• 한국도로학회논문집
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• 제15권5호
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• pp.11-20
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• 2013

PURPOSES : This study is to suggest time to spray curing compound, the amount of curing compound, and the number of times to spray curing compound based on indoor tests. METHODS : Based on the literature review, two methods are used in this study, One is test for water retention of concrete curing material and the other is test for abrasion resistance of concrete surfaces by the rotating-cutter method. Through those methods, curing compound was evaluated. RESULTS : The result of the laboratory experiment for time to spray curing compound indicates that 30 minutes after placing concrete is optimal. For the amount of curing compound, $0.5{\ell}/m^2$ is the minimum quantity for both concretes. Through test of the number of times to spray curing compound, method to spray the whole amount of curing compound in twice is more efficient than it to spray the whole amount at a time. Also, method of separately 30-50 minutes spray is better than method of separately 10-30 minutes spray. CONCLUSIONS : From the testing results, it can be proposed that optimum time to curing compound is $30{\pm}15$ minutes, $0.5{\ell}/m^2$ is efficient for spraying the whole amount of curing compound at a time, and $0.4{\ell}/m^2$ is the best for spraying the whole amount of curing compound in twice, which sprays it in 20 minutes after 30 minutes from placing concrete.

• 한국도로학회논문집
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• 제19권3호
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• pp.11-18
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• 2017

PURPOSES : This study investigates the effect on concrete pavement accordance with the curing methods in cool weather and supports the best method in the field. METHODS : Two field tests evaluated the curing methods of concrete pavement in cool weather. Firstly, five curing methods were tested, including normal curing compound, black curing compound, bubble sheet, curing mat, and curing mat covered with vinyl. Concrete maturity was compared from temperature data. Secondly, normal curing compound and curing mat with vinyl, which showed the best performance, were compared in terms of maturity and join condition index. RESULTS:From the field tests, it is an evident that curing mat with vinyl accelerated the concrete strength. Therefore, it is possible to conduct saw-cut works in cool weather, which minimizes damage on concrete at joint. CONCLUSIONS : For concrete pavement in cool weather, using curing mat with vinyl as the curing method could overcome the strength delay. Therefore, strength and durability problems on concrete at joint due to cool weather would be fewer in the future.

• 한국도로학회논문집
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• 제16권3호
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• pp.51-57
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• 2014

PURPOSES : This study is to suggest tunnel length to spray curing compound, based on the field tests. METHODS : At first field test, length from the entrance of tunnel to wet wall was checked by visual survey. The second and third test, various sensors were installed in concrete or in tunnel, such as RH sensor, temperature sensor, portable weather station and etc.. And also, test for bleeding and retaining water of concrete were conducted to evaluate environmental effect on concrete pavement. RESULTS : The result of the field experiment for tunnel length to spray curing compound indicates that length changes depending on tunnel length, season, and location. Environmental condition of a short tunnel was not much different between location near entrance and at center of tunnel. However, in case of a medium and long tunnel, effect of outside environmental condition decreased, when location moved into tunnel center of it. CONCLUSIONS : From the testing results, it can be proposed that optimum tunnel length to spray curing compound is 60m for a medium and long tunnel, and whole length for a short tunnel.

• 한국도로학회논문집
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• 제7권2호
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• pp.45-55
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• 2005

시멘트 콘크리트 포장은 시공초기의 품질관리가 포장의 장기공용성에 큰 영향을 주는 것으로 알려져 있다. 따라서 시공초기에 발생되는 문제점을 최소화하기 위한 다양한 연구가 국내외에서 활발하게 진행되고 있다. 일반적으로 시멘트 콘크리트의 품질관리에서 양생은 중요한 사항이며, 포장용 시멘트 콘크리트에서도 양생시에 양생제를 사용하여 슬래브 표면에 불투수 막을 형성하여 수분증발을 방지하는 피막양생 (membrane curing)을 많이 사용하고 있다. 양생제의 역할은 콘크리트 표면의 수분증발억제에 있다. 국내에서 사용되고 있는 양생제는 시공품질관리 측면에서 살포량이 적정한지에 대한의문이 계속 제기되어 왔다. 본 연구에서는 시멘트 콘크리트 포장 시공시 살포되는 양생제의 양을 조정하여 다양한 살포량에 따른 증발량 관측을 통해 양생제 살포량과 수분증발량 변화와의 상관관계를 제시하였다. 이를 위해 2002년과 2003년 여름철에 고속도로 시공현장에서 4회에 걸쳐 다양한 양생제 살포량$(0에 따른 증발량 콘크리트 포장의 온도변화, 콘크리트 표면의 강도발현속도(초음파 전달속도) 등을 측정하였다. 본 연구에서 얻은 결론은 현재 국내 시공현장에서의 양생제 살포량은 약 $160ml/m^2$으로 나타났고, 수분증발은 억제하고 적정한 보습효과를 얻기 위한 최적 양생제 살포량은 약 $400ml/m^2$인 것으로 분석되었다. 강도발현속도 시험결과 양생제의 살포량의 변화가 장기강도에 큰 영향을 미치지 않는 것으로 판단되었다.

