• Environmental Engineering Research
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• v.22 no.2
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• pp.169-174
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• 2017

Vacuum swing adsorption (VSA) is a promising treatment method for volatile organic compounds (VOCs). This study focuses on a VSA process for regenerating activated carbon spent with VOCs, and then investigates its adsorption capacities. Toluene was selected as the test VOC molecule, and the VSA regeneration experiments results were compared to the thermal swing adsorption process. Cyclic adsorption-desorption experiments were performed using a lab-scale apparatus with commercial activated carbon (Samchully Co.). The VSA regeneration was performed in air (0.5 L/min) at 363.15 K and 13,332 Pa. The comparative results depicted that in terms of VSA regeneration, it was found that after the fifth regeneration, about a 90% regeneration ratio was maintained. These experiments thus confirm that the VSA regeneration process has good recovery while operating at low temperatures (363.15 K) and 13,332 Pa.

• Journal of Electrochemical Science and Technology
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• v.13 no.2
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• pp.213-226
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• 2022

In the present study, the corrosion behavior of aluminum Al-7075 tempered (T-6 condition) alloy was evaluated by immersion testing and electrochemical testing in 1.75% and 3.5% NaCl environment at acidic, neutral and basic pH. The data obtained by both immersion tests and electrochemical corrosion tests (potentiodynamic polarization and electrochemical impedance spectroscopy tests) present that the corrosion rate of the alloy specimens is minimum for the pH=7 condition of the solution due to the formation of dense and well adherent thin protective oxide layer. Whereas the solutions with acidic and alkaline pH cause shift in the corrosion behavior of aluminum alloy to more active domains aggravated by the constant flux of acidic and alkaline ions (Cl^- and OH^-) in the media which anodically dissolve the Al matrix in comparison to precipitated intermetallic phases (cathodic in nature) formed due to T6 treatment. Consequently, the pitting behavior of the alloy, as observed by cyclic polarization tests, shifts to more active regions when pH of the solutions changes from neutral to alkaline environment due to localized dissolution of the matrix in alkaline environment that ingress by diffusion through the pores in the oxide film. Microscopic analysis also strengthens the results obtained by immersion corrosion testing and electrochemical corrosion testing as the study examines the corrosion behavior of this alloy under a systematic evaluation in marine environment.

• Restorative Dentistry and Endodontics
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• v.38 no.1
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• pp.31-35
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• 2013

Objectives: This study compared the cyclic fatigue resistance of nickel-titanium (NiTi) files obtained in a conventional test using a simulated canal with a newly developed method that allows the application of constant fatigue load conditions. Materials and Methods: ProFile and K3 files of #25/.06, #30/.06, and #40/.04 were selected. Two types of testing devices were built to test their fatigue performance. The first (conventional) device prescribed curvature inside a simulated canal (C-test), the second new device exerted a constant load (L-test) whilst allowing any resulting curvature. Ten new instruments of each size and brand were tested with each device. The files were rotated until fracture and the number of cycles to failure (NCF) was determined. The NCF were subjected to one-way ANOVA and Duncan's post-hoc test for each method. Spearman's rank correlation coefficient was computed to examine any association between methods. Results: Spearman's rank correlation coefficient (${\rho}$ = -0.905) showed a significant negative correlation between methods. Groups with significant difference after the L-test divided into 4 clusters, whilst the C-test gave just 2 clusters. From the L-test, considering the negative correlation of NCF, K3 gave a significantly lower fatigue resistance than ProFile as in the C-test. K3 #30/.06 showed a lower fatigue resistance than K3 #25/.06, which was not found by the C-test. Variation in fatigue test methodology resulted in different cyclic fatigue resistance rankings for various NiTi files. Conclusions: The new methodology standardized the load during fatigue testing, allowing determination fatigue behavior under constant load conditions.

