• 한국전기전자재료학회논문지
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• 제36권4호
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• pp.376-384
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• 2023

Nitrogen-doped graphene was synthesized by a hydrothermal method using graphene oxide (GO) as the raw material, urea as the reducing agent and nitrogen as the dopant. The morphology, structure, composition and electrochemical properties of the samples are characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), nitrogen adsorption-desorption analysis, electrical conductivity and electrochemical tests. The results show that urea can effectively reduce GO and achieve nitrogen doping under the hydrothermal conditions. By adjusting the mass ratio of raw materials to dopants, the graphene with different nitrogen doping contents can be obtained; the nitrogen content range is from 5.28~6.08% (atomic fraction percentage).When the ratio of dopant to urea is 1:30, the nitrogen doping content reaches a maximum of 6.08%.The supercapacitor performance test shows that the nitrogen content prepared by the ratio of 6.08% is the best at 0.1 A·g^-1. The specific capacitance is 95.2 F·g^-1.

• 한국주조공학회지
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• 제32권5호
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• pp.231-240
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• 2012

In present study, the effect of heat treatment on the microstructure and mechanical properties of the gravity cast superchargers housing using A356 alloy were investigated. In order to identify the characteristics of superchagers housing casting with heat treatment, Vickers hardness test, electrical conductivity test, opical and scanning electron microscopy were performed. And also, to investigate their mechanical properties, the T6 treated superchagers housing casting in optimum heat treatment condition were carried out tensile test using UTM (Universal Testing Machine).

• 대한전기학회:학술대회논문집
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• 대한전기학회 2005년도 추계학술대회 논문집 전기물성,응용부문
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• pp.96-99
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• 2005

In this study, we build system and techniques of evaluating the interruption performance of the GCB with experimental method. We constructed a simplified synthetic test circuit of which ability is up to 245kV, 50kA BTF test. And We composed a model test circuit breaker with puffer assisted self blasting type GCB. With this circuit breaker, we carried out the experiment of no load and SLF90. During the tests, we measured the several factors such as stroke, pressure, arc temperature, the voltage and current near the current zero and dI/dt, dV/dt. Arc conductivity before 200ns before current zero which is one of the indexes of the thermal recovery of a GCB was measured. With these kinds of measurement, we could estimate the performance of a GCB fundamentally. Futhermore these results were used to adjust the arc modeling with CFD(computational fluid dynamics) and we could increase the plausibility of the analytical method.

• Computers and Concrete
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• 제31권2호
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• pp.97-110
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• 2023

This study investigates experimentally the impact of magnetized water (MW) on the fresh and hardened characteristics of concrete. Five types of MW are produced using magnetic fields of 1.4 and 1.6 Tesla for treating water with 100, 150, and 250 cycles. The concrete properties are assessed using the slump test, compressive strength test, scanning electron microscopy (SEM) analysis, energy dispersive X-ray analysis (EDX), and Fourier transform infrared spectrophotometry (FTIR). Furthermore, the chemical-physical characteristics of tap water (TW) and MW are evaluated. The results showed the magnetic field intensity has a significant impact on the magnetization effect; the best magnetizing conditions were found when TW was exposed successively to magnetic fields of 1.6 T and 1.4 T for 150 cycles. In addition, 150 MW cycles can be used to improve the compressive strength and workability of concrete by 40% and 17%, respectively. pH, total dissolved solids, and electrical conductivity improved by 15%, 17%, and 7%, respectively, when using MW. Additionally, MW can be used to enhance cement hydration chemical processes and made concrete's structure denser.

• 한국작물학회지
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• 제40권1호
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• pp.77-85
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• 1995

벼, 옥수수, 보리, 밀, 콩, 팥, 배추, 무, 상추, 시금치, 고추, 토마토 등 12개 작물의 최근 성숙엽의 절편을 pH 3.0, 4.0, 5.0, 5.6의 인공산성비 용액에 1, 2, 3, 4시간 침지하여 침지용액의 pH 및 EC 변화와 침지 잎 절편의 변색정도를 조사하였다. 또 이 결과와 인공산성비에 대한 내성과의 상관관계와 침지용액의 pH 및 EC 변화와 잎에서 용출된 양이온과의 상관관계를 요약하면 다음과 같다 1. 잎 침지용액의 pH가 안정되고, 작물간 차이가 현저한 것은 pH 4.0 인공산성비 용액에 I~4시간 침지하였을 때이며, 침지용액의 pH는 용액의 Ca및 Mg 함량과 정의 상관이 있었으나 K 및 Na 함량과는 상관이 없었다. 2. 잎 침지용액의 EC가 안정되고, 작물간 차이가 현저한 것은 pH 5.0인공산성비 용액에 1∼4시간 침지하였을 때이며, 침지용액의 EC는 용액의 K, Ca, Mg 함량과 정의 상관이 있었으나 Na 함량과는 상관이 없었다. 3. 침지용 인공산성비의 pH가 3.0 이상일 때는 침지 후 4시간까지 엽색이 변하지 않았으며, pH 2.0에서는 작물과 침지시 간에 따라 엽색이 변하는 정도가 달랐다. 4. 포장에서 인공산성비에 의한 잎 피해정도와 잎 절편 침지용액의 pH와는 정의 상관이 있었으나 EC 및 잎 절편의 색깔 변화와는 상관이 없었다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1996년도 하계학술대회 논문집 C
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• pp.1719-1721
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• 1996

