• 제목/요약/키워드: effect of heat treatment

검색결과 2,442건 처리시간 0.035초

Effect analysis in Laser Metal Deposition of SKD61 using AISI M2 power (AISI M2 파우더를 이용한 SKD61 재질의 레이저 메탈 디포지션 기초 특성 분석)

  • Kim, Won-Hyuck;Jung, Byung-Hun;Oh, Myeong-Hwan;Choi, Seong-Won;Kang, Dae-Min
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • 제14권3호
    • /
    • pp.50-56
    • /
    • 2015
  • In this study, AISI M2 powder was selected primarily through various pieces of literature in order to improve the hardness and wear resistance. Among the laser metal deposition parameters, laser power was studied to improve the deposition efficiency in the laser metal deposition using a diode-pumped disk laser. An SKD61 hot work steel plate and AISI M2 powder were used as a substrate and powder for laser metal deposition, respectively. Experiments for the laser metal deposition were carried out by changing the laser power and track layer. The quality of the track surface and cross-section after applying the single-layer method was better than that obtained from applying the multi-layer method. As the laser power increased, the track thickness was increased, and the surface roughness deviation was decreased. In laser power condition of 1.6kW, the maximum hardness of the deposition track was 790Hv. This value was 40% better than the hardness of the SKD61 after heat treatment.

Parameters to Affect the Cirtical Characteristics of YBaCuO Bulk Prepared by MPMG (MPMG법을 이용한 YBaCuO 초전도체의 임계특성에 영향을 미치는 파라미터)

  • Gang, Hyeong-Gon;Im, Seong-Hun;Park, Seong-Jin;Han, Byeong-Seong
    • The Transactions of the Korean Institute of Electrical Engineers C
    • /
    • 제48권4호
    • /
    • pp.221-225
    • /
    • 1999
  • This paper shows the parameters to affect the critical characteristic of YBaCuO superconducting bulk fabricated by MPMG (Melt Powdered Melt Growth)process. In order to investigate proper processing variables, the effect of the holding time at the melting temperature and that of the slow cooling time in $O_2\; ambient\; on\; the\; J_c$ were experimented. And then with the above obtained heat treatment conditions, the effects of addition of $Y_2BaCuO_5\; and\; Ag\; on\; the\; J_c$ were also investigated. A proper slow cooling time yields phase transformation from Tetragonal $(YBa_2Cu_3O_6)$ to Orthorhombic $(YBa_2Cu_3O_7)$ during an annealing time in $O_2$. Ag addition plays a role in increasing the $T_c\; and\; the J_c$, but the magnetization decreases. The $J_c$ and the magnetization increase with addition of Y211. $J_c$ of the sample added Ag 10wt% is superiorover 3000 G. Proper holding time, slow cooling time and amount of impurity addition are important parameters in fabricating the YBaCuO bulk by MPMG process with high $J_c$.

  • PDF

A Case Report of an Adult Atopic Dermatitis Patient Whose Eczema and SCORAD Index Were Improved by Herbal Medicine and Acupuncture Therapy (한약 및 침치료 후 피부습진의 SCORAD 점수를 호전시킨 성인 아토피성 피부염 환자 증례보고)

  • Hong, Seungcheol;Kim, Youngji;Song, Juyeon;Park, Song-won;Yi, Chan-sol;Jeong, Ji-cheon
    • The Journal of Internal Korean Medicine
    • /
    • 제39권5호
    • /
    • pp.1004-1014
    • /
    • 2018
  • This case reports the effect of herbal medicine and acupuncture therapy on the scoring atopic dermatitis (SCORAD) index for an adult atopic dermatitis patient. An adult male in his 30s with complaints of severe eczema on the whole body was diagnosed with heat toxin blazing exuberance pattern (熱毒內蘊) and treated with herbal medicine, including an orally-administrated decoction, externally-applied decoction, extracted powder capsule, and acupuncture for a total of 30 days. We observed skin symptoms, SCORAD index, follow-up photographs, and any adverse events. After treatment, SCORAD index decreased from 74.5 to 38.7 (51.9% from baseline). Skin symptoms such as redness, itching, and exudation were improved without any adverse events reported. This case suggests that herbal medicine and acupuncture therapy could be effective in improving eczema in adult atopic dermatitis patients.

