• Polymer(Korea)
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• v.34 no.6
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• pp.574-578
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• 2010

In this study, the caprolactone modified hydroxy acrylates (CHAs) were synthesized by ring-opening reaction of caprolactone and 2-hydroxyethyl acrylate (2-HEA) as initiator. Also, the caprolactone modified urethane acrylate (UA) oligomers were synthesized by condensation reaction of previously synthesized CHAs, 2-hydroxyethyl acrylate (2-HEA) and hexamethylene diisocyanate trimer (HDT). Using the hydroxy number of CHAs, the molecular weights of the CHAs were calculated easily and their molecular weight was similar to the theoretical molecular weight of them. The viscosity of UA oligomers decreased as increasing a content of CHA in the UA oligomer. Cure films were prepared from UA oligomer, reactive diluents, and UV initiator to investigate their physical properties. The thermal stability and color difference on high temperature for the cured film were improved as increasing the crosslinking density. Their surface hardness was also increased as increasing crosslinking density of the cured films, but their elongation at break was decreased.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.31 no.4
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• pp.420-425
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• 1986

This study was conducted to investigate the influence of air temperature and relative humidity on excessive drying rate of burley tobacco. In experiment I, 4 temperatures and I humidity by day and air curing by night were treated from initial curing stage. In experiment II, 15 combinations of 3 temperatures and 5 humidities were applied from the yellow stage of cure. Yellowish cured leaves resulted from overdrying at high temperature and especially, at low humidity. How- ever, these were not produced at 75-80% RH and under 35$^{\circ}C$ by day with air curing b y night. The proper range of temperature and humidity for desirable color of cured leaf were the combinations of 30$^{\circ}C$, 75-80% RH or 35$^{\circ}C$, 80-85% RH. As excessive drying leaves increased, physical properties of cured leaves were poorer and chemical contents were less decomposed.

• Food Science of Animal Resources
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• v.37 no.3
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• pp.429-439
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• 2017

This study investigated the antioxidative and functional effects of a curing agent containing grapefruit seed extract (GSE) on the quality and storage characteristics of chicken breast. The total polyphenol and total flavonoid contents of GSE were 45.06 mg/g and 36.06 mg/g, respectively. The $IC_{50}$ value of 2,2-diphenyl-1-picrylhydrazyl hydroxyl scavenging of GSE was $333.33{\mu}g/mL$. The chicken breast comprised six groups: no-treatment (N), 0.2% ascorbic acid + 70 ppm sodium nitrite (C), 0.05% GSE (G0.05), 0.1% GSE (G0.1), 0.3% GSE (G0.3), and 0.5% GSE (G0.5). The pH and cooking loss of cured chicken breast decreased with increasing GSE levels, and the water holding capacity increased with increasing GSE levels. The hardness and chewiness of GSE-treated chicken breast were higher than those of N and C. Hunter's L and a color values increased significantly after GSE addition. Moreover, 0.1% GSE (G0.1) increased the flavor and total acceptability scores. The 2-thiobarbituric acid and volatile basic nitrogen values of the 0.5% GSE group decreased significantly compared with those of C group. Total microbial counts of GSE-treated chicken breast were higher than those of C, but that lower than those of N. Adding GSE to chicken breast delayed lipid peroxidation and had antimicrobial effects during cold storage. GSE improved shelf life and palatability; therefore, it could be used as a natural antioxidant and functional curing agent ingredient in meat products.

• Restorative Dentistry and Endodontics
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• v.36 no.4
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• pp.324-335
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• 2011

Objectives: This study investigated the effects of the color components of light-cured composite resin before and after polymerization on degree of conversion (DC) and biaxial flexural strength (FS). Materials and Methods: Four enamel shades (A1, A2, A3, A4) and two dentin shades (A2O, A3O) of Premisa (Kerr Co.) and Denfil (Vericom Co.) were evaluated on their CIE $L^*,\;a^*,\;b^*$ color components using the spectrophotometer before curing, after curing and at 7 day. The DC of same specimens were measured with Near-infrared spectrometer (Nexus, Thermo Nicolet Co.) at 2 hr after cure and at 7 day. Finally, the FS was obtained after all the other measurements were completed at 7 day. The correlations between each color component and DC and FS were evaluated. Results: The light-curing of composite resin resulted in color changes of Premisa in red-blue direction and Denfil in green-blue direction. The DC and FS were affected by product, time and shade (3-way ANOVA, p < 0.05) and product and shade (2-way ANOVA, p < 0.05), respectively. Premisa only showed a significant correlation between the DC and CIE $a^*$ component - before and after polymerization (Pearson product moment correlation, p < 0.05). The FS of Premisa showed significant negative correlations with CIE $a^*$ and CIE $b^*$ components. Conclusions: The DC and FS of the light-curing composite resin were affected by the color components of the material before and after polymerization.

