• Journal of the Korean Chemical Society
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• v.34 no.1
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• pp.1-9
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• 1990

Cholesteryl pentanoate $(C_{32}O_2H_{54})$ is orthorhombic, space group $P2_12_12_1$, with a = 21.930(3), b = 21.404(3), c = 6.419(5) $\AA$, Z = 4, V = 3012.8(5)$\AA$$^3$, $D_c$ = 1.04 g$cm^{-3}$, ${\lambda}(Mo\; K{\alpha}$ = 0.71069 $\AA$, $\mu$ = 0.58 $cm^{-1}$, F(000) = 1048, T = 298, R = 0.086 for 1502 unique observed reflections with I > 1.0 $\sigma$ (I). The structure was solved by direct methods and refined by cascade diagonal least-squares refinement. The C-H bond lengths and the methyl groups are fixed and refined as their ideal geometry. A comparison with other cholesteryl esters gives normal structure for the tetracyclic ring, while the tail regions of the side chain and the ester group which stands on end, show a variation from their normal values, presumably due to thermal effects. The molecules are stacked together by non-bonded van der Waals forces with the shortest intermolecular distance of 3.529 $\AA$.

• Journal of Magnetics
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• v.5 no.1
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• pp.23-25
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• 2000

We have investigated the effects of Ar and$O_2$-ion milling on the exchange coupling field ($H_{ex}$) and coercive field ($H_c$) at the interfaces between substrates and NiO/NiFe films, to understand the exchange biasing mechanism. The $O_2$-ion milling was successfully performed by means of the electron cyclotron resonance (ECR) process. We found that the local roughness gradient of the NiO surface increased by $O_2$-ion milling. The ratio of $H_{ex}/H_c$ increased from 0.87 to 1.77, whereas $H_c$ decreased by almost a half as a results of the ion milling. The decrease in $H_c$could be interpreted as due to the refinement of magnetic domain size, which arose from the increase of the local roughness gradient of the NiO surface. The decrease in low $H_c$, and increase in $H_{ex}$ in NiO spin valves by ECR-ion milling are in the right direction far use in magnetoresistance (MR) heads.

• Journal of the Korean Mathematical Society
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• v.35 no.2
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• pp.491-502
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• 1998

We obtain new fixed point theorems on maps defined on "locally G-convex" subsets of a generalized convex spaces. Our first theorem is a Schauder-Tychonoff type generalization of the Brouwer fixed point theorem for a G-convex space, and the second main result is a fixed point theorem for the Kakutani maps. Our results extend many known generalizations of the Brouwer theorem, and are based on the Knaster-Kuratowski-Mazurkiewicz theorem. From these results, we deduce new results on collectively fixed points, intersection theorems for sets with convex sections and quasi-equilibrium theorems.

• Journal of applied mathematics & informatics
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• v.6 no.1
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• pp.89-98
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• 1999

We propose some new iterative methods for solving the generalized variational inequalities where the underlying operator T is monotone. These methods may be viewed as projection-type meth-ods. Convergence of these methods requires that the operator T is only monotone. The methods and the proof of the convergence are very simple. The results proved in this paper also represent a signif-icant improvement and refinement of the known results.

• Structural Engineering and Mechanics
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• v.15 no.5
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• pp.579-608
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• 2003

This paper deals with adaptive finite element analysis of linearly elastic structures using different error estimators based on flux projection (or best guess stress values) and residual methods. Presentations are given on a typical h-type adaptive analysis, a mesh refinement scheme and the coupling of adaptive finite element analysis with automatic mesh generation. Details about different error estimators are provided and their performance, reliability and convergence are studied using six node quadratic triangular elements. Several examples are presented to demonstrate the reliability of different error estimators.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 1993.04a
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• pp.3-10
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• 1993

A new three-dimensional transition solid elements was presented for the automated three-dimensional adaptive h-refinement where the steep stress gradient exists. To be consistent with 8-node solid element with nonconforming modes in accuracy, these transition elements were improved through the addition of the associated nonconforming modes. Numerical examples show that the performance of the element and the applicability to 3D adaptations are satisfactory.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 1992.10a
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• pp.39-44
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• 1992

This paper is concerned with formulations of the hierarchical $C^{o}$-plate element on the basis of Reissner-Mindlin plate theory. On reason for the development of the aforementioned element is that it is still difficult to construct elements based on h-version concepts which are accurate and stable against the shear locking effects. An adaptive mesh refinement and selective p-distribution of the polynomial degree using hp-version of the finite element method we proposed to verify the superior convergence and algorithmic efficiency with the help of the clamped L-shaped plate problems.s.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 1990.10a
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• pp.3-8
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• 1990

A new finite element technology based on p-version of F.E.M. is discussed with reference to its potential for application to stress intensity factor computations. In linear elastic fracture mechanics, especially cracked cylindrical shells. It is shown that the p-version nutlet is far better suited for computing the stress intensity factors than the conventional h-version models with the help of three test problems. The main advantage of this technology is that the accuracy of approximation can be established without mesh refinement or the use of special procedures.

• Journal of Welding and Joining
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• v.33 no.2
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• pp.1-7
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• 2015

This article describes the basic technical concepts for applying the friction stir welding (FSW) process to titanium and its alloys. Titanium and its alloys are demanding applications of FSW. During FSW, a protective atmosphere is needed at the welding region to prevent the joints from oxidation due to the absorption of interstitial elements (O, N, and H) at high temperature. The process parameters for FSW have great influence on the microstructure and properties of the joints. No phase transformation occurred in CP Ti because FSW was achieved below the ${\beta}$-transus temperature. Therefore, the mechanical properties of the joints with CP Ti were governed by recrystallization and grain refinement. Furthermore, the strong crystallographic texture indicating <0001>//ND formed in the stir zone. On the other hands, the phase transformation occurred in Ti-6Al-4V alloy because the process temperature reached above ${\beta}$-transus temperature. For this reason, the mechanical properties of the joints with Ti-6Al-4V alloy were altered by not only recry stallization and grain refinement but also phase transformation during FSW. Engineers who want to get sound FSW joints with Ti-6Al-4V alloy have to pay attention to the control about process conditions.

• Corrosion Science and Technology
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• v.14 no.6
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• pp.313-324
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• 2015

Austenitic stainless steels have been widely used in many engineering fields because of their high corrosion resistance and good mechanical properties. However, welding or aging treatment may induce intergranular corrosion, stress corrosion cracking, pitting, etc. Since these types of corrosion are closely related to the formation of chromium carbide in grain boundaries, the alloys are controlled using methods such as lowering the carbon content, solution heat treatment, alloying of stabilization elements, and grain boundary engineering. This work focused on the effects of aging and UNSM (Ultrasonic Nano-crystal Surface Modification) on the intergranular corrosion of commercial 316L stainless steel and the results are discussed on the basis of the sensitization by chromium carbide formation and carbon segregation, residual stress, grain refinement, and grain boundary engineering.