• 제목/요약/키워드: hard phase

검색결과 438건 처리시간 0.025초

염 보조 초음파 분무 열분해법을 이용한 ZrO2:Eu3+ 나노입자의 합성 및 발광 특성 (Synthesis and Photoluminescence Properties of ZrO2:Eu3+ Nanoparticles Using Salt-Assisted Ultrasonic Pyrolysis Process)

  • 황보영;임효령;이영인
    • 한국재료학회지
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    • 제27권5호
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    • pp.270-275
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    • 2017
  • Inorganic phosphors based on $ZrO_2:Eu^{3+}$ nanoparticles were synthesized by a salt-assisted ultrasonic spray pyrolysis process that is suitable for industrially-scalable production because of its continuous nature and because it does not require expensive precursors, long reaction time, physical templates or surfactant. This facile process results in the formation of tiny, highly crystalline spherical nanoparticles without hard agglomeration. The powder X-ray diffraction patterns of the $ZrO_2:Eu^{3+}$ (1-20 mol%) confirmed the body centered tetragonal phase. The average particle size, estimated from the Scherrer equation and from TEM images, was found to be approximately 11 nm. Photoluminescence (PL) emission was recorded under 266 nm excitation and shows an intense emission peak at 607 nm, along with other emission peaks at 580, 592 and 632 nm which are indicated in red.

인청동의 내마모성향상에 대한 연구 (A Study on the Improvement of the Wear Resistance of P-bronze)

  • 송건;권숙인;차영현
    • Tribology and Lubricants
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    • 제4권1호
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    • pp.56-68
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    • 1988
  • The wear resistance of P-bronze which is widely used as worm gear material was investigated. In order 1o study the effect of additional elements on the wear resistance of Pbronze, the applied load and sliding time were selected as variables, and SCM4, were used as against metal. The addition of Fe improve wear resistance, for it precipities hard Fe$_3$ P phase and the work hardening coefficients are lowered due to decreasing solubility of P. When Fe is added in conventional P-bronze, the alloy is rather sliding than forming wear debris by frictional force during wear test. Experimental results indicated that the wear mechanisms for P-bronze are mainly consisted of abrasive wear due to Beilby layer forming mechanism and adhesive wear due to thermally activated wear mechanism. Moreover, the weight loss is decreased in accordance with increasing load and time. However the rate of wear loss is decreased as the sliding time is increased.

In-Process Evaluation of Surface Characteristics in Machining

  • Jang, Dong-Young;Hsiao, Alex
    • Tribology and Lubricants
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    • 제11권5호
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    • pp.99-107
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    • 1995
  • This paper reported research results to develop an algorithm of on-lin evaluation of surface profiles and roughness generated by turning. The developed module consisted of computer simulation of surface profiles using mechanism of cutting mark formation and cutting vibrations, and online measurement of cutting vibrations. The relative cutting vibrations between tool and worpkiece were measured through an inductance pickup at the rate of one sample per rotation of the workpiece. The sampling process was monitored using an encoder to avoid conceling out the phase lag between waves. The digital cutting signals from the Analog-to-Digital converter were transferred to the simulation module of surface profile where the surface profiles were generated. The developed algorithm or surface generation in a hard turning was analyzed through computer simulations to consider the stochastic and dynamic nature of cutting process. Cutting tests were performed using AISI 304 Stainless Steel and carbide inserts in practical range of cutting conditions. Experimental results showed good correlation between the surface profiles and roughness obtained using the developed algorithm and the surface texture measured using a surface profilemeter. The research provided the feasibility to monitor surface characteristics during tribelogical tests considering wear effect on surface texture in machining.

Statistical Analysis of Gene Expression in Innate Immune Responses: Dynamic Interactions between MicroRNA and Signaling Molecules

