• Carbon letters
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• v.20
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• pp.1-9
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• 2016

Activated carbon was synthesized from coconut shells. The Brunauer, Emmett and Teller surface area of the synthesized activated carbon was found to be 1640 m²/g with a pore volume of 1.032 cm³/g. The average pore diameter of the activated carbon was found to be 2.52 nm. By applying the size-strain plot method to the X-ray diffraction data, the crystallite size and the crystal strain was determined to be 42.46 nm and 0.000489897, respectively, which indicate a perfect crystallite structure. The field emission scanning electron microscopy image showed the presence of well-developed pores on the surface of the activated carbon. The presence of important functional groups was shown by the Fourier transform infrared spectroscopy spectrum. The adsorption of methyl orange onto the activated carbon reached 100% after 12 min. Kinetic analysis indicated that the adsorption of methyl orange solution by the activated carbon followed a pseudo-second-order kinetic mechanism (R² > 0.995). Therefore, the results show that the produced activated carbon can be used as a proper adsorbent for dye containing effluents.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.6 no.2
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• pp.141-154
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• 1996

Intrinsic layers of homoepitaxial InP grown by the hydride vapor phase epitaxy (VPE) technique were investigated by Fourier-transform photoluminescence(FTPL) and variable temperature Hall measurements. The effect of process variables (i.e., source zone temperature and inlet mole fractions of HCl and $PH_{3}$) on the backgroudn impurity levels was investigated. The background carrier concentration was found to decrease with decreasing source zone temperature and increasing HCl, but was relatively independent of $PH_{3}$ for the range of mole fraction studied. The presence of background donors and acceptors was clearly verified in the FTPL spectra, and the major impurities were tentatively identified as Si donors and Zn acceptors as well as some unidentified acceptors.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.51 no.11
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• pp.551-558
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• 2002

A time-domain combined field integral equation (CFIE) is presented to obtain the transient scattering response from arbitrarily shaped three-dimensional conducting bodies. This formulation is based on a linear combination of the time-domain electric field integral equation (EFIE) with the magnetic field integral equation (MFIE). The time derivative of the magnetic vector potential in EFIE is approximated using a central finite difference approximation and the scalar potential is averaged over time. The time-domain CFIE approach produces results that are accurate and stable when solving for transient scattering responses from conducting objects. The incident spectrum of the field may contain frequency components, which correspond to the internal resonance of the structure. For the numerical solution, we consider both the explicit and implicit scheme and use two different kinds of Gaussian pulses, which may contain frequencies corresponding to the internal resonance. Numerical results for the EFIE, MFIE, and CFIE are presented and compared with those obtained from the inverse discrete Fourier transform (IDFT) of the frequency-domain CFIE solution.

• Carbon letters
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• v.16 no.3
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• pp.171-182
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• 2015

Mesophase pitch is an important starting material for making a wide spectrum of industrial and advanced carbon products. It is produced by pyrolysis of petroleum residues. In this work, mesophase formation behavior in petroleum residues was studied to prepare environmentally-benign mesophase pitches, and the composition of petroleum residues and its influence on the mesophase formation was investigated. Two petroleum residues, i.e., clarified oil s (CLO-1, CLO-2) obtained from fluid catalytic cracking units of different Indian petroleum refineries, were taken as feed stocks. A third petroleum residue, aromatic extract (AE), was produced by extraction of one of the CLO-1 by using N-methyl pyrrolidone solvent. These petroleum residues were thermally treated at 380℃ to examine their mesophase formation behavior. Mesophase pitches produced as a result of thermal treatment were characterized physico-chemically, as well as by instrumental techniques such as Fourier-transform infrared spectroscopy, nuclear magnetic resonance, X-ray diffraction and thermogravimetry/derivative thermogravimetry. Thermal treatment of these petroleum residues led to formation of a liquid-crystalline phase (mesophase). The mesophase formation behavior in the petroleum residues was analyzed by optical microscopy. Mesophase pitch prepared from CLO-2 exhibited the highest mesophase content (53 vol%) as compared to other mesophase pitches prepared from CLO-1 and AE.

• Journal of the Korean Institute of Intelligent Systems
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• v.9 no.4
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• pp.426-435
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• 1999

A high impedance fault(HIF) is one of the serious problems facing the electric utility industry today. Because of the high impedance of a downed conductor under some conditions these faults are not easily detected by over-current based protection devices and can cause fires and personal hazard. In this paper a new method for detection of HIF which uses adaptive neuro-fuzzy inference system (ANFIS) is proposed. Since arcing fault current shows different changes during high and low voltage portion of conductor voltage waveform we firstly divided one cycle of fault current into equal spanned four data windows according to the mangnitude of conductor voltage. Fast fourier transform(FFT) is applied to each data window and the frequency spectrum of current waveform are chosen asinputs of ANFIS after input selection method is preprocessed. Using staged fault and normal data ANFIS is trained to discriminate between normal and HIF status by hybrid learning algorithm. This algorithm adapted gradient descent and least square method and shows rapid convergence speed and improved convergence error. The proposed method represent good performance when applied to staged fault data and HIFLL(high impedance like load)such as arc-welder.