Growth and Effect of Thermal Annealing for ZnIn2S4 Single Crystal Thin Film by Hot Wall Epitaxy (Hot Wall Epitaxy (HWE)법에 의한 ZnIn2S4 단결정 박막 성장과 열처리 효과)

  • Park, Chang-Sun;Hong, Kwang-Joon
    • Korean Journal of Materials Research
    • /
    • 제18권6호
    • /
    • pp.318-325
    • /
    • 2008
  • Single crystal $ZnIn_2S_4$ layers were grown on thoroughly etched semi-insulating GaAs(100) substrate at $450^{\circ}C$ with hot wall epitaxy (HWE) system by evaporating $ZnIn_2S_4$ source at $610^{\circ}C$. The crystalline structure of the single crystal thin films was investigated by the photoluminescence (PL) and double crystal X-ray rocking curve (DCRC). The temperature dependence of the energy band gap of the $ZnIn_2S_4$ obtained from the absorption spectra was well described by the Varshni's relation, $E_g(T)=2.9514\;eV-(7.24{\times}10^{-4}\;eV/K)T^2/(T+489\;K)$. After the as-grown $ZnIn_2S_4$ single crystal thin films were annealed in Zn-, S-, and In-atmospheres, the origin of point defects of $ZnIn_2S_4$ single crystal thin films has been investigated by the photoluminescence (PL) at 10 K. The native defects of $V_{Zn}$, $V_S$, $Zn_{int}$, and $S_{int}$ obtained by PL measurements were classified as a donors or acceptors type. And we concluded that the heat-treatment in the S-atmosphere converted $ZnIn_2S_4$ single crystal thin films to an optical p-type. Also, we confirmed that In in $ZnIn_2S_4$/GaAs did not form the native defects because In in $ZnIn_2S_4$ single crystal thin films existed in the form of stable bonds.

Development of Humidity Sensor Based on Ceramic/Metal Halide Composite Films for Non-Contact Biological Signal Monitoring Applications (비접촉 생체신호 모니터링 응용을 위한 세라믹/메탈 할라이드 복합막 기반 습도센서 개발)

  • Park, Tae-Ung;Kim, Ik-Soo;Kim, Min-Ji;Park, Chulhwan;Seo, Eui-kyoung;Oh, Jong-Min
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • 제35권4호
    • /
    • pp.412-417
    • /
    • 2022
  • Capacitive-type humidity sensors with a high sensitivity and fast response/recovery times have attracted a great attention in non-contact respiration biological signal monitoring applications. However, complicated fabrication processes involving high-temperature heat treatment for the hygroscopic film is essential in the conventional ceramic-based humidity sensors. In this study, a non-toxic ceramic/metal halide (BaTiO3(BT)/NaCl) humidity sensor was prepared at room temperature using a solvent-free aerosol deposition process (AD) without any additional process. Currently prepared BT/NaCl humidity sensor shows an excellent sensitivity (245 pF/RH%) and superior response/recovery times (3s/4s) due to the NaCl ionization effect resulting in an immense interfacial polarization. Furthermore, the non-contact respiration signal variation using the BT/NaCl sensor was determined to be over 700% by maintaining the distance of 20 cm between the individual and the sensor. Through the AD-fabricated sensor in this study, we expect to develop a non-contact biological signal monitoring system that can be applied to various fields such as respiratory disease detection and management, infant respiratory signal observation, and touchless skin moisture sensing button.

Fabrication of ZrB2-based Composites for Ultra-high Temperature Materials (초고온 소재용 ZrB2계 복합소재의 제조)

  • Kim, Seong-Won;Chae, Jung-Min;Lee, Sung-Min;Oh, Yoon-Suk;Kim, Hyung-Tae;Nahm, Sahn
    • Journal of Powder Materials
    • /
    • 제16권6호
    • /
    • pp.442-448
    • /
    • 2009
  • $ZrB_2$-based composites are candidate materials for ultra-high temperature materials (UHTMs). $ZrB_2$ has become an indispensable ingredient in UHTMs, due to its high melting temperature, relatively low density, and excellent resistance to thermal shock or oxidation. $ZrB_2$ powders are usually synthesized by solid state reactions such as carbothermal, borothermal, or combined carbothermal reaction. SiC is added to this system in order to enhance the oxidation resistance of $ZrB_2$. In this study, $ZrB_2$?based composites were successfully synthesized and densified through two different processing paths. $ZrB_2$ or $ZrB_2$ 25 vol.%SiC was fully synthesized from oxide starting materials with reducing agents after heat treatment at 1400$^{\circ}C$. Besides, $ZrB_2$?20 vol.%SiC was fully densified with $B_4C$ as a sintering additive after hot pressing at 1900$^{\circ}C$. The synthesis mechanism and the effect of sintering additives on densification of $ZrB_2$ ?SiC composites were also discussed.

The Effect of Grain Size and Cooling Rate on Phase Transformation for Mechanically Alloyed Ni-36at.%Al Alloy (기계적 합금화된 Ni-36at.%Al 합금의 상변태에 미치는 결정립 크기 및 냉각속도의 영향)

  • Kim, Seong-Uk;Kim, Dae-Geon;Kim, Ji-Sun;An, In-Seop;Kim, Yeong-Do
    • Korean Journal of Materials Research
    • /
    • 제10권9호
    • /
    • pp.642-647
    • /
    • 2000
  • Nanocrystalline NiAl alloy containing 36at.%Al was synthesized by mechanical alloying (MA). Synthesized powder was sintered by a pulse electric current sintering (PECS) facility. Effecting parameters on the phase transformation were discussed in terms of cooling rate and time spent on heat treatment. The behavior of phase transformation for sintered parts was examined by differential scanning calorimetry (DSC) and X-ray diffraction (XRD) method. Microstructure was observed by scanning electron microscopy (SEM). Martensitic lattice parameter and volume fraction was calculated by direct comparison method in X-ray diffraction analysis.