• Restorative Dentistry and Endodontics
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• v.42 no.2
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• pp.118-124
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• 2017

Objectives: This study aimed to evaluate the color stability of bulk-fill and nanohybrid resin-based composites polished with 3 different, multistep, aluminum-oxide impregnated finishing and polishing disks. Materials and Methods: Disk-shaped specimens (8 mm in diameter and 4 mm in thickness) were light-cured between two glass slabs using one nanohybid bulk-fill (Tetric EvoCeram, Ivoclar Vivadent), one micro-hybrid bulk-fill (Quixfil, Dentsply), and two nanohybrid incremental-fill (Filtek Ultimate, 3M ESPE; Herculite XRV Ultra, Kerr) resin-based composites, and aged by thermocycling (between $5-55^{\circ}C$, 3,000 cycles). Then, they were divided into subgroups according to the polishing procedure as SwissFlex ($Colt\grave{e}ne/Whaledent$), Optidisc (Kerr), and Praxis TDV (TDV Dental) (n = 12 per subgroup). One surface of each specimen was left unpolished. All specimens were immersed in coffee solution at $37^{\circ}C$. The color differences (${\Delta}E$) were measured after 1 and 7 days of storage using a colorimeter based on CIE Lab system. The data were analyzed by univariate ANOVA, Mann-Whitney U test, and Friedmann tests (${\alpha}=0.05$). Results: Univariate ANOVA detected significant interactions between polishing procedure and composite resin and polishing procedure and storage time (p < 0.05). Significant color changes were detected after 1 day storage in coffee solution (p < 0.05), except Quixfil/Optidisc which was color-stable after 7 days (p > 0.05). Polishing reduced the discoloration resistance of Tetric EvoCeram/SwissFlex, Tetric EvoCeram/Praxis TDV, Quixfil-SwissFlex, and all Herculite XRV Ultra groups after 7 days storage (p < 0.05). Conclusions: Discoloration resistance of bulk-fill resin-based composites can be significantly affected by the polishing procedures.

• Restorative Dentistry and Endodontics
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• v.18 no.1
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• pp.215-226
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• 1993

Color stability of tooth colored restorative resins is an important factor, particularly in anterior teeth restoration. The purpose of this study was to evaluate the color stability and opacity change of several light curing composite resins. Specimens of eight composite resins(Prisma AP. H., Brilliant Enamel, Charisma, Durafil, Helio Progress, Herculite XR, P-50 and Silux Plus) were divided into two groups : In Group 1, the specimens were polymerized by visible light curing unit for 60 seconds on both sides and in Group 2, the post-cured specimens were heat tempered by light/heat curing unit for 45 units(about 18 min.). All specimens were stored in distilled water at $60^{\circ}C$ for 30 days. The color characteristics($L^*,a^*,b^*$) and opacity of the specimens before and after immersion were measured by spectrocolorimetry and the total color difference(${\Delta}E^*$) and opacity change (${\Delta}Y%$) were computed. The results obtained were as follows : 1. SP and APH in both groups, DF, HP and HXR in Group 1 showed ${\Delta}E^*$-value above 2.0. 2. DF, HP, SP and HXR in Group 1 showed higher ${\Delta}E^*$-value than in Group 2, but the others had no significant difference. 3. The opacity of CH and HXR in Group 1, and of CH and BE in Group 2 decreased after immersion, while that of the others increased. 4. Opacity change of BE, P50 and HXR was significantly different between Group 1 and 2. These results suggest that color change in the post-cure heat tempered specimens by light/heat curing unit was smaller than that of the specimens polymerized by visible light curing unit. No clinically detectable opacity changes were noted for any materials in either goup.

