• Journal of the Microelectronics and Packaging Society
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• v.8 no.4
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• pp.43-45
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• 2001

For photosensitive and micro-structuring in $Li_2O-A1_2O_3-SiO_2$glasses by laser treatment, Nd:YAG laser in 355 nm and 1064 nm wavelength was irradiated to the glass to investigate fracture characterization and optical changes. The fractured glass surfaces irradiated by 1064 nm laser was observed by Scanning Electron Microscope(SEM) and optical microscope, and optical changes caused by 355 nm later was identified from absorption spectra. In this study, it could be expected that the laser treatment technology will be utilized for 3-dimensional micro-structure, internal waveguide, optical memory by optical absorption changes in glass matrix.

• Transactions of the Korean Society of Mechanical Engineers
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• v.8 no.3
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• pp.195-200
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• 1984

In-plane tension fatigue tests(R=0.1) were carried out to investigate the initiation and growth behaviors of very small surface fatigue cracks on smooth unnotched surfaces of type 304 stainless steel at room temperature. The present paper deals with the unification of two approaches to the analysis of fatigue: the one approach is based on fracture mechanics concept and the other on low-cycle fatigue concept. The results are;(1)Maximum crack length, 2 $a_{max}$, initiated at a very small surface scratch not exceeding 20 .mu.m which can exist on the surface after buffing. And the density of small surface crack is remarkably low compared to that of mild steel. (2) The growth rate, d(2a)/dN, of very small fatigue cracks can be represented by one straight line as a function of either stress intensity factor range, .DELTA. $K_{I}$ or cyclic total strain intensity factor range, .DELTA. $K_{\epsilon}$$_{I}$/, for various values of the nominal stress range.e.e.e.e.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.6 no.3
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• pp.17-25
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• 1997

This paper aims to clarify the effects of grinding conditions on the grinding force, ground surface and chipping size of workpiece in surface grinding of various ferrites with the resin bond diamond wheel. The main conclusions obtained were as follows: In a constant peripheral wheel speed, the specific grinding energy is fitted by straight lines with grinding depth coefficient($\delta$) in a logarithmic graph. The effect of both depth of cut and workpiece speed on grinding energy becomes larger in the order of Mn-Zn, Cu-Ni-Zn and Sr. When using the diamond grain of the lower toughness, the roughness of the ground surface becomes lower. The ground surfaces show that the fracture process during grinding becomes more brittle in the order of Sr, Mn-Zn and Cu-Ni-Zn. The chipping size at the corner of workpiece in grinding increases with the the increases of the depth of cut and workpiece speed, and the decrease of peripheral wheel speed. The effect of both depth of cut and workpiece speed on chipping size becomes more larger in the order of Sr, Mn-Zn and Cu-Ni-Zn.

• Proceedings of the KSME Conference
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• 2008.11a
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• pp.725-726
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• 2008

This paper proposes elastic stress intensity factors and crack opening displacements (CODs) for a slanted axial through-wall cracked cylinder under an internal pressure based on detailed 3-dimensional (3-D) elastic finite element (FE) analyses. Based on the elastic FE results, the stress intensity factors along the crack front and CODs through the thickness at the center of the crack were provided. These values were also tabulated for three selected points, i.e., the inner and outer surfaces and at the mid-thickness. The present results can be used to evaluate the crack growth rate and leak rate of a slanted axial through-wall crack due to stress corrosion cracking and fatigue. Moreover, the present results can be used to perform a detailed Leak-Before-Break analysis considering more realistic crack shape development.

• Journal of Korea Foundry Society
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• v.10 no.5
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• pp.417-425
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• 1990

The purpose of this study is to investigate the effect of Be addition on the microstructure and mechanical properties of as-cast and homogenization treated Al-Li-(Be)alloys. The ductility of as-cast Al-Li alloy was increased by the addition of Be and the fracture morphology was changed from brittle to ductile mode. Also, hardness and strength have been decreased by homogenization treatment. The morphology of eutectic structure which consists of ${\alpha}(Al)$ and ${\alpha}(Be)$ was changed from lammellae to spherical type by homogenization treatment. The shape of ${\alpha}(Be)$ phase has been revealed as hollow type by TEM observation. It consists of outer surfaces with well defined crystal facets and the core filled with ${\alpha}(Al)$. The microstructure of as-cast Al-Li-Be alloys showed coarse ${\delta}'$, fine ${\delta}'$, and coarse ${\delta}$ phases. The coarse and fine ${\delta}'$ phases were formed at Be-rich phase /matrix interfaces and in matrix, respectively. By homogenization treatment, the ${\delta}$ phase in Al-Li and Al-Li-Be alloys dissolved and the size of ${\delta}$ phase in Al-Li-Be alloys was finer than that of Al-Li alloy.

