• 제목/요약/키워드: dilatometer

검색결과 120건 처리시간 0.025초

수종복합레진의 경도측정에 관한 실험적 연구 (AN EXPERIMENTAL STUDY ON HARDNESS IN COMPOSITE RESINS)

  • 엄정문
    • Restorative Dentistry and Endodontics
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    • 제4권1호
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    • pp.35-38
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    • 1978
  • The purpose of this study was to measure micro-knoop hardness and coefficient of thermal expansion on composite resins (Epolite, Adaptic, Hipol and Compo T.) Four different type of composite resins were measured at the varying depth of 30, 60, 90, 150, 200, 400, 700 and 1000 micron from the surface to deep portion. The specimens were stored both in the air room temperature for 2 days, 30 days and in water at $37^{\circ}C$ for 30 days. Thermal expansions of specimens(4mm in diameter and 50mm in height) were measured in quartz tube dilatometer from $20^{\circ}$ to $70^{\circ}C$ The following results were obtained. 1. The hardness of superficial portion were lower than inner portion of resin. 2. The value of hardness obtained from the specimen stored in room temperature in the water at $37^{\circ}C$ for 30 days were lower than above described Cases. 3. The coefficient of thermal expansion of Adaptic had $29.75{\times}10^{-6}/^{\circ}C$, Hipol had $30{\times}10^{-6}/^{\circ}C$, Epolite had $39.85{\times}10^{-6}/^{\circ}C$ and Compo T had $36.95{\times}10^{-6}/^{\circ}C$.

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3원계 U-Ce-O의 소결 Kinetics 연구

  • 김형수;박춘호;배기광;정상태;최창범
    • 한국재료학회지
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    • 제3권3호
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    • pp.276-281
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    • 1993
  • 3원계 U-Ce-O산화물의 소결거동을 연구하기 위하여 $UO_2$$CeO_2$분말을 ball-mill 방법으로 혼합한 (U, Ce)$O_2$의 영향이고, 나중에 나타나는 극대점은 $CeO_2$의 영향 때문이다. 또한 $Ceo_{2}$함량이 증가할수록 소결이 지연됨을 알수 있었다. 동일한 10wt. % $CeO_2$함량에서, 4시간동안 ball-milling을 하였을때가 소결속도는 가장 빨랐다.

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시화호 주변 연약지반 피에조콘계수 산정에 관한 통계적 분석 (Evaluation of Piezocone Factors Applicable to Soft Ground Around Siwha Lake by Statistical Analysis)

  • 정진혁;박수범;이송
    • 한국지반공학회논문집
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    • 제24권4호
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    • pp.89-100
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    • 2008
  • 국외에서 개발한 상관식이나 도표 등을 활용하여 국내 지반특성을 반영함에 있어 이를 그대로 국내지반에 적용하는 데에는 한계가 있다. 따라서 국내에 적합한 피에조콘계수 활용을 위해서는 국내 지반에 대한 시험결과를 직접적으로 이용하여 피에조콘계수를 결정할 필요가 있다. 이에 본 연구에서는 서해안 시화호 주변에 광범위하게 분포하고 있는 연약지반을 대상으로 실내시험 및 현장시험을 수행한 결과를 피에조콘 관입시험과 비교 분석하고, 비배수전단강도와 콘 관입저항력과의 상관성 분석을 통하여 피에조콘계수를 산정하였다. 또한 산정된 결과의 신뢰성 확보를 위하여 통계분석 기법을 활용하여 연구대상 지역에 적합한 피에조콘계수를 재산정해 보았다.

Bearing capacity of a Flysch rock mass from the characterization of the laboratory physical properties and the Osterberg test

  • Hernan Patino;Ruben A. Galindo
    • Computers and Concrete
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    • 제33권5호
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    • pp.573-594
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    • 2024
  • This article presents a research study, with both laboratory and field tests, of a deep foundation in a markedly anisotropic medium. Particularly it has focused on the evaluation of the behavior of a pile, one meter in diameter, embedded in a rocky environment with difficult conditions, in the Flysch of the Spanish city of San Sebastián. To carry out the research, the site of a bridge over the Urumea River was chosen, which was supported by pre-excavated reinforced concrete piles. 4 borings were carried out, by the rotation and washing method, with continuous sampling and combined with flexible dilatometer tests. In the field, an Osterberg load test (O-cell) was performed, while in the laboratory, determinations of natural moisture, natural unit weight, uniaxial compressive strength (UCS), point load strength (PLS), compressive wave propagation velocity (Vc) and also triaxial and direct shear tests were carried out. The research results indicate the following: a) the empirical functions that correlate the UCS with the PLS are not always linear; b) for the studied Flysch it is possible to obtain empirical functions that correlate the UCS with the PLS and with the Vc; c) the bearing capacity of the studied Flysch is much greater than if it is evaluated by different load capacity theories; d) it is possible to propose an empirical function that allows evaluating the mobilized shear strength (τm), as a function of the UCS and the displacement relative of the pile (δr).

