• Title/Summary/Keyword: growth characterization

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Growth and characterization of ZnSe/GaAs epilayer by hot-wall epitaxy method (Hot-Wal Epitaxy 방법에 의한 ZnSe/GaAs 박막 성장과 특성)

  • 정태수;강창훈;유평렬
    • Journal of the Korean Vacuum Society
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    • v.8 no.3B
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    • pp.302-307
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    • 1999
  • We have grown a high quality ZnSe(100) epilayer on the GaAs(100) substrate by hot-wall epitaxy method. The FWHM value from double-crystal x-ray diffraction rocking curve and growth rate of the ZnSe epilayer grown under the optimal growth conditions were 195 arcsec and 0.03 $\mu \textrm m$/min, respectively. The $I_2^U$ and $I_2^L$ peaks, which split by strain due to lattice mismatch between substrate and epilayer, were measured from the photoluminescence experiment. And we found that the residual impurities in ZnSe epilayer were concerned with Al or CI elements from the calculated binding energy of donor impurity.

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Growth and Characterization of L-Histidine Tetrafluoroborate Single Crystals as a New Laser Damage Resistant Material

  • YOKOTANI, Atsushi;TAKEZOE, Noritaka;KUMURA, Satoshi;KONAGAYISHI, Susumu;KUROSAWA, Kou
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.06a
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    • pp.7-10
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    • 1998
  • L-Histidine tetrafluoroborate single crystals have been grown from the aqueous solution. The profitable pH value to grow large crystals, the relative flow rate to get clear crystals, crystals habit and the orientation of the obtained crystal have been clarified. We have also demonstrated that the LHBF crystal has very high damage threshold which is potentially good for generation of the phase conjugated waves.

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Growth And Characterization of $LiNbO_3$ Single Crystals ($LiNbO_3$단결정성장 및 특성 연구)

  • 손진영;노광수;이진형
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.2 no.1
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    • pp.43-50
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    • 1992
  • $ LiNbO_3$ single crystals were grown using the Czochralski Method at various pulling speeds. Macroscopic defects such as cracks, bubbles and cellular structures were observed in some crystals. Cracks and bubbles observed in the crystals depended on the pulling speed and cooling rate. $ LiNbO_3$ crystals of about 15mm diameter could be grown properly at 6-7mm/h pulling speed and $ 20^{circ}C/h$ cooling rate. In order to investigate dielectric properties and optical properties for device application, these properties were measured for the sample cut along a axis and c axis at different temperatures.

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Crystal Growth of $RE_{1-x}Ca_xMnO_3$(RE=La, Nd) by Floating Zone Method (부유대역용융법에 의한 $RE_{1-x}Ca_xMnO_3$ (RE=La, Nd)의 결정성장)

  • 정준기;조남희;김철진;이태근
    • Korean Journal of Crystallography
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    • v.11 no.4
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    • pp.231-237
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    • 2000
  • CMR Materials RE/sub 1-x/Ca/sub x/MnO₃(RE=La, Nd, A=Ca, Sr) were grown using the floating zone image furnace with halogen lamps as heat source. The growth condition was at 2∼10 mm/hr growth rate in air atmosphere, were 445∼50 rpm and 20∼25 rpm of rotation rate of feedrod and growing crystal, respectively. The grown crystals showed shiny black color and annealed at 1500℃ in a box furnace to release the residual stress during cooling. Characterization analyses of the crystal were carried out using XRD and SEM. The crystal structure of Nd/sub 0.7/Ca/sub 0.3/MnO₃ was analyzed with smart CCD XRD was lattice parameter of a=5.425(4)Å, b=5.434(4)Å, and c=7.712(5)Å, an orthorombic system with space group of pbnm.

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The cultivation and characterization of imaged abalone pearls (문양화 전복진주의 양식 및 특성평가)

  • 박라영;김판채
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.14 no.2
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    • pp.78-81
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    • 2004
  • The nacre of imaged abalone pearls was obtained as a calcium carbonate of aragonite type. This result was same the nacre of natural abalone pearl. From the observation of SEM for the nacre adhered on the pearl nucleus, it was known that the layers of calcium carbonate and conchiolin were stratified. The growth rate of nacre was found to be 0.0056∼0.0074 mm/day, which is twice faster than that of traditional method used shells. The pendant and brooch were manufactured using the imaged abalone pearls.

Single crystal growth and characterization of changeable colored cubic zirconia (변색효과 cubic zirconia의 단결정 성장과 특성평가)

  • Park, Byeong-Seok;Choi, Jong-Keon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.17 no.3
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    • pp.108-112
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    • 2007
  • Cubic Zirconia single crystals having changeable color with light source were grown by skull melting method. Strong absorption of yellow color region light by Co and Nd and the absorption in violet color region by Fe led the color change from blue-green to red-purple with the light source from fluorescent to incandescent lamp. Color of crystals varied not only by the dopants but yttria contents and the conditions far heat treatment.