  • PDF

Effect of processing method on quality characteristics of gluten-free rice cookies containing legume flours (두류가 첨가된 글루텐-프리 쌀쿠키의 품질 특성에 가공방법이 미치는 영향)

  • Kim, Yuyeon;Jeong, Duyun;Chung, Hyun-Jung
    • Korean Journal of Food Science and Technology
    • /
    • 제50권5호
    • /
    • pp.504-510
    • /
    • 2018
  • Different processing methods, including steeping, boiling, roasting, and pressure roasting were used to deactivate anti-nutritional factors and remove off-flavor present in legumes. The physical and textural characteristic of cookie made with the treated flours were examined. The lightness of roasted cowpea flour was higher than that of the other treated legume flours, whereas that of pressure-roasted mungbean flour was the lowest. The boiled and pressure-roasted legume flours exhibited substantially lower pasting viscosity since the starches in these flours were considerably gelatinized during the heat treatment. Steeped mungbean flour had a significantly higher final viscosity than the other treated legume flours. Cookies containing mungbean flour had a higher protein content but lower lipid content than those containing cowpea flour. Cookies made with cowpea flour had a greater hardness than those made with mungbean flour. Cookies containing roasted flour had relatively better color properties than did those containing flours that were treated using other methods.

Experimental and numerical investigations on axial crushing of square cross-sections tube with vertical wave

  • Eyvazian, Arameh;Eltai, Elsadig;Musharavati, Farayi;Taghipoor, Hossein;Sebaey, T.A.;Talebizadehsardari, Pouyan
    • Steel and Composite Structures
    • /
    • 제36권2호
    • /
    • pp.119-141
    • /
    • 2020
  • In this paper, wavy square absorbers were experimentally and numerically investigated. Numerical simulations were performed with LS-Dyna software on 36 wavy absorbers and their crushing properties were extracted and compared with the simple one. The effect of different parameters, including wave height, wave depth, and wave type; either internal or external on the crushing characteristics were also investigated. To experimentally create corrugation to validate the numerical results, a set of steel mandrel and matrix along with press machines were used. Since the initial specimens were brittle, they were subjected to heat treatment and annealing to gain the required ductility for forming with mandrel and matrix. The annealing of aluminum shells resulted in a 76%increase in ultimate strain and a 60% and 56% decrease in yield and ultimate stresses, respectively. The results showed that with increasing half-wave height in wavy square absorbers, the maximum force was first reduced and then increased. It was also found that in the specimen with constant diameter and half-wave depth, an increment in the half-wave height led to an initial increase in efficiency, followed by a decline. According to the conducted investigations, the lowe maximum force can be observed in the specimen with zero half-wave depth as compared to those having a depth of 1 cm.

Cold Isostatic Pressing and Sintering Behavior of (Al +12.5%Cu)3Zr Nanocrystalline Intermetallic Compound Synthesized by Mechanical Alloying (기계적합금화한 (Al +12.5%Cu)3Zr 초미립 금속간화합물의 CIP 성형 및 소결 거동)

  • Moon, H.G.;Hong, K.T.;Kim, S.J.
    • Korean Journal of Materials Research
    • /
    • 제12권8호
    • /
    • pp.634-640
    • /
    • 2002
  • To improve the ductility of mTEX>$(Al +12.5%Cu)<_3$Zr intermetallics, which are the potential high temperature structural materials, the mechanical alloying behavior, the effect of pressure and temperature on the $Ll_2$, phase formation and the behavior of the cold isostatic press and sintering were investigated. However mechanically alloyed A1$_3$Zr alloy have been known to have high mechanical strength even at high temperature, its workability was poor. A method of solution is refined grain size and phase transformation from $DO_{23}$ to $Ll_2$.$ Ll_2$ structure TEX>$(Al+12.5%Cu)<_3$Zr with nanocrystalline microstructure intermetallic powders where were prepared by mechanical alloying of elemental powders. Grain sizes of the as milled powders were less than 10nm (from transmission electron microscopy, TEM). Thermal analyses showed that $Ll_2$ structure was stable up to$ 800^{\circ}C$ for 1hour $(Al+ 12.5%Cu)<_3$Zr. $(Al+12.5%Cu)<_3$Zr has been consolidated by cold isostatic pressing (CIP 138, 207, 276, 414MPa) at room temperature and subsequent heat treatment at high temperatures where $Ll_2$ structure was stable under vacuum atmosphere. The results showed that 94.2% density of Ll$_2$ compacts was obtained for the (Al +12.5%Cu)$_3$Zr by sintering at 80$0^{\circ}C$ for 1hour (under CIPed 207MPa). This compact of the grain size was 40nm.