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AN IN VITRO STUDY OF MICROLEAKAGE OF COMPOSITE RESINS (복합레진의 미세누출에 관한 연구)

  • Lee, Sun-Young;Yang, Yeon-Mi;Baik, Byeong-Ju;Jeon, Cheol-Wan;Kim, Jae-Gon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.30 no.4
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    • pp.593-599
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    • 2003
  • The purposes of this study were to evaluate the microleakage of class V composite resin restorations utilizing the different curing lights, to assess the flowable resin, $Filtek^{TM}Flow$(3M Dental Products, USA) and composite resin, $Filtek^{TM}Z250$(3M Dental Products, USA) which need 20s curing time for halogen light could replace $Z100^{TM}$ Restorative(3M Dental Products, USA) for the microleakage, and to evaluate the effect of adhesive resin on marginal microleakage. Light curing units used in this study were conventional halogen light, XL3000(3M Dental Products, USA) and plasma arc light, Flipo(Lokki, France). Class V cavities were prepared and each cavity was filled with each composite resin. After being filled, the teeth were stored in distilled water, polished, thermocycled and soaked in 1% methylene blue solution. Following results were obtained from evaluation of the sectioned surface. 1. There was no statistically significant difference in microleakage of $Filtek^{TM}Flow$ and $Filk^{TM}Z250$ between two kinds of curing units(p>0.05). 2. Flowable resin, $Filtek^{TM}Flow$ showed more microleakage than Z100 and $Filtek^{TM}Z250$ regardless of curing units(p<0.05). 3. Adhesive resin reduced the microleakage of composite resin in both halogen light and plasma arc light(p<0.05).

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AN EVALUATION OF WEAR CHARACTERISTICS OF LIGHT-CURED RESTORATIVE COMPOSITES ON ENAMEL SURFACE (광중합형 복합레진과 법랑질간의 마모특성 평가)

  • Baik, Byeong-Ju;Lee, Seung-Young;Lee, Doo-Cheol;Kim, Jae-Gon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.28 no.2
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    • pp.261-270
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    • 2001
  • This study was performed to evaluate wear characteristics of light-cured composites when opposed by human enamel. Seven light-cured restorative composites were selected and enamel cusps sectioned from premolars. All samples were stored in distilled water at $37^{\circ}C$ for 10 days. 68.6 N of weight was loaded during the test. The measurements of vertical loss of enamel cusps, weight loss and volume loss of composites, and SEM observations of the polished and abraded surfaces were made after 30,000 cycles. The results obtained were summarized as follows; 1. The highest hardness value of 70.4 was observed in the Spectrum group and the lowest value of 19.8 was observed in the Heliomolar group. Results of Tukey test showed that an overall significant difference was indicated except the Spectrum, Z100 and Clearfil AP-X groups(p<0.05). 2. Enamel showed the good abrasion resistance against the Heliomolar group of microfilled composite and the Palpique Toughwell group containing the submicron hybrid type spherical fillers. 3. The abrasive wear resistance of hybrid composites was improved with the decrease of mean particle size and hybrid of submicron particle fillers. 4. SEM observation of worn surfaces revealed the protrusion, attrition and missing of fillers, cracks developing and delamination in the matrix.

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Quality Characteristics of Brown Sauce Made with Freeze-dried Salicornia herbacea L. Powder (함초를 이용한 브라운소스에 관한 품질특성)

  • Kim, Ja-Kyoung;Yoo, Seung-Seok
    • Culinary science and hospitality research
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    • v.18 no.5
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    • pp.243-255
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    • 2012
  • This research has been conducted to develop the best recipe for brown sauce containing freeze-dried Salicornia powder. For this purpose, we made brown sauces with different contents of freeze-dried Salicornia powder and performed physico-chemical characteristic and sensory test. The highest salinity of freeze-dried Salicornia powder was 0.15% when 1% freeze-dried Salicornia powder was added to distilled water, SP1. The highest brightness of brown sauce was achieved with 1.2% freeze-dried Salicornia powder and was 45.29 with BSP12. More powder led to significant increases of the samples(p<0.001) in salinity and brightness. DPPH radical scavenging increased with greater freeze-dried Salicornia powder. Taste was highest at 6.36 with 0.6% powder and there was no significant difference compared to BSP6 and BSP9. Based on these findings, it was concluded that the brown sauce with Salicornia has antioxidative characteristics and the best salinity is achieved with 0.6% freeze-dried Salicornia powder. Salicornia had enough salinity to substitute salt to a certain degree and improved the quality of brown sauce in terms of the sensory test.

