• Restorative Dentistry and Endodontics
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• v.32 no.2
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• pp.130-137
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• 2007

This in vitro study examined the effect of surface defects on cutting blades on the extent of the cyclic fatigue fracture of HEROShaper Ni-Ti rotary files using fractographic analysis of the fractured surfaces. A total of 45 HEROShaper (MicroMega) Ni-Ti rotary flies with a #30/.04 taper were divided into three groups of 15 each. Group 1 contained new HEROShapers without any surface defects. Group 2 contained HEROShapers with manufacturing defects such as metal rollover and machining marks. Croup 3 contained HEROShapers that had been clinically used for the canal preparation of 4-6 molars A fatigue-testing device was designed to allow cyclic tension and compressive stress on the tip of the instrument whilst maintaining similar conditions to those experienced in a clinic. The level of fatigue fracture time was measured using a computer connected the system. Statistical analysis was performed using a Tukey's test. Scanning electron microscopy (SEM) was used for fractographic analysis of the fractured surfaces. The fatigue fracture time between groups 1 and 2, and between groups 1 and 3 was significantly different (p<0.05) but there was no significant difference between groups 2 and 3 (p>0.05). A low magnification SEM views show brittle fracture as the main initial failure mode At higher magnification, the brittle fracture region showed clusters of fatigue striations and a large number of secondary cracks. These fractures typically led to a central region of catastrophic ductile failure. Qualitatively, the ductile fracture region was characterized by the formation of microvoids and dimpling. The fractured surfaces of the HEROShapers in groups 2 and 3 were always associated with pre-existing surface defects. Typically, the fractured surface in the brittle fracture region showed evidence of cleavage (transgranular) facets across the grains, as well as intergranular facets along the grain boundaries. These results show that surface defects on cutting blades of Ni-Ti rotary files might be the preferred sites for the origin of fatigue fracture under experimental conditions. Furthermore this work demonstrates the utility of fractography in evaluating the failure of Ni-Ti rotary flies.

• Safety and Health at Work
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• v.1 no.1
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• pp.43-50
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• 2010

Objectives: The objective of this study was to investigate the effect of chain installation condition on stress distribution that could eventually cause disastrous failure from sudden deformation and geometric rupture. Methods: Fractographic method used for the failed chain indicates that over-stress was considered as the root cause of failure. 3D modeling and finite element analysis for the chain, used in a crane hook, were performed with a three-dimensional interactive application program, CATIA, commercial finite element analysis and computational fluid dynamic software, ANSYS. Results: The results showed that the state of stress was changed depending on the initial position of the chain that was installed in the hook. Especially, the magnitude of the stress was strongly affected by the bending forces, which are 2.5 times greater (under the simulation condition currently investigated) than that from the plain tensile load. Also, it was noted that the change of load state is strongly related to the failure of parts. The chain can hold an ultimate load of about 8 tons with only the tensile load acting on it. Conclusion: The conclusions of this research clearly showed that a reduction of the loss from similar incidents can be achieved when an operator properly handles the installation of the chain.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.12
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• pp.2055-2060
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• 2003

Striation is a typical pattern observed on the fatigue fracture surface and the spacing is known to correspond to a macroscopic fatigue crack growth rate, and many models for the predict in the formation of such striation have been proposed. However, these theories and methods can't be applied under random loading spectrum. In this study, the fatigue tests were carried out on aluminum alloy under random loading spectrum. The fatigue fracture surfaces were observed in the scanning electron microscope (SEM) and great quantities of SEM micrographs were synthesized and saved in computer system. The space and morphology of several large-scale striations, which are expected to from at the relatively greater load range in loading block, were observed. The crack length for each loading blocks was decided in consideration of regularity and repetition of those striations. It is shown that the applicability of fractographic methods on the fatigue fracture surface under random loading spectrum.

• Applied Microscopy
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• v.26 no.4
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• pp.447-456
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• 1996

Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

• KEPCO Journal on Electric Power and Energy
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• v.7 no.1
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• pp.125-128
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• 2021

This paper presents the root cause failure analysis of the circulating water pump in the 560 MW thermal power plant. A fractured austenitic stainless-steel shaft operated for 24 years was examined. Fracture morphology was investigated by micro and macro-fractographic analysis. The metallurgical analyses including chemical analysis, metallography and hardness testing were performed. The analysis reveals that the pump shaft was fractured due to the reverse bending load with combination of rotating bending load. Corrective actions for plant operator was recommended based on the analysis.

