타이타늄 클래드 판재로 만든 히팅 블록에 대하여 열화상 카메라로 표면 온도를 측정한 결과 최대 $107.3^{\circ}C$ 측정되었으며, 필라멘트 가이드 부근에서는 $183.2^{\circ}C$ 측정되었다. 기존 필라멘트의 부위의 온도 보다 $89^{\circ}C$ 낮은 온도 분포를 보였다.

• 대한임상검사과학회지
• /
• 제40권2호
• /
• pp.113-117
• /
• 2008

It designed a study to examine the efficiency of DNA and RNA extraction from archival formalin-fixed, paraffin-embedded tissues using an non-heating and heating method. Archival paraffin blocks of liver, kidney, colon were randomly selected. Each paraffin block was prepared in 20 microtubes. For each paraffin blocks were tested non-heating DNA extraction to 10 microtubes and heating protocol under pH 7.0 and $100^{\circ}C$ to 10 microtubes. Evaluation of the results of DNA extraction was carried out by measuring concentration by UV spectrophotometry and then PCR amplification. DNA extraction content that non-heating method was liver $5{\pm}0.7{\mu}g/mL$, kidney $2{\pm}0.3{\mu}g/mL$, colon $6{\pm}0.4{\mu}g/mL$ and heating method was liver $12{\pm}0.6{\mu}g/mL$, kidney $7{\pm}0.5{\mu}g/mL$, colon $10.{\pm}0.3{\mu}g/mL$. Successful RNA extraction was observed, by ${\beta}$-actin amplification, in 46.7% sections for samples treated by the heating method versus 30.0% using non-heating DNA extraction. The extracted nucleic acid showed better values for samples heated at $100^{\circ}C$. Therefore heating extraction of nucleic acid is reliable, quick and efficiency.

• 대한용접접합학회:학술대회논문집
• /
• 대한용접접합학회 2005년도 춘계학술발표대회 개요집
• /
• pp.285-287
• /
• 2005

During fabrication of deck house block in passenger ships, the problem of unexpected large deformation and distortion frequently occurs. In this case, line and spot heating method were widely used to correct the distortion of thin plate structure. Spot heating was especially used for the case under 5mm thickness. Few papers are available on the working conditions of spot heating method but only little information on deformation control. In this study, evaluation was carried out on the temperature distribution of spot heating methods using FEA and practical experiments for various heating time. IIn FEA, heat input model was established using Tsuji's double Gaussian heat input mode (Tsuji, I., 1988). This model was verified by comparing with experimental data. Also radial shrinkage and angular distortion due to spot heating were determined and compared with experimental results. Thermo elasto-plastic analysis was performed using commercial FE code, MSC/MARC. Radial shrinkage and angular distortion were measured using 3D measuring apparatus. Based on these results, simplified analysis model for deformation by spot heating was established.

• 대한조선학회논문집
• /
• 제41권4호
• /
• pp.85-91
• /
• 2004

The objective of the present paper is to develop an analysis method for the correction of welding deformation of stiffened plate by line heating. In this paper, the equivalent loading method, based on the inherent strain theory, was used to analyze the heat-straightening of a stiffened plate. Equivalent loads were obtained by integrating the inherent strains which were determined from the highest temperature and the degree of restraint. Finally, the obtained equivalent loads were imposed, as applied loads, on the elastic analysis for the prediction of correction of welding deformation in stiffened plate. The proposed method is expected as a basic study in heat-straightening analysis of welding deformation in large scale block.

• 한국태양에너지학회 논문집
• /
• 제26권3호
• /
• pp.79-87
• /
• 2006

This study aims to presents the applicability of apartment building for renewable energy systems using method of uncomplicated calculation and computer simulation. According to the weather conditions (NASA Surface meteorology and Solar Energy) analysis, it has been found that photovoltaic and wind power system can be applied to apartment buildings application. In case study considering layout and block plan, adaptation of solar water heating, photovoltaic and wind energy system to apartment buildings was proved to produce a profit. And the application strategies of renewable energy systems can be used not only for the investment decisions for economic analysis but also for the comparative analysis of uncomplicated calculation and computer simulation.

• 한국화재소방학회논문지
• /
• 제34권3호
• /
• pp.67-75
• /
• 2020

본 연구는 산업현장에서 사용되는 분전반 내 터미널 블록의 탄화 사고를 예방하기 위한 목적으로, 전선 접속부 볼트의 이상(Abnormal) 풀림 각도에 따라 변화하는 정상전류 및 과전류의 접속부 발열 위험성을 확인하고 열적 특성을 통해 위험성을 분석하였다. 이를 위하여 터미널 블록에 Resistance temperature detector (RTD) 센서 보드를 설치하여 실시간으로 터미널 블록의 발열 온도와 온도의 변화를 측정하는 새로운 기법을 적용하였다. 실험 결과 정격 전류가 작은 터미널 블록 모델의 발열 온도가 높게 나타남에 따라 부하전류에 따른 터미널 블록 용량 선정의 중요성을 확인하였다. 또한 정격전류가 높은 터미널 블록의 정격 전류가 높을수록, 이상 풀림 정도가 클수록 탄화점이 빨라짐을 확인하였다. 이러한 발열 온도 모니터링을 통해서 실시간 발열 온도를 측정할 수 있었고 열적 분석을 통해서 단계별 위험수위 설정이 가능함을 확인할 수 있었다. 본 연구의 탄화 위험성 측정 및 분석 결과는 탄화로 인한 화재 위험성에 대한 응용 연구의 이론적 기초를 제공할 수 있다. 또한 본 연구에서 새롭게 적용한 온도 센서 보드를 활용한 열화 측정 방법은 위험수준관리 및 전기적 접촉 불량으로 인한 화재 예방 활동에 광범위하게 적용 가능할 것으로 사료된다.

• 대한설비공학회:학술대회논문집
• /
• 대한설비공학회 2009년도 하계학술발표대회 논문집
• /
• pp.603-607
• /
• 2009

About a Structure is performance external insulation is fundamantal performance for enrgy-saving. these day, most of residential structures have constructed by internal insulation method structure. The method structure internal insulation have construction and economical efficiency, but on the other hand, be generated heat loss by heat bridge especially, be generated loss heat-energy logical consequence in structure ondol. The external insulation structure method has a mert able to minimum to loss heat about heat-bridge. But the external insulation technique is unsatisfactory statues within the know-how and method of construction and materials compared with developed countries. The recently, the requirement of market related to the external insulation technique is resulted by the energy efficiency system, but it can lead to the lack of alternative technique In study on the korea type passive house building design for insulation block method of wall system has to experimental characteristic heat-energy of practice building. In result field-experimental, the heat-bridge appeared to characteristic spent heat-energy of blow 2L class and have a suffience performance it.