  • Piras, Vincent;Selvarajoo, Kumar;Fujikawa, Naoki;Choi, Sang-Dun;Tomita, Masaru;Giuliani, Alessandro;Tsuchiya, Masa
    • Genomics & Informatics
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    • 제5권3호
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    • pp.107-112
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    • 2007
  • MicroRNAs (miRNAs) are known to negatively control protein-coding genes by binding to messenger RNA (mRNA) in the cytoplasm. In innate immunity, the role of miRNA gene silencing is largely unknown. In this study, we performed microarray-based experiments using lipopolysaccharide (LPS)-stimulated macrophages derived from wild-type, MyD88 knockout (KO), TRIF KO, and MyD88/TRIF double KO mice. We employed a statistical approach to determine the importance of the commonality and specificity of miRNA binding sites among groups of temporally co-regulated genes. We demonstrate that both commonality and specificity are irrelevant to define a priori groups of co-down regulated genes. In addition, analyzing the various experimental conditions, we suggest that miRNA regulation may not only be a late-phase process (after transcription) but can also occur even early (1h) after stimulation in knockout conditions. This further indicates the existence of dynamic interactions between miRNA and signaling molecules/transcription factor regulation; this is another proof for the need of shifting from a 'hard-wired' paradigm of gene regulation to a dynamical one in which the gene co-regulation is established on a case-by-case basis.

P2O5함량에 따른 Bioglass의 구조 분석 및 물성 측정 (Investigation on Structure and Physical Properties of Bioglasses with Various P2O5 Content)

  • 임기홍;황진명;김철영
    • 한국세라믹학회지
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    • 제26권4호
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    • pp.559-567
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    • 1989
  • Bioglasses have been known to be as one of the promising biomateials, which can be used for replacing defective hard and soft tissue. There have been many reports on biological results for this type of glass, but no systematic work has carried out on the structures and properties of the bioglass itself. In the present study, the effect of P2O5 in bioglasses on their structures and properties was examined. Infrared and Raman spectroscopy for the glass structural analysis, differential thermal and X-ray diffraction analysis for the crystallization of the bioglass were performed, and several physical properties were measured. When the glasses were heat-treated, Na2O.2CaO.3SiO2 was the major crystalline phase and $\beta$-NaCaPO4 crystal was found for the glass with high P2O5 content. The added P2O5 in the glasses enhanced the polymerization of silicate glass structure and it changed the chain-like glass structure to a sheet-like structure, and some P2O5 may stay as phosphate monomer. With addition of P2O5 in the glass the density of the glasses decreased, but not much changes in their thermal expansion coefficient, softening point and microhardness were observed.

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입자분쇄 시간변화에 따른 압전세라믹스 제작공정과 특성 분석 (Processing and Characterization of Piezoelecteric Geramics Depending on Ball Milling Time)

  • 박종호;배숙희;김철수;송석천;허창회;이상렬
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2000년도 추계학술대회 논문집 학회본부 C
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    • pp.413-415
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    • 2000
  • Piezoelectric ceramics of PZT have been developed to apply for transformers in notebook. Use of piezoelectric ceramics in applications like piezoelectric transformers was made possible by the development of new materials with high electromechanical coupling coefficients and high mechanical quality factor. "Hard" ferroelectiric ceramics of complex composition based on lead zirconate titanate with Mn additive have been prepared. The perovskitic phase reaction of the oxides. The crucial role played by the intermediate mixing and grinding procedures in the assessment of the final properties of the material was investigated. Densification up to approximately the theoretical density value was achieved. The polarization was obtained by subjecting the samples at $30kVcm^{-1}$ poling electric field, in a silicon oil bath heated at $110^{\circ}C$. Their microstructural and morphological properties were checked by X-ray diffraction analysis and scanning electron microscopy. The optimized samples presented very high qualify and electromechanical coupling factors, together with small dielectric loss.

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AIP법으로 증착된 TiN/CrN 다층박막의 특성 분석 (Analysis of Properties Multi-Layered TiN/CrN Thin Films Deposited by AIP Method)

  • 백민숙;윤동주;허기복;김병일
    • 한국재료학회지
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    • 제28권7호
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    • pp.405-410
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    • 2018
  • TiN and CrN thin films are among the most used coatings in machine and tool steels. TiN and CrN are deposited by arc ion plating(AIP) method. The AIP method inhibits the reaction by depositing a hard, protective coating on the material surface. In this study, the characteristics of multi-layer(TiN/CrN/TiN(TCT), CrN/TiN/CrN(CTC)) are investigated. For comparison, TiN with the same thickness as the multilayer is formed as a single layer and analyzed. Thin films formed as multilayers are well stacked. The characteristics of micro hardness and corrosion resistance are better than those of single layer TiN. The TiN/CrN peak is confirmed because both TCT and CTC are formed of the same component(TiN, CrN), and the phase is first grown in the (111) direction, which is the growth direction. However, the adhesion and abrasion resistance of the multilayer films are somewhat lower.