고체산화물 연료전지의 Samarium Oxide 혼합 공기극에 대한 열특성 분석 (Thermal Characteristics of Samarium-based Composite Cathode ($Sm_{0.5}Sr_{0.5}CoO_{3-\delta}/ Sm_{0.2}Ce_{0.8}O_{1.9}$) for Intermediate Temperature-operating Solid Oxide Fuel Cell)

  • 백승욱;배중면
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회B
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    • pp.2021-2025
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    • 2007
  • Performance of single cell at solid oxide fuel cell (SOFC) system is largely affected by electrocatalytic and thermal properties of cathode. Samarium-based perovskite oxide material is recently recognized as promising cathode material for intermediate temperature-operating SOFC due to its high electrocatalytic property. Perovskite structured $Sm_{0.5}Sr_{0.5}CoO_{3-\delta}$ and its composite material, $Sm_{0.5}Sr_{0.5}CoO_{3-\delta}/Sm_{0.2}Ce_{0.8}O_{1.9}$ were investigated in terms of area specific resistance (ASR), thermal expansion coefficient (TEC), thermal cycling and long term performance. $Sm_{0.2}Ce_{0.8}O_{1.9}$ was used as electrolyte material. Electrochemical ac impedance spectroscopy (EIS) and dilatometer were used to measure the cathodic properties. Composite cathode ($Sm_{0.5}Sr_{0.5}CoO_{3-\delta}$: $Sm_{0.2}Ce_{0.8}O_{1.9}$ = 6:4) showed a good ASR of 0.13${\Omega}$ $cm^2$ at 650$^{\circ}C$ and its TEC value was 12.3${\times}$10-6/K at 600$^{\circ}C$ which is similar to the value of ceria-based electrolyte of 11.9${\times}$10-6/K. Performance of composite cathode was maintained with no degradation even after 13 times thermal cycle test.

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장변위공내재하시험기를 이용한 철도교 기초의 P-y곡선에 관한 연구 (P-y Curves from Large Displacement Borehole Testmeter for Railway Bridge Foundation)

  • 류창열;이슬;김대상;조국환
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2011년도 정기총회 및 추계학술대회 논문집
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    • pp.836-842
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    • 2011
  • The lateral stability of bridge foundations against train moving load, emergency stopping load, earthquakes, and so on is very important for a railway bridge foundation. A borehole test is much more accurate than laboratory tests since it is possible to minimize the disturbance of ground conditions on the test site. The representative borehole test methods are Dilatometer, Pressuremeter and Lateral Load Tester, which usually provide force-resistance characteristics in elastic range. In order to estimate P-y curves using those methods, the non-linear characteristics of soil which is one of the most important characteristics of the soil cannot be obtained. Therefore, P-y curves are estimated usually using elastic modulus ($E_O$, $E_R$) of lateral pressure-deformation ratio obtained within the range of elastic behavior. Even though the pile foundation is designed using borehole tests in field to increase design accuracy, it is necessary to use a higher safety factor to improve the reliability of the design. A Large Displacement Borehole Testmeter(LDBT) is developed to measure nonlinear characteristics of the soil in this study. P-y curves can be directly achieved from the developed equipment. Comparisons between measured P-y curves the LDBT developed equipment, theoretical methods based on geotechnical investigations, and back-calculated P-y curves from field tests are shown in this paper. The research result shows that the measured P-y curves using LDBT can be properly matched with back-calculated P-y curves from filed tests by applying scale effects for sand and clay, respectively.

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도재소부전장금관용 Opaque 분말과 도재전장관용 core 분말의 물리화학적 성질 및 금속과의 결합력에 대한 비교연구 (A COMPARATIVE STUDY OF THE PHYSICOCHEMICAL PROPER TIES AND BOND STRENGTH TO METAL BETWEEN THE REGULAR OPAQUE POWDER AND CORE POWDER)

  • 임장섭;정창모;전영찬
    • 대한치과보철학회지
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    • 제35권1호
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    • pp.144-164
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    • 1997
  • The purpose of this study were to investigate the chemical composition, mean particle size, linear thermal expansion coefficient and metal-bonding strength of the regular opaque powder and core powder. In this study, 4 types of ceramic powders, namely Duceram Jacket Opaque powder, Duceram Opaque powder, Vita Hi-Ceram powder, Vita VMK Paint On-88 powder were used. Chemical composition was evaluated by EDS(Energy Dispersive X-ray Spectrophotometer, Oxford QX-2000, England), particle size was measured by MALVERN Instruments(MALVERN Instruments SB. OC., U.S.A.. ad linear thermal expansion coefficient was measured by dilatometer(Motoyama, Japan). Bond strength was measured by the Universal tsting machine(Istron Co., Ltd., U.S.A.). The Results were as follows : 1. Through recognition of the relative difference in chemical composition between the core powder and the regular opaque powder, the difference in the proportion of $Al_2O_3$ in each type of material is demonstrated ; Duceram Jaket Opaque powder : 30.16%, Duceram Opaque powder : 16.60%, Vita Hi-Ceram : 63.64%, Vita VMK Paint-On 88 : 16.16%. 2. There was no significant difference in the proportion of metal-bonding materials between the core powder and the regular opaque powder. 3. In the regular opaque powder, alkaline materials were incoporated in order to increase the coefficient of thermal expansion. 4. In the particle size analysis, there was no significant difference in mean particle size or in the particle size distribution between the core powder and the regular opaque powder. 5. In the thermal expansion test for temperature range of $25-600^{\circ}C$, the regular opaque powder had higher coefficient of thermal expansion than that of core powder. 6. In the 4 point flexural bending test, there was no statistically significant difference in the mean bond strength between the core powder and the opaque powder among the Duceram products.