• The Journal of Korean Academy of Prosthodontics
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• v.45 no.1
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• pp.12-20
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• 2007

Purpose: The purpose of this study was to compare the fracture strength of the zirconia monolithic all-ceramic crowns according to the thickness (0.5mm, 0.8mm, 1.1mm) and metal-ceramic crowns (1.0mm, 1.5mm) Material and method: Twelve crowns for each of 3 zirconia crown groups were fabricated using CAD/CAM system (Kavo, Germany) and twelve crowns for each of 2 metal-ceramic crown groups were made by the conventional method. All crowns were luted to the metal dies using resin cement. Half of the specimens were exposed to thermocycling ($5-55^{\circ}C$, 1 Hz) and cyclic loading (300,000 cycles, 50N). Subsequently, all crowns were mounted on the testing jig in a universal testing machine. The load was directed at the center of crown with perpendicular to the long axis of each specimen until catastrophic failure occurred. Analysis of variance and Tukey multiple comparison test (P<.05) were used for statistical analysis of all groups, and paired t-test (P<.05) was followed for statistical comparison between each groups' fracture load before and after cyclic loading. Results: 1. The fracture strength of the zirconia monolithic crowns and the metal-ceramic crown increased as thickness increased (P<.05). 2. The cyclic loading and thermocycling significantly decreased the fracture strength of the zirconia monolithic crowns (P<.05). 3. The standard deviation of fracture strength of the zirconia monolithic crowns was very low. Conclusion: The fracture strength of the zirconia monolithic crowns for the posterior area tends to be higher with thickness increased and 0.8mm or over in thickness is recommended to have similar or over the fracture strength of metal-ceramic crowns.

• Journal of the Korean Society for Nondestructive Testing
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• v.36 no.3
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• pp.225-230
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• 2016

Fiber Bragg grating (FBG) sensors are currently the most prevalent sensors because of their unique advantages such as ease of multiplexing and capability of performing absolute measurements. They are applied to various structures for structural health monitoring (SHM). The signal characteristics of FBG sensors under thermal loading should be investigated to enhance the reliability of these sensors, because they are exposed to certain cyclic thermal loads due to temperature changes resulting from change of seasons, when they are applied to structures for SHM. In this study, tests on specimens are conducted in a thermal chamber with temperature changes from -$20^{\circ}C$ to $60^{\circ}C$ for 300 cycles. For the specimens, two types of base materials and adhesives that are normally used in the manufacture of packaged FBG sensors are selected. From the test results, it is confirmed that the FBG sensors undergo some degree of compressive strain under cyclic thermal load; this can lead to measurement errors. Hence, a pre-calibration is necessary before applying these sensors to structures for long-term SHM.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.24 no.4
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• pp.151-157
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• 2014

The degradation mechanisms of thermal barrier coatings (TBCs) were investigated in different thermal fatigue condition in terms of microstructural analyses. The isothermal and cyclic oxidation tests were conducted to atmospheric plasma sprayed-TBCs on NIMONIC 263 substrates. The delamination occurred by the oxide layer formation at the interface, the Ni/Cr-based oxide was formed after Al-based oxide layer grew up to ${\sim}10{\mu}m$ in the isothermal condition. In the cyclic oxidation with dwell time, the failure occurred earlier (500 hr) than in the isothermal oxidation (900 hr) at same temperature. The thickness of Al-based oxide layer of the delaminated specimen in the cyclic condition was ${\sim}4{\mu}m$ and the interfacial cracks were observed. The acoustic emission method revealed that the cracks generated during the cooling step. It was considered that the specimens were prevented from the formation of the Al-based oxide by cooling treatment, and the degradation mode in the cyclic test was dominantly interfacial cracking by the difference of thermal expansion coefficients of the coating layers.

• Geomechanics and Engineering
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• v.7 no.3
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• pp.297-316
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• 2014

This paper presents a detailed study focused on investigating the effects of silt content on the static and dynamic properties of sand-silt mixtures. Specimens with a low-plastic silt content of 0, 15, 30 and 50% by weight were tested in static triaxial, cyclic triaxial, and resonant columns in addition to consolidation tests to determine such parameters as compression index, internal friction angle, cohesion, cyclic stress ratio, maximum shear modulus, normalized shear modulus and damping ratio. The test procedures were performed on specimens of three cases: constant void ratio index, e = 0.582; same peak deviator stress of 290 kPa; and constant relative density, $D_r$ = 30%. The test results obtained for both the constant-void-ratio-index and constant-relative-density specimens showed that as silt content increased, the internal friction angle, cyclic stress ratio and maximum shear modulus decreased, but cohesion increased. In testing of the same deviator stress specimens, both cohesion and internal friction angle were insignificantly altered with the increase in silt content. In addition, as silt content increased, the maximum shear modulus increased. The cyclic stress ratio first decreased as silt content increased to reach the threshold silt content and increased thereafter with further increases in silt content. Furthermore, the damping ratio was investigated based on different silt contents in three types of specimens.