트리에탄올아민을 착화제로 사용한 무전해 니켈도금욕에서의 석출물의 조성 및 기계적 성질 (Composition and Mechanical Properties of Nickel Deposit Obtained from Electroless Nickel Plating Bath Contained Triethanolamine as Complexing Agent)

  • 여운관;문인형
    • 한국표면공학회지
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    • 제19권2호
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    • pp.31-43
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    • 1986
  • The properties of the electroless nickel deposit mainly depends on the pH of the bath, the plating temperature, and the molar ratio of nickel to hypophosphite but they are also affected by its formulation and concentration of complexing and buffering agents. According to changeing the concentration of triethanolamine and boric acid, phosphorous contents, microsturcture, crystalline, hardness and wear resistance of deposits obtained from ammoniacal alkaline bath were investigated by EPMA, differential thermal analyser, X-ray diffractometer and wear tester. The results are as follows; (1) Increasing concentration of triethanolamine in the bath, the deposits is slightly inclined to increase its phosphorous content(3.7% P). (2) In the as-plated state, the deposits are not crystallized state but they are thermally unstable phase, and they are crystallized with precipitating $Ni_3P$ at 400$^{\circ}C$. (3) The deposit containing 2.3% P has higher hardness value in the as plated and heat treated state at below 300$^{\circ}C$ than those of 3.7% phosphorous deposit (1090Hk). But in the case of heat treating at 400$^{\circ}C$, the former has lower hardness value (1000Hk) than the latter and has remarkably Ni(III) orientation by heat treatment. (4) The 3.7% phosphorous deposit heat treated at 400$^{\circ}C$ has better wear resistance than hard chromium plating.

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Implementation of an Ultrasound Elasticity Imaging System

  • Cho Gae-Young;Yoon Ra-Young;Park Jeong-Man;Kwon Sung-Jae;Ahn Young-Bok;Bae Moo-Ho;Jeong Mok-Kun
    • 대한의용생체공학회:의공학회지
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    • 제27권3호
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    • pp.117-124
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    • 2006
  • Recently, active research has been going on to measure the elastic modulus of human soft tissue with medical ultrasound imaging systems for the purpose of diagnosing cancers or tumors which have been difficult to detect with conventional B-mode imaging techniques. In this paper, a real-time ultrasonic elasticity imaging system is implemented in software on a Pentium processor-based ultrasonic diagnostic imaging system. Soft tissue is subjected to external vibration, and the resulting tissue displacements change the phase of received echoes, which is in turn used to estimate tissue elasticity. It was confirmed from experiment with a phantom that the implemented elasticity imaging system could differentiate between soft and hard regions, where the latter is twice harder than the former, while operating at an adequate frame rate of 20 frames/s.

저궤도 위성의 전력 시스템 안정화를 위한 모델링 및 제어 (Stabilization Converter Design and Modeling of LEO Satellite Power Systems)

  • 윤석택;원영진;이진호
    • 한국위성정보통신학회논문지
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    • 제5권2호
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    • pp.29-33
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    • 2010
  • 위성 산업은 상업적 군사적 유용성 등의 특성으로 인해 지속적인 발달이 이루어져 왔다. 이중에서도 위성의 전력 시스템은 위성의 수명에 직접적인 관련을 가지고 있으며, 실제 궤도상에서의 Test가 불가능한 특성을 보인다. 또한 저궤도 소형위성은 전력에 민감하므로, 효과적인 전력의 안정화 및 신뢰성 향상은 중요한 문제이다. 일반적으로 저궤도 위성의 전력은 각 부하의 특성에 따라 변환 및 제어가 이루어진다. 따라서 저궤도위성의 전력 시스템은 일반적으로 여러 단계의 전력 변환을 거치게 되므로, 신뢰성 향상을 위한 1차 및 2차 혹은 그 이상 단계의 Converter의 일반화 모델링 및 안정화를 위한 제어기 설계 및 외란에 의한 영향성의 분석이 요구된다. 본 논문에서는 저 궤도 위성 전력계 시스템의 전력 변환을 위한 Converter의 일반화 모델링을 통해 안정화 설계를 위한 파라미터를 추정하고 이를 통한 신뢰성 향상 및 최적 제어 방법에 대해 알아보기로 한다.