This paper describes the thermally stimulated current(TSC) of PAAS spin coated film and the electrical properties of pre TSC measurement and after TSC test specimens. The TSC measurement were performed from room temperature to about $280^{\circ}C$ and the temperature was increased by $5^{\circ}C/min$ automatically. It shows that two peaks of TSC are observed at about $50^{\circ}C$ and about $160^{\circ}C$. Result of this measurement indicate that one peak; $50^{\circ}C$ is from alkyl group; other peak at $160^{\circ}C$ is due to alkyl and C-O group of PAAS. Addition to larger peak at about $160^{\circ}C$ is due to dipolemoment of PAAS film. This result is proved by DSC measurement of PAAS film. The electrical properties of pre and after TSC were measured by currant-voltage(l-V) characteristics. The current-voltage characteristics after TSC specimens are increased the conductivity. The electrical properties of pre-after TSC measurement specimen is in the middle of imidization of PAAS. Because of this result a thermal imidization was performed at $300^{\circ}C$ for 1 hour.

• 한국수소및신에너지학회논문집
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• 제28권5호
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• pp.521-530
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• 2017

Improving the microstructure of NiO/YSZ is one of several approaches used to enhance the electrical and mechanical properties of an anode support in Solid Oxide Fuel Cells (SOFCs). The aim of the work reported in this paper was to predict the relationship between these microstructural changes and the resulting properties. To this end, modification of the anode microstructure was carried out using different sizes of Poly (Methyl Methacrylate) (PMMA) beads as a pore former. The electrical conductivity and mechanical strength of these samples were measured using four-probe DC, and three-point bend-test methods, respectively. Thermal etching followed by high resolution SEM imaging was performed for sintered samples to distinguish between the three phases (NiO, YSZ, and pores). Recently developed image analysis techniques were modified and used to calculate the porosity and the contiguity of different phases of the anode support. Image analysis results were verified by comparison with the porosity values determined from mercury porosimetry measurements. Contiguity of the three phases was then compared with data from electrical and mechanical measurements. A linear relationship was obtained between the contiguity data determined from image analysis, and the electrical and mechanical properties found experimentally. Based upon these relationships we can predict the electrical and mechanical properties of SOFC support from the SEM images.

• 한국초전도ㆍ저온공학회논문지
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• 제11권1호
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• pp.1-4
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• 2009

Mechanical and electrical properties of silver stabilizer layer of coated conductor, which as prepared with nano silver paste as starting materials, have been investigated, Nano silver paste was coated on a YBCO film by dip coating process at a diping speed of 20m/min. Coated film was dried in air and heat treated at $400{\sim}700^{\circ}C$ in an oxygen atmosphere. Adhesion strength between YBCO and silver layer was measured by a tape est(ASTM D 3359). Hardness and electrical conductivity of the samples were measured by pencil hardness test (ASTM D 3363) and volume resistance test by LORESTA-GP (MITSHUBISHD, respectively. The sample heat-treated at $500^{\circ}C$ showed poor adhesion 1B, but samples heat treated at higher than $600^{\circ}C$ showed enhanced adhesion of 5B. The silver layer heat-treated at $700^{\circ}C$ showed the high hardness value larger than 9 H, low volume resistance, surface resistance value as well as superior current carrying capacity compared to sputtered silver. SEM observations showed that a dense silver layer was formed with a thickness of about $2{\mu}m$. Dip coated silver layer prepared by using nano silver paste showed superior electrical and mechanical characteristics.

• 한국지반공학회:학술대회논문집
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• 한국지반공학회 2008년도 춘계 학술발표회 초청강연 및 논문집
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• pp.435-441
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• 2008

More time is required for consolidating soft clay when its hydraulic conductivity around the vertical drains is reduced by soil disturbance. One of the methods to be proposed to solve such problem is the electro-osmotic flow application. This study presents the experimental results of model tests using a modified oedometer and a large-scale cylinder with a sand drain. Results show that the development of negative excessive pore water pressure due to the DC electrical field in saturated clay can be transformed to additional loads causing more consolidation settlement.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2002년도 추계학술대회 논문집
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• pp.151-154
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• 2002

In this paper a mathematical model, the results of computer simulation and exprimental investigations of electrochemical machining with a too-electrode are presented. The experimental investigations were carried out in order to evaluate the influence of working voltage, initial interelectrode gap size, and metal remove rate. Accuracy of computer simulation evaluated by differences between results of experimental test and computer simulation depends on electrochemical machining coefficient, total overpotential of electrode process, current density, electrical conductivity of electrolyte, and etc. Metal removal rate would be predicted by the simulation of ECM process.