• 한국주조공학회지
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• 제32권2호
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• pp.75-80
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• 2012

In this study, we are aimed to prevent grain growth of semi-solid AZ31 magnesium alloys during reheating process. The semi-solid AZ31+(Ca) billets were investigated by using metallographic analysis, X-ray diffraction, scanning electron microscopy and energy dispersive spectroscopy in order to elucidate the effect of Ca addition during reheating process. The grain growth of semi-solid AZ31+(Ca) billet was reduced with increasing Ca content during reheating. The grain size of AZ31+(Ca) billet decreased with increasing volume fraction of Al2Ca particles. The grain growth rate constant K calculated by Oswald ripening LSW theory in AZ31+1.5wt.% Ca billet was the lowest 129.

• 한국주조공학회지
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• 제37권1호
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• pp.14-20
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• 2017

The microstructure, electrical conductivity and hardness variation of an AZ91-5wt%Sn Mg alloy sample during a solid-solution and aging heat treatment were instigated by optical microscopy, scanning electron microscopy, X-ray diffraction and by Rockwell hardness techniques in this study. The XRD result shows that the main phases in the as-casted alloy are ${\alpha}$-Mg, $Mg_{17}Al_{12}$ and $Mg_2Sn$. From the SEM images of the AZ91-5wt%Sn Mg alloy after the solution treatment, the $Mg_{17}Al_{12}$ phases in the alloy were found to have dissolved into the matrix with an increase in the holding time during the solution treatment, but $Mg_2Sn$ phases were clearly observable. The highest peak hardness of the AZ91-5wt%Sn Mg alloy is 82HRE at an aging temperature of $200^{\circ}C$.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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• pp.861-864
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• 2002

Ferroelectric $Bi_{4-x}Nd_xTi_3O_{12}$(BNdT) thin films with the composition(x=0.75) were prepared on pt/Ti/$SiO_2$/Si(100) substrate by metal-organic deposition. The electrical and structural characteristics of BNdT thin films were investigated to develop ferroelectric thin films for capacitor layers of FRAM. After spin coating, thin films were annealed at $650^{\circ}C$ for 1hour in oxygen atmosphere. Scanning electron micrographs showed uniform surfaces composed of rod-like grains. The $Bi_{4-x}Nd_xTi_3O_{12}$(X=0.75) thin film capacitors with a Pt top electrode showed better ferroelectric properties. At the applied voltage of 5V, the dielectric constant$(\varepsilon_r)$, dissipation factor$(tan{\delta})$, remanent polarization(2Pr) and nonvolatile swiching charge of the $Bi_{4-x}Nd_xTi_3O_{12}$(x=0.75)thin films were about 346.7, 0.095, $56{\mu}C/cm^2$ and $38{\mu}C/cm^2$ respectively. Also the capacitor did not show any significant fatigue up to $8{\times}10^{10}$ read/write switching cycles at a frequency of 1MHz.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.2
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• pp.1033-1036
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• 2004

Si nanocrystallites thin films on p-type (100) Si substrate have been fabricated by pulsed laser deposition using a Nd:YAG laser. After deposition, samples were annealed at the temperatures of 400 to $800^{\circ}C$. Hydrogen passivation was then performed in the forming gas (95% $N_2$ + 5% $H_2$) for 1 hr. Strong violet-indigo photoluminescence has been observed at room temperature from nitrogen ambient-annealed Si nanocrystallites. The variation of photoluminescence (PL) Properties of Si nanocrystallites thin films has been investigated depending on annealing temperatures with hydrogen passivation. From the results of PL, Fourier transform infrared (FTIR), and high-resolution transmission electron microscopy (HRTEM) measurements, it is observed that the origin of violet-indigo PL from the nanocrystalline silicon in the silicon oxide film is related to the quantum size effect of Si nanocrystallites and oxygen vacancies in the SiOx(x : 1.6-1.8) matrix affects the emission intensity.

• ETRI Journal
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• 제18권4호
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• pp.339-346
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• 1997

Good quality a-axis oriented thin films of $YBa_2Cu_3O_{7-x}$ may be grown by the use of a $PrBa_2Cu_3O_{7-x}$ (PBCO) layer as a template. Here we present a detailed study of the nucleation of the PBCO layer, explaining the orientations observed. It is determined that the wavy surface of a $LaSrGaO_4$ (LSGO) (100) substrate consists of the {101} planes by observing cross-sectional transmission electron microscopy images of the interface between the PBCO film and the substrate. The images and selected area diffraction patterns show that a mixed c-and b-axis oriented PBCO layer was initially grown on the substrate, followed by pure b-axis oriented PBCO growth. We explain that the c-axis oriented growth is the result of the growth of the PBCO (019) planes on the LSGO (101) planes. We conclude that the nucleation and growth of the PBCO films at the initial stages depends on the crystallographic plane of the substrate surfaces, however, as the film grows further, the kinetics of the deposition process favors b-axis oriented growth.