• Restorative Dentistry and Endodontics
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• v.34 no.5
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• pp.424-429
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• 2009

This study aimed to assess the influence of different cross-sectional area on the cyclic fatigue fracture of Ni-Ti rotary files using a fatigue tester incorporating cyclical axial movement. Six brands of Ni-Ti rotary files (ISO 30 size with. 04 taper) of 10 each were tested: Alpha system (KOMET), HeroShaper (MicroMega), K3 (SybronEndo), Mtwo (VDW), NRT (Mani), and ProFile (Dentsply). A fatigue-tester (Denbotix) was designed to allow cyclic tension and compressive stress on the tip of the instrument. Each file was mounted on a torque controlled motor (Aseptico) using a 1:20 reduction contra-angle and was rotated at 300 rpm with a continuous, 6 mm axial oscillating motion inside an artificial steel canal. The canal had a $60^{\circ}$ angle and a 5 mm radius of curvature. Instrument fracture was visually detected and the time until fracture was recorded by a digital stop watch. The data were analyzed statistically. Fractographic analysis of all fractured surfaces was performed to determine the fracture modes using a scanning electron microscope. Cross-sectional area at 3 mm from the tip of 3 unused Ni-Ti instruments for each group was calculated using Image-Pro Plus (Imagej 1.34n, NIH). Results showed that NRT and ProFile had significantly longer time to fracture compared to the other groups (p < .05). The cross-sectional area was not significantly associated with fatigue resistance. Fractographycally, all fractured surfaces demonstrated a combination of ductile and brittle fracture. In conclusion, there was no significant relationship between fatigue resistance and the cross-sectional area of Ni-Ti instruments under experimental conditions.

• Proceedings of the Korean Society For Composite Materials Conference
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• 1999.04a
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• pp.1.1-4
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• 1999

The toughening mechanism and fracture behavior of rubber/polymer composites were investigated with respect to two factors; (1) the composition ratio of polymers(PPO and PS which have a different chain flexibility) and (ii) the rubber particle size in PPO/PS blend system Izod impact test and fractographic observation of the fracture surface using scanning electron microscope were conducted, Finite element analysis were carried out to gain understanding of plastic deformation(shear yielding and crazing) of these materials.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.107-113
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• 2009

In this study, the importance of failure analysis on large ring forged products was assessed and the process and methodology were introduced. Failure analysis case study of the large ring forged steel product with approximately 10 mm long internal crack found by non-destructive test (NDT) was presented. The micrographic and fractographic observations and the verifying tests were conducted on the cracked specimen to identify the possible metallurgical reason for the defects, and the metallurgical aspects of internal crack formation were discussed.

• Proceedings of the KSME Conference
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• 2008.11a
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• pp.244-249
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• 2008

It happened a failure on special bolt which supported main landing gear actuator up-lock rod of 00 aircraft. Fracture was occurred at end of center drilled hole and thread machined on bolt. Metallographic, fractographic, and other characteristics of embrittlement analysis and experiments carried out on the failed bolt to find out the reason. Bolt surface was cadmium electroplated(EP) to give lubrication and provide excellent corrosion resistance. Resultly, Bolt was failed due to cadmium embrittlement occurred during baking treatment as well as center drilled hole. for the failure that are relevant to failure analysis and prevention. For their successful functional application, cadmium EP bolts require proper and adequate baking treatment after electroplating, and is complete with no center drilled hole

• Korean Journal of Materials Research
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• v.14 no.8
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• pp.579-586
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• 2004

A study on the effects of oxide growth on the mechanical properties degradation of pure zirconium and Zircaloy-4 is carried out with high temperature tensile tests. It is found that the mechanical properties can deteriorate with the oxide growth less than $1\%$ of total specimen cross section, especially at $300\~400^{\circ}C$ that is zirconium alloy cladding temperature during the nuclear reactor operation. It is also revealed that Young's modulus changes little but yield strength and tensile strength drop down to $20\% and 40\%$ of the room temperature strength, respectively, in the temperature range. Fractographic analysis shows that the number of dimples decreases and fractured surface becomes smooth with increasing oxide thickness.