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$CaO-P_2O_5-SiO_2$계 유리의 물성 (Properties of $CaO-P_2O_5-SiO_2$ Glasses)

  • 조정식;김철영
    • 한국세라믹학회지
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    • 제30권4호
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    • pp.289-298
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    • 1993
  • Properties in terms of the variation of the glass compositions, which were density (p), molar volume(Vm), atom/ion packing density (Dp), refractive index (nD), transformation temperature (Tg), dilatometric softening point (Td), thermal expansion coefficient (α), Young's modulus (E), and knoop hardness (KHN) were investigated in CaO-SiO2 glasses and CaO-P2O5-SiO2 glasses containing less than 10mole% of P2O5. Those properties were measured by density measurement kit, Abbe refractometer, dilatometer, ultrasonic pulse echo equipment, and micro hardness tester. When CaO content was increased in CaO-SiO2 glasses, p, Dp, nD, Tg, Td, α, E and KHN were increased, while Vm was decreased. When P2O5 was added to the CaO-SiO2 glasses with constant CaO/SiO2 ratio as 1.07, p, Dp, nD, Tg, Td, α, E and KHN were decreased, while Vm was increased. When the amount of P2O5 in glasses was kept constant, the changes of the properties with variation of CaO content in the CaO-P2O5-SiO2 glasses were very similar to those of CaO-SiO2 glasses. These phenomena could be explained by the structural role of P2O5 in the CaO-P2O5-SiO2 glasses, which was polymerization of siicate structures and resulted in [PO4] monomer structure in glasses. Due to this structural characteristics, the bond strength and packing density were changed with compositions. Proportional relationships between 1) np and Dp, 2) Tg, Td, α and CaO content, 3) E and Vm-1, and 4) KHN and P2O5 content were evaluated in this investigation.

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강릉 보광리 분청도편의 성분과 미세구조 연구 (Composition and Microstructure of Punch'ong Sherds from Bokwang-ri, Kangnung)

  • 김경남;한상목;신대용
    • 보존과학회지
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    • 제8권1호
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    • pp.10-15
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    • 1999
  • 강릉 보광리 도요지에서 출토된 분청 도편의 성분과 미세구조의 특징을 EDS부착의 주사전자현미경과 X선 회절분석기, 열팽창측정기를 이용하여 조사하였다. 도편의 태토 성분은 $SiO_2(73-78\%),\;Al_2O_3(13-16\%)$, $RO{\cdot}R_2O(4-5\%,\;R=Ca,\;Mg,\;Na,\;K),\;R_xO_y(3-6\%,\;R=Fe,Ti)$로 구성되어 있으며, $SiO_2$의 양은 많은 편이나 $Al_2O_3$의 양은 적은 편이었다. 유약은 CaO 함량이 $21-30\%$로 높은 것으로 보아 석회계열의 유약으로 생각된다. 또한 도편의 소성온도는 $1150^{\circ}C$부근의 온도로 추정된다.

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B2O3첨가에 따른 V2O5-P2O5-ZnO계 유리의 물성 및 구조와 봉착특성 (Effect of B2O3 Addition on Thermal, Structure, and Sealing Properties V2O5-P2O5-ZnO Glass)

  • 성아람;김유리안;김형순
    • 한국재료학회지
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    • 제26권10호
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    • pp.549-555
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    • 2016
  • We have investigated a glass-forming region of $V_2O_5-P_2O_5-ZnO$ glass and the effects of the addition of modifier oxides ($B_2O_3$) to the glass systems as a sealing material to improve the adhesion between the glass frits and a soda lime substrate. Thermal properties and coefficient of thermal expansion were measured using a differential scanning calorimetry, a dilatometer and a hot stage microscopy. Structural changes and interfacial reactions between the glass substrate and the glass frit after sintering (at $400^{\circ}C$ for 1 h) were measured by Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and scanning electron microscope. The results showed that the adhesion strength increases as the content of $B_2O_3$ at 5 mol% increases because of changes in the structural properties. It seems that the glass structures change with $B_2O_3$, and the $Si^{4+}$ ions from the substrate are diffused to the sealing glass. From these results, we could understand the mechanism of strengthening of the adhesion of soda lime silica substrate by ion-diffusion from the substrate to the glass.