• 한국주조공학회지
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• 제32권5호
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• pp.231-240
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• 2012

In present study, the effect of heat treatment on the microstructure and mechanical properties of the gravity cast superchargers housing using A356 alloy were investigated. In order to identify the characteristics of superchagers housing casting with heat treatment, Vickers hardness test, electrical conductivity test, opical and scanning electron microscopy were performed. And also, to investigate their mechanical properties, the T6 treated superchagers housing casting in optimum heat treatment condition were carried out tensile test using UTM (Universal Testing Machine).

• Parasites, Hosts and Diseases
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• 제50권2호
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• pp.177-180
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• 2012

Cercaria caribbea LVIII Cable, 1963 (Digenea: Cyathocotylidae) was detected from a brackish water gastropod species (Cerithideopsilla cingulata) in a coatal area of Shinan-gun, Jeollanam-do (Province), the Republic of Korea, and its surface ultrastructure was studied using a scanning electron microscope. The cercariae were found freely swimming or enveloped within daughter sporocysts when the snail host was mechanically broken. They were morphologically characterized by a linguiform and ventrally concave body, a long and bifurcated tail, and the presence of a holdfast (=tribocytic) organ posterior to the ventral sucker. On the whole ventral and dorsal surfaces, peg-like tegumental spines were densely distributed. Around the oral sucker, several sensory papillae, each with a short cilium, were distributed, and on the tail, sensory papillae, each with an extensively long cilium, were observed. This is the first record describing a cyathocotylid cercaria from a brackish water gastropod in the Republic of Korea.

• Journal of Plant Biotechnology
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• 제1권1호
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• pp.31-38
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• 1999

An artificial symbiosis was established between diazotropic Azomonas insignis and strawberry (Fragaria x ananassa). The partnership was created by in vitro techniques through callus induction and organogenesis. The basis of this partnerships is the bacterial dependence on the plants metabolic activity, using maltose in the medium as a carbon and energy source which can be utilized by the plant cells only. The presence of bacteria in the intercellular spaces of the callus tissues and regenerated plants was proven by microscopic techniques. Nitrogenase activity could also be detected in the plant tissues. For successful and high frequency introduction of bacteria to the plant tissues, biolistic gun method was used. On the basis of the DNA transfer method, Azotobacter vinelandii bacteria were delivered directly into strawberry tissues by the particle bombardment. This was the first use of living bacteria as microprojectils for bombardment of plant tissues. The treatment was successful, the presence of bacteria in the developing callus tissue and regenerated plants were detected by light and electron microscopy.

• 대한기계학회논문집A
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• 제27권6호
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• pp.1034-1040
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• 2003

Tension mask is a part of CRT type devices, which is installed right behind glass-made front panel. Numerous slits on the thin metal sheet enable the electron beams emitted from posterior gun to be focused, resulting in enhanced definition. Flattened and enlarged displays necessitate the imposition of pretension on the masks, in order to improve the robustness of display quality against vibration or impact. High temperature assembly process subsequent to pretensioning, however, degenerates creep resistance of mask material, and common mask may become susceptible to undesirable elongation due to creep. Once tensile stress becomes high enough to induce creep deformation, pretension is substantially loosened. In this study, tension mask assembly is modeled as a combined structure of beams and wire array, and a numerical simulation is attempted for pretensioning followed by high temperature process. Based on a model study, creep occurrence is found to be probable and its adverse influence is quantified. As fur maintaining high tensile force, simply increasing pretension does not seem to be helpful. Instead, the structure of frame needs to be modified somehow, or material for mask needs to be selected properly.

• Carbon letters
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• 제14권3호
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• pp.180-185
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• 2013

In this study, activated carbons nanofibers (ACNFs) were prepared from polyacrylonitrile-based nanofibers by physical ($H_2O$ and $CO_2$) and chemical (KOH) activation. The surface and structural characteristics of the porous carbon were observed by scanning electron microscopy and X-ray diffraction, respectively. Pore characteristics were investigated by $N_2$/77K adsorption isotherms. The specific surface area of the physically ACNFs was increased up to $2400m^2/g$ and the ACNFs were found to be mainly composed of micropore structures. Chemical activation using KOH produced ACNFs with high specific surface area (up to $2500m^2/g$), and the micropores were mainly found in the ACNFs. The physically and chemically ACNFs showed both mainly type I from the International Union of Pure and Applied Chemistry classification.