• Proceedings of the Earthquake Engineering Society of Korea Conference
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• 2005.03a
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• pp.18-25
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• 2005

Stochastic ground-motion method is adopted to simulate horizontal PGA values for the offshore Uljin earthquake recorded at nationwide seismic stations. For this purpose, the Fourier spectra are calculated at every stations based on comprehensive results of wave propagation and site effect which were previously revealed through inversion process applied to large accumulated spectral D/B. In addition, the apparent source spectrum of the offshore Uljin earthquake is estimated by removing the path and site response from the observed spectra. The distance dependent time-duration model is revised by iteratively fitting the PGA values generated by using the raw spectra data to the observed PGA data. The stochastic ground-motion method predicts the observed PGA values within a error of ${\sigma}_{log10}=0.1$. Transfer functions of a site relative to another site are estimated based on the error residual of the inversion results and used to convert PGA values at multiple stations to expected PGA values at a reference station of TJN. The converted PGA values can be used as basic data to evaluate the ground-motion attenuation relations developed for seismic hazard analysis that concerns the large damaging earthquakes.

• Mass Spectrometry Letters
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• v.3 no.3
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• pp.63-67
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• 2012

The need of heavy and unconventional crude oil as an energy source is increasing day by day, so does the importance of petroleomics: the pursuit of detailed knowledge of heavy crude oil. Crude oil needs techniques with ultra-high resolving capabilities to resolve its complex characteristics. Therefore, ultra-high resolution mass spectrometry represented by Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS) has been successfully applied to the study of heavy and unconventional crude oils. The analysis of crude oil with high resolution mass spectrometry (FT-ICR MS) has pushed analysis to the limits of instrumental and methodological capabilities. Each high-resolution mass spectrum of crude oil may routinely contain over 50,000 peaks. To visualize and effectively study the large amount of data sets is not trivial. Therefore, data processing and visualization methods such as Kendrick mass defect and van Krevelen analyses and statistical analyses have played an important role. In this regard, it will not be an overstatement to say that the success of FT-ICR MS to the study of crude oil has been critically dependent on data processing methods. Therefore, this review offers introduction to peotroleomic data interpretation methods.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.04b
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• pp.3-6
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• 2009

Aluminum nitride (AIN) thin films were deposited on a polycrystalline 3C-SiC intermediate layer by a pulsed reactive magnetron sputtering system. Characteristics of the AIN/SiC heterostructures were investigated by field emission scanning electron microscopy (FE-SEM), atomic force microscopy (AFM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FT-IR). The columnar structure of AIN thin films was observed by FE-SEM. The surface roughness of AlN films on the 3C-SiC buffer layer was measured using AFM. The XRD pattern of AlN films on SiC buffer layers was highly oriented at (002). Full width at half maximum (FWHM) of the rocking curve near (002) reflections was $1.3^{\circ}$. The infrared absorbance spectrum indicated that the residual stress of AIN thin films grown on SiC buffer layers was nearly negligible. The 3C-SiC intermediate layers are promising for the realization of nitride based electronic and mechanical devices.

• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.381.1-381.1
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• 2014

In this study, we investigated the deposition behavior and the etch resistivity of plasma polymerized carbon hardmask (ppCHM) film with the variation of process temperature. The etch resistivity of deposited ppCHM film was analyzed by thickness measurement before and after direct contact reactive ion etching process. The physical and chemical properties of films were characterized on the Fourier transform infrared (FT-IR) spectroscope, Raman spectroscope, stress gauge, and ellipsometry. The deposition behavior of ppCHM process with the variation of temperature was correlated refractive index (n), extinction coefficient (k), intrinsic stress (MPa), and deposition rate (A/s) with the hydrocarbon concentration, graphite (G) and disordered (D) peak by analyzing the Raman and FT-IR spectrum. From this experiment we knew an optimal deposition condition for structure of carbon hardmask with the higher etch selectivity to oxide. It was shown the density of ppCHM film had 1.6~1.9 g/cm3 and its refractive index was 1.8~1.9 at process temperature, $300{\sim}600^{\circ}C$. The etch selectivity of ppCHM film was shown about 1:4~1:8 to undoped siliconoxide (USG) film (etch rate, 1300 A/min).

• Journal of Power Electronics
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• v.9 no.2
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• pp.224-231
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• 2009

The induction motor rotor fault diagnosis system using current signals, which are measured using an axis-transformation method, is presented in this paper. In inverter-fed motor drives, unlike line-driven motor drives, the stator currents are rich in harmonics; therefore fault diagnosis using stator current is not trivial. The current signals for rotor fault diagnosis need precise and high resolution information, which means the diagnosis system demands additional hardware such as a low pass filter, high resolution ADC, and encoder, etc. The proposed axis-transformation method with encoder and without encoder is expected to contribute to a low cost fault diagnosis system in inverter-fed motor drives without the need for any additional hardware. In order to confirm the validity of the developed algorithms, various experiments for rotor faults are tested and the line current spectrum of each faulty situation using Park transformation is compared with the results obtained from fast Fourier transforms.