Isolation and Characterization of Pseudomonas sp. T-1 Degrading Terephthalic Acid (Terphthalic Acid를 분해한는 Pseudomonas sp. T-1의 분리 및 특성)

  • 서승교
    • Journal of Environmental Health Sciences
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    • v.21 no.4
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    • pp.44-48
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    • 1995
  • 26 bacterial strains capable of growing on Terephthalic acid (TPA) in minimal medium were isolated from soil and wastewater by selective enrichment culture, and among them, one isolate which was the best in the cell growth and TPA degradation was selected and identified as Pseudomonas sp. T-1 by its characteristics. Cell growth almost revealed a stationary phase at 24 hrs after cultivation. Cell growth dramatically increased in a minimal medium containing 0.1% of TPA as a sole carbon source and TPA was not detected any more at 80 hrs after cultivation. Therefore, it is suggested that Pseudomonas sp. T-1 could be effectively used for the biological treatment of wastewater containing TPA.

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Isolation and Physiological Characterization of Bacillus clausii SKAL-16 Isolated from Wastewater

  • Lee, Sung-Hun;Park, Doo-Hyun
    • Journal of Microbiology and Biotechnology
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    • v.18 no.12
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    • pp.1908-1914
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    • 2008
  • An alkaliphilic bacterium, Bacillus clausii SKAL-16, was isolated from soil that had been contaminated with vegetable oil. The optimal pH and general pH range for bacterial growth was 8, and 7 to 10, respectively. The bacterium could grow on tributyrin and glycerol, but could not grow on acetate and butyrate. The SKAL-16 strain excreted butyric acid during growth on tributyrin, and selectively ingested glycerol during growth on a mixture of butyric acid and glycerol. The SKAL-16 generated intracellular lipase, but did not produce esterase and extracellular lipase. The DNA fragment amplified with the chromosomal DNA of SKAL-16 and primers designed on the basis of the esterase-coding gene of Bacillus clausii KSM-KI6 was not identical with the esterase-coding gene contained in the GenBank database. Pyruvate dehydrogenase, isocitrate dehydrogenase, and malate dehydrogenase activities were detected in the cell-free extract (crude enzyme).

Characterization of Hydrazine Solution Processed Multi-layered CuInSe2 Thin Films (하이드라진 용액법으로 형성된 CuInSe2 다층 박막 분석)

  • Chung, Choong-Heui
    • Journal of Surface Science and Engineering
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    • v.48 no.4
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    • pp.169-173
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    • 2015
  • $CuInSe_2$ thin films which have been widely used for thin solar cells as a light absorber were prepared by hydrazine solution processing, and their microstructural properties were investigated. Hydrazine $CuInSe_2$ precursor solutions were prepared by dissolving $Cu_2S$, S, $In_2Se_3$ and Se powder in hydrazine solvent. Multilayer $CuInSe_2$ chalcopyrite phase thin films were prepared by repeating spin-coating process using the precursor solution. Unfortunately, the presence of the interfaces between each $CuInSe_2$ layer formed by multi-layer coating impeded grain growth across the interface. Here, by doing simple interface engineering to solve the limited grain growth issue, the large grained (${\sim}1{\mu}m$) $CuInSe_2$ thin films were obtained.

Characterization of Creep-Fatigue Crack Growth Behavior for HAZ Crack Using {TEX}$C_{t}${/TEX} ($C_t$를 사용한 용접열영향부 균열의 크리프-피로 균열성장거동 특성화)

  • 백운봉;서창민;윤기봉
    • Journal of Welding and Joining
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    • v.18 no.6
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    • pp.89-95
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    • 2000
  • Creep-fatigue crack growth behavior at the heat affected zone of 1Cr-0.5Mo steel weldment has been experimentally studied. Load hold times of the tests for trapezoidal fatigue waveshapes were varied among 0, 30, 300 and 3,600 seconds. Time-dependent crack growth rates were characterized by the {TEX}$C_{t}${/TEX} estimated with the equation proposed by the previous finite element analysis work. It was concluded that the {TEX}$C_{t}${/TEX} values calculated from the properties of parent metal were quite comparable to the accurate {TEX}$C_{t}${/TEX} values calculated from both of weld and parent metals. Scatter of data was claimed due to the difference of exact location of the cracks in HAZ. The cracks have a tendency to change their path from the original location eventually to the relatively soft HAZ(ie, near-FGHAZ region, fine grained heat affected zone).

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