• Title/Summary/Keyword: deposition time

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Effectiveness of Uranium Recovery by the Electrodeposition Method (전기정착법(電氣定着法)에 의한 우라늄의 회수효과(回收效果))

  • Lee, Byung-Ki;Hong, Jong-Sook;Jung, Lae-Eak
    • Journal of Radiation Protection and Research
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    • v.8 no.2
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    • pp.36-40
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    • 1983
  • Uranium radionuclides are electrodeposited on inexpensive stainless steel cathode from a mixed oxalate-chloride electrolyte. The factors affecting the optimum condition for the deposition are determined by studying the effects of deposition time, initial current, electrode spacing, pH of electrolyte and uranium concentration in the electrolyte at fixed cathode area. The experiment which was repeated 3 times at each uranium concentration with 60 minutes of deposition time, gave an error of less than 4% standard deviation at the 90% confidence level with average yield greater than 99%.

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Development of Variable Deposition Manufacturing for Ethylene Vinyl Acetatecopolymer (EVA를 이용한 가변 용착 쾌속 조형 공정 개발)

  • 이상호;신보성;정준호;안동규;양동열
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2000.05a
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    • pp.771-774
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    • 2000
  • RP techniques have inherent disadvantages caused by their working principles: stair-stepped surface of parts due to layer-by-layer stacking of layers, low build speed caused by line-by-line solidification to finish one layer, and post processing to improve surface finish, etc. The objective of this study is to propose a new RP technique, variable deposition manufacturing (VDM), which can make up for the disadvantages of the existing RP techniques, and to develop an apparatus to implement the technique. The proposed process can greatly reduce the building time and improve the surface finish of parts generated. The experiments are carried out to obtain the range of temperature of molten material to maintain its fluidity and to investigate the effect of gas cooling on the preservation of the slopes. Based on the results, some simple shapes such as a line-shape. an S-shape, and a circle-shape were fabricated from Ethylene Vinyl Acetatecopolymer (EVA). In order to examine the applicability of VDM to more general shapes, a tensile specimen and a yo-yo shape were manufactured by the proposed RP method using EVA material as the first trial approach. The present basic study has shown the possibility of a practicable utilization of the proposed VDM process to prototyping of a general three-dimensional shape.

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The Effect of Chemical Vapor Infiltrated SiC Whiskers on the Change in the Pore Structure of a Porous SiC Body

  • Joo, Byoung-In;Park, Won-Soon;Choi, Doo-Jin;Kim, Hai-Doo
    • Journal of the Korean Ceramic Society
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    • v.43 no.4 s.287
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    • pp.199-202
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    • 2006
  • In this study, SiC whiskers were grown on a porous SiC diesel particulate filter for nanoparticle filtering. To grow the whiskers at the inner pore without closing the pores, we used chemical vapor infiltration with a solution source and a dilute. As the deposition time increased, the whiskers grew and formed a network structure. After 180 min of deposition, the mean diameter of the whiskers was 174 nm and the compressive strength was 58.4 MPa. The pores shrank from $10{\mu}m\;to\;0.4{\mu}m$ and, because the whiskers filed the inner pores, the gradient of permeability decreased as the deposition time increased. However, by using the network structure of whiskers deposited for 120 min and 180 min, we obtained a diesel particulate filter with pores of $0.98{\mu}m\;and\;0.4{\mu}m$, respectively. Furthermore, the filter shows better permeability than a porous body with pores of $1{\mu}m$. In short, by filtering the nanoparticulate materials, the network structure of whiskers improves the strength, reduces the pore size and minimizes the permeability drop.

Undrained Shear Strength of Clay and Stability of Sub]marine Slope Undergoing Rapid Deposition (점토의 비배수 전단강도와 지적성퇴적에 의한 해저사면의 안정성)

  • 김승열
    • Geotechnical Engineering
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    • v.4 no.4
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    • pp.5-18
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    • 1988
  • A series of CU triaxial compression tests were conducted to investigate the variation of -untrained shear strength of underconsolidated clay at different degrees of consolidation. The soil samples were artificially made by one-dimensional consolidation using soft Bangkok Clay. The test results showed that the undrained shear strength of clay parabolically increased convoking downward with increasing degrees of consolidation. However, all the measured shear strength were unanimously related to the effective stress. These experimental results were used in the numerical analysis. A finite element computer program was developed to investigate the stability of submarine .slope undergoing rapid deposition taking into account the variation in soil compressibility and permeability during the consolidation process. The relationships of degree of consolidation with time as a function of rate of deposition and angle of slope were established. A method of predicting the time of slope failure and the volume of moving mass of soil was also made.