• Structural Engineering and Mechanics
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• v.53 no.2
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• pp.189-204
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• 2015

After the large destruction of Lisbon due to the 1755 earthquake, the city had to be almost completely rebuilt. In this context, an innovative structural solution was implemented in new buildings, comprising internal timber framed walls which, together with the floors timber elements, constituted a 3-D framing system, known as "cage", providing resistance and deformation capacity for seismic loading. The internal timber framed masonry walls, in elevated floors, are constituted by a timber frame with vertical and horizontal elements, braced with diagonal elements, known as Saint Andrew's crosses, with masonry infill. This paper describes an experimental campaign to assess the in-plane cyclic behaviour of those so called "frontal" walls. A total series of 4 tests were conducted in 4 real size walls. Two models consist of the simple timber frames without masonry infill, and the other two specimens have identical timber frames but present masonry infill. Experimental characterization of the in-plane behaviour was carried out by static cyclic shear testing with controlled displacements. The loading protocol used was the CUREE for ordinary ground motions. The hysteretic behaviour main parameters of such walls subjected to cyclic loading were computed namely the initial stiffness, ductility and energy dissipation capacity.

• Restorative Dentistry and Endodontics
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• v.45 no.3
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• pp.37.1-37.8
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• 2020

Objectives: This study aims to compare the cyclic fatigue resistance of VDW.ROTATE, TruNatomy, 2Shape, and HyFlex CM nickel-titanium (NiTi) rotary files at body temperature. Materials and Methods: In total, 80 VDW.ROTATE (25/0.04), TruNatomy (26/0.04), 2Shape (25/0.04), and HyFlex CM (25/0.04) NiTi rotary files (n = 20 in each group) were subjected to static cyclic fatigue testing at body temperature (37℃) in stainless-steel artificial canals prepared according to the size and taper of the instruments until fracture occurred. The number of cycles to fracture (NCF) was calculated, and the lengths of the fractured fragments were measured. The data were statistically analyzed using a 1-way analysis of variance and post hoc Tamhane tests at the 5% significance level (p < 0.05). Results: There were significant differences in the cyclic fatigue resistance among the groups (p < 0.05), with the highest to lowest NCF values of the files as follows: VDW.ROTATE, HyFlex CM, 2Shape, and TruNatomy. There was no significant difference in the lengths of the fractured fragments among the groups. The scanning electron microscope images of the files revealed typical characteristics of fracture due to cyclic fatigue. Conclusions: The VDW.ROTATE files had the highest cyclic fatigue resistance, and the TruNatomy and 2Shape files had the lowest cyclic fatigue resistance in artificial canals at body temperature.

• Restorative Dentistry and Endodontics
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• v.42 no.3
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• pp.224-231
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• 2017

Objectives: To determine the actual revolutions per minute (rpm) values and compare the cyclic fatigue life of Reciproc (RPC, VDW GmbH), WaveOne (WO, Dentsply Maillefer), and TF Adaptive (TFA, Axis/SybronEndo) nickel-titanium (NiTi) file systems using high-speed camera. Materials and Methods: Twenty RPC R25 (25/0.08), 20 WO Primary (25/0.08), and 20 TFA ML 1 (25/0.08) files were employed in the present study. The cyclic fatigue tests were performed using a dynamic cyclic fatigue testing device, which has an artificial stainless steel canal with a $60^{\circ}$ angle of curvature and a 5-mm radius of curvature. The files were divided into 3 groups (group 1, RPC R25 [RPC]; group 2, WO Primary [WO]; group 3, TF Adaptive ML 1 [TFA]). All the instruments were rotated until fracture during the cyclic fatigue test and slow-motion videos were captured using high-speed camera. The number of cycles to failure (NCF) was calculated. The data were analyzed statistically using one-way analysis of variance (ANOVA, p < 0.05). Results: The slow-motion videos were indicated that rpm values of the RPC, WO, and TFA groups were 180, 210, and 425, respectively. RPC ($3,464.45{\pm}487.58$) and WO ($3,257.63{\pm}556.39$) groups had significantly longer cyclic fatigue life compared with TFA ($1,634.46{\pm}300.03$) group (p < 0.05). There was no significant difference in the mean length of the fractured fragments. Conclusions: Within the limitation of the present study, RPC and WO NiTi files showed significantly longer cyclic fatigue life than TFA NiTi file.