• Journal of the Korean Home Economics Association
• /
• v.41 no.8
• /
• pp.55-62
• /
• 2003

Natural dyes generally fan into two categories; organic dyes coming from animals and plants and inorganic dyes obtained from various minerals such as bengala, loess, ultramarine, prussian blue and etc. The main components of volcanic ash is clay mineral such as kaolinite, illite, quartz. Clay minerals Composing volcanic ash are kaolinite［$Al_4Si_4O_{10}{(OH)_{8}}$］, illite［$K_{X}Al_2(Si,\;Al)_4O_{10}{(OH)}_2$］, quartz［$SiO_2$］, homblende［$Na_{0-1}\;Ca_2{(Mg,\;Fe,\;Al)}_5{(Si,\;Al)}_{8}O_{22}{(OH)}_2$］and etc. And the redish color mainly comes from iron oxide. In this paper, two different classes of dyeing process were tested; dyeing with volcanic ash only and cationic agent pre-treatment followed by dyeing with volcanic ash. The compositions of the volcanic ash powder and the volcanic ash deposited on the cotton knitted fabrics identified by energy dispersive spectrometer and XRD analysis. The major chemical components of volcanic ash deposited on the cotton knitted fabrics were confirmed to be the saicon oxide, iron oxide, and aluminum oxide and etc. According to the analysis by XRD and EDS-SEM, kaolinite, illite and quartz were also identified.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2004.10a
• /
• pp.272-277
• /
• 2004

The elastic waves in the plate are dispersive waves with the characteristics of Lamb waves. However, $S_0$ symmetric mode is less dispersive in the frequency region less than first cut-off frequency. And, in anisotropic plates such as CFRP plates, the propagation velocities vary with the direction. So, the wave vector direction to be the phase velocity direction is not accord with the energy flow direction to be the group velocity direction. In this work, the group velocities of the $S_0$ symmetric mode less than the first cut-off frequency was analyzed with the group velocity dispersion curves in unidirectional CFRP plate. And, the group velocity curve obtained by the group velocity dispersion curves are compared with the measured velocities as varied the propagation direction of the Lamb wave. The measured velocities are good agreement with the corrected group velocity curve except near the fiber direction which is called the cusp region. When the propagation direction is not accorded with the principal axis, the direction of the group velocities declines to the fiber direction in the unidirectional CFRP plates. This implies that the energy propagates preferentially toward fiber direction.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
• /
• 2003.04a
• /
• pp.79-85
• /
• 2003

One of unique characteristics of guided waves is a dispersive behavior that guided wave velocity changes with an excitation frequency and mode. In practical applications of guided wave techniques, it is very important to identify propagating modes in a time-domain waveform for determination of defect location and size. Mode identification can be done by measurement of group velocity in a time-domain waveform. Thus, it is preferred to generate a single or less dispersive mode But in many cases, it is difficult to distinguish a mode clearly in a time-domain waveform because of superposition of multi modes and mode conversion phenomena. Time-frequency analysis is used as efficient methods to identify modes by presenting wave energy distribution in a time-frequency. In this study, experimental guided wave mode identification is carried out in a steel plate using time-frequency analysis methods such as wavelet transform. The results are compared with theoretically calculated group velocity dispersion curves. The results are in good agreement with analytical predictions and show the effectiveness of using the wavelet transform method to identify and measure the amplitudes of individual guided wave modes.

• Proceedings of the Korean Vacuum Society Conference
• /
• 2014.02a
• /
• pp.318.1-318.1
• /
• 2014

Metal nano-crystals have been received much attentions owing to their excellent catalytic property and surface plasmon effect. In the last decade, many studies on synthesizing well-dispersive nanoparticles and on understanding their distinct physical properties have been performed. There were tremendous reports revealing the electrochemical activities and enhancement of surface plasmonic effect were dependent mainly on the size, shape, and composition. So far, most fabrication methods have been based on vacuum based deposition techniques, such as chemical vapor deposition and electron-beam evaporation, and then annealed them to transform into the nanoparticles. Recently, there were several reports regarding to the photoinduced nano-crystal synthesis as an effective way to produce the metal nanoparticles. In this study, we report synchrotron x-ray mediated synthesis of Au nanoparticles on ZnO nanowires. ZnO nanowires were fabricated by hydrothermal method, and then they were dip into a solution having Au clusters. Detailed structural evolution of Au nanoparticles was investigated using scanning electron microscopy and photoluminescence measurements. The results on formation of well-dispersive Au nanoparticles on ZnO nanowires will be presented.