• Bulletin of the Korean Chemical Society
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• 제31권8호
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• pp.2272-2278
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• 2010

A new hybrid thermosetting maleimido epoxy compound 4-(N-maleimidophenyl) glycidylether (N-MPGE) is prepared by reacting N-(4-hydroxyphenyl) maleimide (HPM) with Epichlorohydrin by using benzyltrimethylammonium chloride as a catalyst. The resulting compound possesses both the oxirane ring and maleimide group. The curing reaction of these maleimidophenyl glycidylether epoxy compound (N-MPGE) with amines as curing agents such as ethylendiamine (EDA), diethylentriamine (DETA) and triethylenetetramine (TETA), aminoethylpiperazine (AEP) and isophoronediamine, IPDA), are studied. Incorporation of maleimide groups in the epichlorohydrin provides cyclic imide structure and high cross-linking density to the cured resins. The cured samples exhibited good thermal stability, excellent chemical (acid/alkali/solvent) and water absorption resistance. Morphological studies by the SEM technique further confirmed the phase homogeneity net work of the cured systems.

• 한국응용과학기술학회지
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• 제26권1호
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• pp.18-23
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• 2009

Curing behavior and structural property of an inorganic compound added urea-formaldehyde(UF) and urea-melamine-formaldehyde(UMF) were studied. In addition, tensile strength and formaldehyde emission of plywoods made of those resin binders were studied. Curing temperature and structure were not changed, but tensile strengths of plywoods manufactured both with a UF resin and a UMF resin were decreased slightly as increased amount of inorganic compound. Formaldehyde emissions from plywoods were reduced as increased amount of inorganic compound. Wheat flour as an extender was helped to reduce of formaldehyde emission. From the result of this study it might be estimated that using appropriate amount of inorganic compound and proper resin system can be strengthened bond strength and reduced formaldehyde emission.

• 콘크리트학회논문집
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• 제17권4호
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• pp.655-662
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• 2005

Evaporation of concrete influences the development of both initial transverse cracking and delamination in the concrete slab. It was suggested that spatting distress might develop in the slab where the initial transverse cracking occurred by theoretical equations and a field investigation. Thus, efforts to prevent the evaporation of concrete using proper curing methods are required to minimize the distresses of the slabs. Effective curing thickness (ECT) concept was used in this paper to evaluate various curing methods used to prevent the evaporation from concrete. Curing effectiveness quantified by the ECT of different types and amounts of curing compound under various curing conditions was investigated based on the results of laboratory tests. According to the test results, the wind speed is inferred to be a significant factor of the magnitude and continuance duration of the curing effectiveness.

• 마이크로전자및패키징학회지
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• 제29권4호
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• pp.83-87
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• 2022

최근 반도체 패키지 두께가 점점 얇아짐에 따라 휨(warpage) 문제가 대두되고 있다. 휨(warpage)은 패키지 구성요소들 간의 물성 차이로 인해 발생하기 때문에, 휨(warpage)을 예측하기 위해서는 주된 구성요소인 EMC(Epoxy molding compound)의 정확한 물성 파악이 필수적으로 요구된다. 특히 EMC는 경화 공정 중 경화 수축을 보이는데, 겔점 이후에 발생하는 유효 경화 수축은 휨(warpage) 발생의 핵심 요소이다. 본 연구에서는 유전 센서를 이용해 측정한 소실 계수로부터 실제 반도체 패키지 경화 공정 동안 발생하는 EMC의 겔점이 정의되었다. 유전 센서로부터 얻은 결과를 분석하기 위해 DSC(Differential scanning calorimetry) 시험과 rheometer 시험이 수행되었다. 그 결과, 유전 측정법이 EMC 경화상태 모니터링에 효과적인 방법임이 검증되었다. 유전 측정과 동시에 광섬유 센서를 이용해 EMC의 경화 공정 중 변형률 변화 추이가 함께 측정되었다. 위 결과들로부터 경화 공정 중 발생하는 EMC의 유효 경화 수축이 측정되었다.

• Bulletin of the Korean Chemical Society
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• 제27권10호
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• pp.1542-1548
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• 2006

Maleimide modified epoxy compounds were prepared by reacting N-(4-hydroxyphenyl) maleimide (HPM) with diglycidylether of bisphenol-A. Triphenylphosphine was used as catalyst and methylethylketone as solvent. The resulting compound possessed both the oxirane ring and maleimide group. The curing reaction of the maleimide epoxy compound with amine curing agents such as 1-(2-aminoethyl) piperazine (AEP) and 5-amino-1,3,3-trimethylcyclohexane methylamine isophorone diamine, IPDA) were studied. Incorporation of maleimide groups in the epoxy resin provides cyclic imide structure and high cross-linking density to the cured resins. The cured samples were found to have good thermal stability, chemical resistance (acid/alkali/solvent) and water absorption resistance.

• 한국연초학회지
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• 제25권1호
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• pp.27-33
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• 2003

This study was conducted to determine the changes of nitrogen compounds in lamina and midrib during the curing process with the different curing methods, such as priming and stalk-cut curing. After KB 108 burley tobacco was cultivated by the different fetilization levels such as standard and 20% higher, only the tips and leaf were harvested. Though the contents of total alkaloid and total nitrogen were similar in lamina, midrib showed a very low contents of those components by the different curing method and fertilization levels. The content of nitrate-nitrogen in lamina increased during a middle of curing process, and then these compound was decreased during an end of curing process by stalk-cut curing method. Nitrate-nitrogen contents in the lamina by the priming curing showed a high level caused by rapid drying process during an end of curing process. That component in midrib was 5-6 times higher than that of lamina. The contents of ammonia-nitrogen in the lamina and midrib were increased during a curing process. Though those amount in tips showed a similar by a different fetilization and curing method, midrib of stalk-cut curing showed a slow increasing during a curing process.