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Effect of Provisional Restorative and Filling Materials on Bond Strength of Adhesive Resin Cement between Lithium Disilicate Glass-Ceramic and Dentin (Lithium Disilicate Glass-ceramic과 상아질 간의 접착성 레진 시멘트의 결합강도에 대한 임시 수복재와 임시 충전재의 영향)

  • Oh, Sang-Chun;Sim, Hun-Bo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.29 no.4
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    • pp.359-365
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    • 2013
  • The aim of this study was to evaluate the effect of temporary restorative and filling material on bonding strength between lithium disilicate glass-ceramic and dentin. 60 extracted human molars were cross-sectioned at occlusal third and were embedded into self-cure acrylic resin. Then the teeth were randomly divided into four groups of 15 each. Lithium disilicate glass-ceramic is cemented to dentin as follows: after no any application of the provisional materials (Group A), after application of ALIKETM (GC America Inc.)(Group B), after application of Luxatemp$^{(R)}$ Automix plus (DMG, Germany)(Group C), after application of Fermit$^{(R)}$ (Ivoclar Vivadent, Leichtenstein)(Group D). After the specimens were stored in distilled water for 24 hours, the shear bond strength of the specimens were measured using UTM (Zwick 1456 41, Zwick, Germany) at a crosshead speed of 1mm/min. The data were analysed by one-way ANOVA and Tukey HSD tests. There were no statistically significant differences of bond strength among the groups. Fracture type was showed mixed type of adhesive and cohesive fracture in most of specimens. Within the limitation of this study, bond strength of adhesive resin cement between lithium disilicate glass-ceramic and dentin was not affected by provisional restorative and filling materials.

Functional Properties of Mungbean Protein Isolates (분리녹두단백의 식품기능적 특성에 관한 연구)

  • Kye, In-Sug;Jun, Yeong-Soo;Cheigh, Hong-Sik
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.18 no.3
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    • pp.300-306
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    • 1989
  • This study was investigated to determine the functional properties of mugbean protein isolates(MPI) from sunhwa-nogdu(SH) and conventional mungbean varieties(C). MPI were prepared from defatted mungbean flour by extraction with 0.1N NaOH, precipitation at pH 4.5, washing of dispersed precipitate with buffer solution and distilled water, and subsequent freeze-drying. Crude protein content of MPI was in the range of $88.7{\sim}91.3%$. The lowest solubility was recorded at $pH\;4{\sim}5$, whereas the best buffering action was in the range of $5.5{\sim}7.5$. On the other hand, gelation of MPI was found to depend on the protein concentration. In the cases of foamability, % volume increase and specific volume were higher for 10 min. with a good whipping ability. And also, the MPI properties of two varieties of SH and C were compared and discussed.

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A Study on pH Reduction of Recycled Aggregates Using Coffee Waste and Its Crushability (커피박을 이용한 순환골재의 pH 저감 및 파쇄성 연구)

  • Lee, Young-Jae;Lee, Dong-Yun;Chen, KeQiang;Kim, Moon-Gi;Park, Sung-Sik
    • Journal of the Korean Geotechnical Society
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    • v.32 no.11
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    • pp.21-29
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    • 2016
  • In this study, recycled aggregates crushed from waste concrete were sorted into three groups, 10-13 mm, 13-20 mm, and 20-25 mm. They were treated in different ways and then their crushability was evaluated for each treatment. Coffee waste was used for reducing their pH level. The pH of recycled aggregate was almost 11, regardless of aggregate sizes. The pH of coffee waste was nearly 5 and 10, 30, or 50 g of coffee waste was mixed with 1000 ml of distilled water and recycled aggregates. The lowest pH was about 6.2 when 50 g of coffee waste was mixed. Aggregates were treated with microwave or soaked for 1 day in vinegar (pH = 2) for neutralization reaction. Microwave treated and neutralized aggregates showed 3.3% and 6.2% higher crushing values compared to non-treated one, respectively. Neutralized treatment was more effective for crushing. In crushing tests, a sample height of 120 mm was tried, which gave 6.3% higher crushing value. A four stepped loading with each 100 kN gave 7.1% higher crushing value, compared to standard 100 mm height and 400 kN continuous loading.

Preparation of Chitosan/Poly-${\gamma}$-glutamic Acid Nanoparticles and Their Application to Removal of Heavy Metals (키토산/폴리감마글루탐산 나노입자의 제조 및 중금속 제거에의 응용)

  • Sung, Ik-Kyoung;Song, Jae Yong;Kim, Beom Soo
    • Korean Chemical Engineering Research
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    • v.49 no.4
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    • pp.475-479
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    • 2011
  • Chitosan is a natural polymer that has many physicochemical(polycationic, reactive OH and $NH_2$ groups) and biological(bioactive, biocompatible, and biodegradable) properties. In this study, chitosan nanoparticles were prepared using poly-${\gamma}$-glutamic acid(${\gamma}$-PGA) as gelling agent. Nanoparticles were formed by ionic interaction between carboxylic groups in ${\gamma}$-PGA and amino groups in chitosan. Chitosan(0.1~1 g) was dissolved in 100 ml of acetic acid (1% v/v) at room temperature and stirred overnight to ensure a complete solubility. An amount of 0.1 g of ${\gamma}$-PGA was dissolved in 90 ml of distilled water at room temperature. Chitosan solution was dropped through needle into beaker containing ${\gamma}$-PGA solution under gentle stirring at room temperature. The average particle sizes were in the range of 80~300 nm. The prepared chitosan/${\gamma}$-PGA nanoparticles were used to examine their removal of several heavy metal ions($Cd^{2+}$, $Pb^{2+}$, $Zn^{2+}$, $Cu^{2+}$, and $Ni^{2+}$) as adsorbents in aqueous solution. The heavy metal removal capacity of the nanoparticles was in the order of $Cu^{2+}$ > $Pb^{2+}$ > $Cd^{2+}$ > $Ni^{2+}$ > $Zn^{2+}$.