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A Study on Preparation of A1$_2$O$_3$ Insulation Thick Film by Electrophoretic Method (전기영동법에 의한 A1$_2$O$_3$ 절연성 후막제조에 관한 연구)

  • 전용우;주상현;조용준;소대화
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.231-234
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    • 1998
  • In this experiment, A1$_2$O$_3$thick films were prepared by electrophoretic method using A1$_2$O$_3$ fine powder of which compositions were FA-5-500 and FA-5-900. As a result of measurement for A1$_2$O$_3$ thick film characteristics due to applied voltage, deposition time and additives condition, the result of deposited films exhibited superior than others when the applied voltage and deposition time were 65 volts and 2 seconds in case of using modified suspension medium added additives. When taken a heat treatment and sintered A1$_2$O$_3$ deposition film made by electrophoresis with A1$_2$O$_3$ suspension medium at 1$700^{\circ}C$ for 5 minutes in hydrogen environment, it could be fabricated in good uniformity and electric characteristics as the A1$_2$O$_3$ insulating thick films.

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Characterization of Helicon Plasma by H$_2$ Gas Discharge and Fabrication of Diamond Tinn Films

  • Hyun, June-Won;Kim, Yong-Jin;Noh, Seung-Jeong
    • Transactions on Electrical and Electronic Materials
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    • v.1 no.2
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    • pp.12-17
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    • 2000
  • Helicon waves were excited by a Nagoya type III antenna in magnetized plasma, and hydrogen and methane are fed through a Mass Flow Controller(MFC). We made a diagnosis of properties of helicon plasma by H$_2$gaseous discharge, and fabricated the diamond thin film. The maximum measured electron density was 1${\times}$10$\^$10/ cm$\^$-3/. Diamond films have been growo on (100) silicon substrate using the helicon plasma chemical vapor deposition. Diamond films were deposited at a pressure of 0.1 Torr, deposition time of 40~80 h, a substrate temperature of 700$^{\circ}C$ and methane concentrations of 0.5~2.5%. The growth characteristics were investigated by means of X-ray Photoelectron (XPS) and X-ray Diffraction(XRD), XRD and XPS analysis revealed that SiC was formed, and finally diamond particles were definitely deposited on it. With increasing deposition time, the thickness and crystallization of the daimond thin film increased, For this system the optimum condition of methane concentration was estimated to near to 1.5%.

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Organic Gas Response Characteristics for Horizontal Direction of Fatty Acid LB Ultra-thin Films (지방산 LB초박막의 수평방향에 대한 유기가스 반응특성)

  • Lee, Jun-Ho;Choe, Yong-Seong;Kim, Do-Gyun;Gwon, Yeong-Su
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.48 no.5
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    • pp.379-384
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    • 1999
  • Langmuir-Blodgett(LB) films which have high ordered orientation and ordering structure are fabricated by LB method which deposit the ultra-thin films of organic materials at a molecular level. The electrical characteristics of stearic acid LB ultra-thin films for the horizontal direction were investigated to develop the gas sensor using LB ultra-thin films. The optimal deposition condition to deposit the LB ultra-thin films was obtained from $\pi-A$ isotherms and the deposition status of stearic acid LB ultra-thin films was verified by the measurement of deposition ratio, UV-absorbance, and electrical properties for LB ultra-thin films. The conductivity of stearic acid LB ultra-thin films for horizontal direction was about $10_{-8}[S/cm]$. The activation energy for LB ultra-thin films with respect to variation of temperature was about 1.0[eV], which was correspond to semiconductor material. The response characteristics for organic gas were confirmed by measuring the response time, recovery time, and reproducibility of the LB ultra-thin to each organic gas. Also, the penetration and adsorption behavior of gas molecule were confirmed through the organic gas response characteristics of LB ultra-thin films with respect to temperature.