• The Journal of Korean Academy of Prosthodontics
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• v.35 no.2
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• pp.365-372
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• 1997

This study was executed to measure the shear bond strength of Panavia EX and Panavia 21 when the Ni-Cr-Be alloy castings were cemented to the enamel surfaces with these cements. The cast metal plates of Ni-Cr-Be alloy were sandblasted and cemented to acid etched enamel surface with Panavia EX or Panavia 21. Their shear bond strength were measured with Instron Universal Testing machine. Within the limits of this study, following conclusions were withdrawn. 1. The mean shear bond strength were 26.85.7MPa, in Panavia EX and 28.35.2MPa, in Panavia 21. 2. t-Test revealed no statistical significance between two groups(.05 level) 3. Macroscopically, bond failures were revealed compound fracture at metal and enamel interfaces, in cases of both cements, as the cement attached partly on both metal and enamel surface.

• Journal of the Korean Vacuum Society
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• v.17 no.2
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• pp.122-129
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• 2008

Ferroelectric properties of the PMT-PT were also studied from the temperature dependence of hysteresis loops using a method slightly modified from Sawyer-Tower's. Dielectric, pyroelectric and piezoelectric properties of the ceramics in the system PMT-PT were investigated. The resulted densities of the PMT-PT ceramics system were greater than 97 % of the theoretical value. As observed SEM micrograph of the fracture surfaces of the PMT-PT ceramics system, the average grain sizes were increased about 3-5 ${\mu}m$ to 6-8 ${\mu}m$ with increasing sintering temperature. The specimens with PT<0.30 for PMT-PT solid solution system exhibited the dielectric and pyroelectric properties of a typical relaxor ferroelectrics. The composition with the maximum dielectric constant exhibits relatively superior pyroelectric and piezoelectric properties.

• Journal of the Korean institute of surface engineering
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• v.45 no.6
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• pp.284-288
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• 2012

A study on microstructure control of multi-phase steel have been implemented to higher strength with improved formability. However, it is well known that the high strength of steel are susceptible to hydrogen embrittlement. The mechanisms of hydrogen embrittlement is caused by complex interactions. In this paper, the test specimens were fabricated to 5 type of 590DP steels at different levels of volume faction. The hydrogen charging was conducted by electrochemical hydrogen-charge method with varying charging time. The relationship between hydrogen concentration and volume fraction of 590DP steel was established by SP test and SEM-fractography. It was shown that the hydrogen amounts charged in 590DP steels increased with increasing the volume faction of austenite. The maximum loads of the 590DP steels in SP test were sharply decreased with increasing hydrogen charging time. The results of SEM-fractography investigation showed typical brittle-fracture surfaces for hydrogen-charged 590DP steels.

• Journal of Biomedical Engineering Research
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• v.16 no.4
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• pp.533-542
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• 1995

The present study investigated the effectiveness of pretreatment on dentin bonding. The adhesive resin was 5% 4-methacryloyloxyethyl trimellitate anhydride (4-META) in methyl methacrylate (MMA) combined with poly-MMA powder. Polymerization of this resin was initiated by tri-n-butyl borage (TBB). Ground bovine dentin samples were etched with either an aqueous solution of 10% citric (10-0 solution) (Group I) or aqueous solution of 10% citric acid and 3% ferric chloride(10-3 solution) (Group ll ). After etching, the primer (an aqueous solution of 35% hydroxyethyl methacrylate (HEM- A) and 5% glutaraldehyde was applied on the differently etched surfaces (Group III , Group IV). The 10-0 treatment showed the lowest tensile bond strength, followed by the 10-3 treatment, primer application after the 10-0 treatment and primer application after the 10-3 treatment. The relationship among the surface morphology after pretreatment, fractured surface morphology and tensile bond strength was examined. It revealed that the surface morphology change by different pretreatment influenced the bond strength and the resulting fractured surface morphology. The correlation of tensile bond strength with the fracture morphology was explained.

• Journal of the Korean Ceramic Society
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• v.55 no.4
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• pp.337-343
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• 2018

The influence of solid loading in the slurry composition on the morphology of 3Y-TZP granules fabricated by two-fluid spray drying was investigated for solid contents varying between 30 wt% and 50 wt%. The resulting 3Y-TZP granules showed a sphere-like shape with diameters of $40-70{\mu}m$. However, a donut-like shape and a few cracks were observed on the granule surfaces fabricated using the slurry with 50 wt% solid content. The green density after cold isostatic pressing at 200 MPa was $2.1-2.2g/cm^3$, and a homogeneous fracture surface was obtained by complete destruction of granules. After sintering at $1500^{\circ}C$ for 2 h, all specimens had relative densities of 96.2 - 98.3%. With increasing solid content, the relative density decreased from 98.3% to 96.2%, but the grain size increased from $0.3{\mu}m$ to $0.6{\mu}m$. Highly sinterable zirconia granule powder could be obtained by controlling the slurry composition.