• Journal of the Korean Society of Tobacco Science
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• v.1 no.1
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• pp.56-62
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• 1979

Boring the process of curing of the tobacco ( Nicotiana tabacum L. clicks) leaf, the and other fundamental components of the tobacco leaf was observed The amount of total chlorophyll was reduced from 2902$\mu\textrm{g}$/gr to 1, 131$\mu\textrm{g}$/gr as a function of curing time. In the case of total carotene, the concentration was increased from 373-712$\mu\textrm{g}$/gr. to 3, 003~2, 215$\mu\textrm{g}$/gr. up to 70 hours of curing period. However, after 70 hours of curing, the concentration of total carotene stared to be decreased up to 1, 050~1, 039$\mu\textrm{g}$/gr. Simultaneously, the greenish yellow color becomes to be close an intermediate color between yellow and orange. The amount of total nicotine and nitrogen (2~2%) in the green harvested leaf was essentially identical after the curing process. However, the amount of total sugar was enhanced from 17%, in the green harvested leaf, to 35% at the time of 70 hours curing. At the end of the curing, the amount of total sugar was again reduced up to 16%. The correlation coefficient (r) between the axis of the color coordinate and the ratio of chlorophyll/carotene was estimated to be r=-0.96. This result indicates a linear relationship between those two parameters and the following linear equation is obtained as y=28.87-68.38 x. From the above equation, x=0.442 could be estimated when chlorophyll was completely decomposed (ylongrightarrowO). As a consequence of this result, we can suggest the tobacco leaf of Hicks belongs to the high quality level.

• Journal of the Korean Society of Food Science and Nutrition
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• v.14 no.3
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• pp.215-222
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• 1985

In order to examine the effect of 'Streptococcus lactis' inoculation on the maturation of cured ham, physicochemical changes in brine solution with and without inoculation were compared during period. The pH value of the curing solution in the inoculated sample were slightly higher than those in uninoculated one after 7 days of curing. The color development of cured meat was accelerated by the inoculation of the isolates as showing a 80% of color development within 7 days of curing. Among the 17 amino acids determined from the water protein, glutamic acid, valine and leucine were higher in the inoculated meat than those in uninoculated meat at the 7 and 10 days of curing. The oleic acid content was the highest among the 13 fatty acids detected from the all samples, and the content of oleic acid and total unsaturated fatty acids in inoculated samples were slightly higher than those in uninoculated samples.

• Restorative Dentistry and Endodontics
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• v.34 no.3
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• pp.199-207
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• 2009

The objective of this study was to evaluate the effect of color measuring instrument by measuring the color of dental composite resins. Nine shade light cured composite resin disks were prepared (diameter : 15 mm, thickness : 4 mm). CIE $L^*a^*b^*$ color scale of each disk was measured with 3 different types of spectrophotometer [MiniScan XE plus (Model 4000S, Hunter Lab, USA), CM-3500d (Minolta, Japan) and Specbos 2100 Miniature VIS Reflection spectrometer (Serial No: 319416, JETI Technishe VIS Instrumentic GmbH. Germany)]. Miniscan XE Plus and CM-3500d using identical measuring geometry with different size of viewing aperture. But Specbos 2100 using different measuring geometry. Within the limitation of this study, there were color difference (${\Delta}E^*$) from 2.4 to 7.8 between Miniscan XE Plus and CM-3500d, but $L^*$, $a^*$, $b^*$ values showed the high correlation. However, there were great color difference (${\Delta}E^*$) in the extent of about 20 between instruments with the different measuring geometry. Therefore, color scale measured by color measuring instrument should be used as a relative value rather than an absolute value in the field of dentistry.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.36 no.1
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• pp.1-6
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• 1991

A field experiment was conducted to find out the effects of nitrogen and potassium rates on the chemical constituents and physical properties of burley tobacco (1988； Burley 21. 1989； Burley 21 and KB 101) during successive two years. KB 101 was low in total nitrogen and total alkaloid contents and potassium/total nitrogen ratio of cured leaf. but high in the lightness, red and yellow color and filling power, comparing to Burley 21. The increasing rates of total nitrogen and total alkaloid contents were larger when nitrogen applied to 22.75kg/10a, but they were smaller when nitrogen applied above 22.75 kg/l0a. The potassium content, potassium/total nitrogen ratio, filling power and shatter resistance index of cured leaf were decreased by nitrogen fertilizer addition. The potassium content and shatter resistance index were increased by potassium fertilizer addition. The effect of nitrogen rate on the potassium/total nitrogen ratio of cured leaf was larger than the effect of potassium rate. When the nitrogen fertilizer being applied above 22.75 kg/l0a, there were no advantageous effects on the chemical and physical properties. It is considered to be sufficient that the potassium application is about 35.0 kg/l0a.