• Journal of Welding and Joining
• /
• v.28 no.2
• /
• pp.74-78
• /
• 2010

In this paper, a non-contact method of evaluating the thickness reduction in an aluminum sheet caused by corrosion and friction using SH-EMAT (shear horizontal, electromagnetic acoustic transducer) is described. Since this method is based on the measurement of the time-of-flight and amplitude change of guided waves caused from the thickness reduction, it provides information on the thinning defects. Information was obtained on the changes of the various wave features, such as their time-of-flight and amplitude, and their correlations with the thickness reduction were investigated. The interesting features in the dispersive behavior of selected guided modes were used for the detection of thinning defects. The measurements of these features using SH waves were performed on aluminum specimens with regions thinned by 7.2% to 29.5% of the total thickness. It is shown that the time-of-flight measurement provides an estimation of the thickness reduction and length of the thinning defects.

• Journal of the Korean Vacuum Society
• /
• v.22 no.2
• /
• pp.105-110
• /
• 2013

Single crystalline $In_xGa_{1-x}As$ nanowires are grown on Si (111) substrate via Vapor-Liquid-Solid growth mode using metal-organic chemical vapor deposition. The ternary nanowires have been grown with various growth conditions and examined by electron microscopy. The alloy compositions of the nanowires has been investigated using Energy-dispersive X-ray spectroscopy. We have found that the composition gradient of the nanowire becomes larger with growth temperature and V/III ratio.

• Applied Chemistry for Engineering
• /
• v.25 no.6
• /
• pp.586-591
• /
• 2014

In this study, the diarylide compound pigment of high hiding power and vivid color was synthesized successfully by controlling several factors such as pH, coupler solution temperature, kind and addition amount of dispersion precursor, and crystallization temperature in the process of coupling synthesis. The properties of samples were measured by the means of FT-IR, UV-Vis spectroscopy, PSA, zeta potential, and turbiscan. It was found that the highly dispersive sample could be prepared by introducing the dispersive precursor.

• Applied Chemistry for Engineering
• /
• v.25 no.6
• /
• pp.645-647
• /
• 2014

We synthesized $TiO_2$ ($Ru_x/TiO_2$) incorporating $TiO_2$ and Ru via an one-step hydrothermal method. The physical properties were characterized by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS) and transmission electron microscopy (TEM). The prepared samples were applied as a catalyst for the oxidation of benzyl alcohol to benzaldehyde using molecular oxygen ($O_2$). Especially, the catalytic activities increased as the contents of ruthenium in $TiO_2$ increased without the formation of any byproducts.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
• /
• v.11 no.4
• /
• pp.565-574
• /
• 2000

A new ground penetrating radar imaging method for the estimation of buried artificial structures location and their approximate shapes in dispersive lossy ground is investigated. Fundamental idea is based on estimating delayed time and amplitude retrieval coefficients from scattered signals by buried scatterers. Using absolute value integration of each scanning site not only improve the accuracy of measured scattered signal, but also offers convenient ways to extract the image of buried structures. Multi-term Debye model was employed to describe a dispersive and lossy ground medium. We used the finite difference time domain method to discretize the wave equation in continuous form into the machine suitable form. This imaging method uses a new wave path tracing technique in time domain, which is helpful to identify the exact position of buried structures against the ground surface fluctuations.

• Korean Journal of Materials Research
• /
• v.17 no.8
• /
• pp.408-413
• /
• 2007

Process of the hydroxyapapite(HA) precipitation on bioactive titanium metal prepared by NaOH in a modified-simulated body fluid(mSBF) was investigated by high resolution transmission electron microscope (HRTEM) attached with energy dispersive X-ray spectrometer(EDX). The amorphous titanate phase on titanium surface is form by NaOH treatment and an amorphous titanate incorporated calcium and phosphate ions in the liquid to form an amorphous calcium phosphate. With increasing of soaking time in the liquid, the HA particles are observed in amorphous calcium phosphate phase with a Ca/P atomic ratio of I.30. The octacalcium phosphate (OCP) structure is not detected in HRTEM image and electron diffraction pattern. After a long soaking time, the HA particles grow as needle-like shape on titanium surface and a large particle-like aggregates of needle-like substance were observed to form on titanium surface within needle-like shape. A long axis of needle parallels to c-direction of the hexagonal HA structure.