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Graphene Growth with Solid Precursor-Polyethylene (고체 전구체-폴리에틸렌을 이용한 그래핀 성장)

  • Ryu, Jongseong;An, Sung Jin
    • Korean Journal of Materials Research
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    • v.29 no.5
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    • pp.304-310
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    • 2019
  • Chemical vapor deposition method using $CH_4$ gaseous hydrocarbons is generally used to synthesize large-area graphene. Studies using non-gaseous materials such as ethanol, hexane and camphor have occasionally been conducted. In this study, large-area graphene is synthesized via chemical vapor deposition using polyethylene as a carbon precursor. In particular, we used a poly glove, which is made of low-density polyethylene. The characteristics of the synthesized graphene as functions of the growth time of graphene and the temperature for vaporizing polyethylene are evaluated by optical microscopy and Raman spectroscopy. When the polyethylene vaporizing temperature is over $150^{\circ}C$, large-area graphene with excellent quality is synthesized. Raman spectroscopy shows that the D peak intensity increased and the 2D peak intensity decreased with increasing growth time. The reason for this is that sp3 bonds in the graphene can form when the correct amount of carbon source is supplied. The quality of the graphene synthesized using polyethylene is similar to that of graphene synthesized using methane gas.

Material and Structure Optimization of Substrate Support for Improving CVD Equipment Up Time (CVD 장비 Up Time 향상을 위한 기판 지지대의 재질 및 구조 최적화)

  • Woo, Ram;Kim, Won Kyung
    • Korean Journal of Materials Research
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    • v.29 no.11
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    • pp.670-676
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    • 2019
  • We study substrate support structures and materials to improve uptime and shorten preventive maintenance cycles for chemical vapor deposition equipment. In order to improve the rolling of the substrate support, the bushing device adopts a ball transfer method in which a large ball and a small ball are mixed. When the main transfer ball of the bushing part of the substrate support contacts the substrate support, the small ball also rotates simultaneously with the rotation of the main ball, minimizing the resistance that can be generated during the vertical movement of the substrate support. As a result of the improvement, the glass substrate breakage rate is reduced by more than 90 ~ 95 %, and the equipment preventive maintenance and board support replacement cycles are extended four times or more, from once a month to more than four months, and the equipment uptime is at least 15 % improved. This study proposes an optimization method for substrate support structure and material improvement of chemical vapor deposition equipment.

Comparisons of the Change in Soft Contact Lenses Parameters and the Cleaning Efficiency after Eyeliner Deposition (아이라이너 침착에 의한 소프트 콘택트렌즈 파라미터의 변화 및 세척효과의 비교)

  • Park, Mijung;Kim, Sa Hyun;Ku, Bo Kyoung;Kim, So Ra
    • Journal of Korean Ophthalmic Optics Society
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    • v.18 no.2
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    • pp.107-115
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    • 2013
  • Purpose: This study was conducted to investigate the change of soft contact lens parameters after eyeliner deposition and compare the cleaning efficiency and the recovery rate of lens parameters by different cleaning methods. Methods: The eyeliner was deposited on three types of soft contact lenses made of different materials for 1 hour, 4 hours and 6 hours and those lenses were washed by the eyeglasses ultrasonic cleaning and by hands. The changes in visible light transmittance, diameter and surface of those lenses were compared before and after cleaning of the lens. Results: The visible light transmittance of soft contact lenses decreased along with the deposition time of eyeliner. The patterns of the eyeliner deposition on soft contact lens appeared differently depending on the physical properties of the lens material. Thus, the largest eyeliner deposition was found on narafilcon A lens. The diameters of hilafilcon B and etafilcon A lenses were decreased, however, the diameter of narafilcon A lens was increased. The cleaning efficiency of the eyeliner deposition was greater with the multipurpose solution by hands than with the eyeglasses ultrasonic cleaner. However, the recovery of lens parameters such as the lens diameter, visible light transmittance and lens surface due to the eyeliner deposition to its original state was limited. Conclusions: From these results, it is suggested to minimize eye makeup when wearing soft contact lens. Furthermore, the reduced wearing time and shorter cycle of lens replacement may be needed by considering a change of lens parameter when the repeat eye makeup is applied.