Chloride Penetration Properties of Portland Cement Mortar Substituted with Anion Exchange Resin Powder (음이온교환수지 분말이 치환된 포틀랜드 시멘트 모르타르의 염소이온 침투 특성)

  • Lee, Yun-Su;Lim, Seung-Min;Park, Jang-Hyun;Jung, Do-Hyun;Lee, Han-Seung
    • Journal of the Korea Institute of Building Construction
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    • v.20 no.1
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    • pp.1-9
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    • 2020
  • Chloride ion, which penetrates into the cement composites from the outside, generally diffuses by the concentration gradient. Chloride ions are adsorbed by the chemical reaction with cement hydrates. Recent studies have shown that anion exchange resin (AER) powder can effectively adsorb the chloride ion in the cement composites, and thus, the cement composites containing AER have a high chloride adsorption capacity and a good resistance for chloride penetration. In this study, the chloride adsorption ability of the AER powder was investigated under the conditions of distilled water and calcium hydroxide saturated solution to determine if the AER powder is less effective to increase the chloride adsorption ability after grinding process. The chloride adsorption ability of AER powder was compared with the previous research about the chloride adsorption of AER bead. In addition, the compressive strength, chloride diffusion coefficient (using NT Build 492 method), and the chloride profile of cement mortar substituted with AER powder were investigated. There was no decrease in the chloride adsorption capacity of AER powder but increase in the kinetic property for chloride adsorption after the grinding process. The AER powder could absorb the chloride ion in the mortar quickly, and showed better chloride ion adsorption ability than the cement hydrates.

Effect of Fiber Type and Combination on the Reinforcement of Heat Polymerized Denture Base Resin (섬유의 종류와 조합이 열중합 의치상 레진의 강화에 미치는 영향)

  • Yu, Sang-Hui;Kim, Young-Im
    • Journal of dental hygiene science
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    • v.10 no.6
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    • pp.445-450
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    • 2010
  • The aim of this study was to evaluate the effect according to the fiber type and combination on the reinforcement of heat-polymerized denture base resin. The heat-polymerized resin(Vertex RS, Dentimax, Netherlands) was used in this study. Glass fiber(GL; ER 270FW, Hankuk Fiber Glass, Korea), polyaromatic polyamide fiber(PA; aramid; Kevlar-49, Dupont, U.S.A.) and ultra high molecular weight polyethylene fiber(PE, polyethylene; P.E, Dong Yang Rope, Korea) were used to reinforce the denture base resin specimens. The final size of test specimen was $64mm{\times}10mm{\times}3.3mm$. The specimens of each group were stored in distilled water at $37^{\circ}C$ for 50 hours before measurement. The flexural strength and flexural modulus were measured by an universal testing machine(Z020, Zwick, Germany) at a crosshead speed of 5 mm/min in a three-point bending mode. In this study, all fibers showed reinforcing effects on denture base resin(p<0.05). In terms of flexural strength and flexural modulus, glass fiber 5.3 vol.% showed most effective reinforcing effect on heat polymerized denture base resin. For flexural modulus, PA/GL was the highest in denture base resin specimen for hybrid FRC using two combination (p<0.05). Glass fiber 5.3 vol.% and PA/GL are considered to be applied effectively in reinforcing the heat polymerized denture base resin.

Effect of Fluoridated Bleaching Agents and Post-treatment Fluoride Application on the Color and Microhardness of Enamel Surface (불소를 함유한 치아미백제가 치아 표면의 색과 미세경도에 미치는 영향)

  • Shim, Youn-Soo;Jung, Sang-Hee
    • Journal of dental hygiene science
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    • v.10 no.4
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    • pp.295-300
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    • 2010
  • The aim of this study were to elucidate effects of fluoridated bleaching agents and post-treatment fluoride application on the color and microhardness of enamel surface. Twenty freshly extracted human adult molar were each sectioned into halves, the specimens divided and treated according to four experimental groups: 1, untreated controls: 2, treatment with 10% carbamide peroxide (CP) bleaching agent; 3, treatment with 10% CP containing 0.11% fluoride; 4, treatment with 10% CP followed by a 0.9% sodium fluoride gel application. Group 2-4 were compared with the baseline data. treated 8 h per day for 14 days then immersed in distilled water for 2 weeks. Changes in enamel color and microhardness were evaluated on Days 7 and 14. All the bleached enamel specimens revealed increased whiteness and overall color value. Groups 2 and 4 showed significantly decreased enamel microhardness compared to their baseline. The specimens treated with fluoridated bleaching agents showed relatively less reduction in enamel microhardness than those treated with nonfluoridated agents during the bleaching treatment. The addition of fluoride did not impede the tooth whitening. The fluoridated bleaching agents reduced the microhardness loss of enamel.