• Title/Summary/Keyword: coating film

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Preparation and Characterization of $Ge_{20}As_{20}Se_{60}$ Amorphous Chalcogenide Thin Film by Spin Coating (Spin-coating에 의한 $Ge_{20}As_{20}Se_{60}$ 비정질 chalcogenide 박막의 제조 및 광특성 분석)

  • 이강구;최세영
    • Journal of the Korean Ceramic Society
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    • v.37 no.3
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    • pp.219-226
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    • 2000
  • Amorphous Ge20As20Se60 chalcogenide thin films were prepared by spin coating technique from mixed solutions of As40Se60 and Ge40Se60 dissolved in ethylenediamine. Films were prepared at a roating speed of 3500 rpm and spinning time was 10 second and heat-treateed at 27$0^{\circ}C$ for 1 hour. The resulting film thickness and RMS roughness were approximately 340 nm and 15$\AA$. Photostructure changes were investigated with 514.5nm Ar+ laser irradiation and heat-treatment. After Ar+ laser irradiation, transmittance and transmission efficiency decreased respectively up to 24.9% at 2.43 eV and 67.5% at 3.27 eV, and absorption edge shifted toward long wavelength. Optical bandgap changed from 2.03 to 1.83 eV, and absoprtion coefficient and absorption efficiency increased up to 0.33$\times$105cm-1 at 3.37eV and 88.3% at 1.31 eV, respectively. These photodarkening state were recovered reversibly by heat-treatment at 27$0^{\circ}C$ for 1 hour. Photodarkening and thermal bleaching effects by laser irradiation and heat-treatment revealed reversible amorphous-to-amorphous transition varying only coordination number.

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Improvement of Spray Coating Uniformity using ESD Electrodes (ESD 전극을 이용한 분무코팅 균일도 개선에 관한 연구)

  • Dang, Hyun-Woo;Yang, Seong-Wook;Doh, Yang-Hoi;Choi, Kyung-Hyun
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.15 no.2
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    • pp.118-124
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    • 2016
  • In this study, experiments are conducted to improve spray coating uniformity by using second and third electrodes based on the electrospray atomization mechanism. The uniformity of fabricated thin films can be improved by adjusting the design of the second electrode. The implementation of the second electrode with an elongated hole and a bending angle of $90^{\circ}$ results in highly uniform films. In addition, induced area to substrate is increased by lowering the applied voltage using the third electrode with a round rod shape. A linear correlation between applied voltage and induced area is confirmed. Thin film thickness and surface roughness are measured after the fabrication of thin films through the electrospray process. It is confirmed that a thin film is formed having an average thickness of 273.44 nm, a thickness uniformity of less than 10%, and a surface roughness of 3 nm.

NH3 sensing properties of porous CuBr films prepared by spin-coating (스핀 코팅법으로 제작한 다공성 CuBr 필름의 암모니아 감응특성)

  • Kim, Sang-Kwon;Yu, Byeong-Hun;Yoon, Ji-Wook
    • Journal of Sensor Science and Technology
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    • v.30 no.6
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    • pp.451-455
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    • 2021
  • Porous copper bromide (CuBr) films are highly advantageous for detecting ammonia (NH3). The fabrication of porous CuBr films requires complex high-temperature processes or multistep processes. Herein, we report the uncomplicated preparation of porous CuBr films by a spin-coating method and the films' excellent NH3 sensing properties. The porous films were prepared by spin-coating 100, 150, and 200 mM CuBr solutions, and then dried in a vacuum oven for 2 h. All the films showed a high NH3 response; in particular, the film prepared using a 100 mM CuBr solution showed an extremely high response (resistance ratio = 852) to 5 ppm NH3. The film also showed fast response and recovery times, 272 s and 10 s respectively, even at room temperature. The outstanding NH3 sensing characteristics were explained in relation to the porosity and thickness of the prepared films. The high-performance NH3 sensors used in this study can be used for both indoor air quality and environmental monitoring applications.

Development of Blue Light Cut Films Using a Roll-to-Roll Nano Micro Coating System

  • Hwang, Joong Kook;Shina, Hoon-Kyu;Chang, Sang-Mok
    • Transactions on Electrical and Electronic Materials
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    • v.17 no.3
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    • pp.178-181
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    • 2016
  • In this study a coating experiment was performed to fabricate blue light cut films, which represent a 390~430 nm cut off rate of more than 40% and a transmittance rate of more than 90%, using a roll-to-roll nano micro coating system. The study also analyzed the characteristics of the blue light cut films. Thus, the hardness, which is more than 3H, is ensured through fabricating films using a Sol-Gel process that will determine the proper hardness level. Also, the experiment shows excellent results by cutting blue light through a mixing blue light powder.

Parameters Affecting the TiN Coated Machining Tool's Life (질화 티타늄이 코팅된 절삭공구의 수명에 영향을 미치는 인자)

  • 최병대;김동수
    • Journal of the Korean institute of surface engineering
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    • v.28 no.2
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    • pp.77-82
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    • 1995
  • In this study, we examined the relationships between the coating film's properties, such as microhardness, adhesion of coating fil $m_strate, and machining tool's life time. Samples were prepared by coating TiN on the 5.5 diameter twist drills using reactive ion plating technology, For measuring microhardness and adhesion of fil $m_strate, HSS plate was used for substrate. TiN coated drill's life time was dependent on the adhesion of fil $m_strate and averagely increased by several ten times more than uncoated drill's. The major parameter affecting TiN coated drill's life time was the strong adhesion between coating film and substrate.ate.

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Eddy Current System For Coating Thickness Measurement

  • Rerkratn, Apinai;Pulkham, Jirayut;Chitsakul, Kitiphol;Sangworasil, Manas;Keawpoonsuk, Anucha;Songsataya, Kiettiwan
    • 제어로봇시스템학회:학술대회논문집
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    • 2005.06a
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    • pp.1907-1910
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    • 2005
  • Coating thickness is an important variable that plays a role in product quality, process control, and cost control. Measurement of film thickness can be done with many different instruments. In this paper, we introduce the new eddy current system for measure the thickness of nonconductive coatings on nonferrous metal substrates. The experimental results are shown that the proposed system is able to measure thickness of plastic film coating on aluminum plates in the range of 0 to 1000 microns with satisfy sensitivities, linearity, resolution and stability of the system.

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Anti-reflection Coating of Silicon Nitride Film for Solar Cell by RF Magnetron Sputtering (RF 마그네트론 스퍼터링을 이용한 태양전지용 질화 실리콘 반사방지막)

  • Choi, Kyoon;Choi, Eui-Seok;Hwang, Jin-Ha;Lee, Soo-Hong
    • Journal of the Korean Ceramic Society
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    • v.44 no.10
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    • pp.585-588
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    • 2007
  • Silicon nitride films for an anti-reflection coating were deposited on silicon via RF magnetron sputtering using a $Si_3N4$ target. The best result was obtained at the sputtering condition of 340 W RF power, 5 mtorr Ar atmosphere, $100^{\circ}C$ substrate temperature. The films showed 7.9% reflectance minimum with 2.35 refractive index. 0.21 absorption coefficient at 66.6 nm thickness. The surface morphology showed a smooth and dense film with good adhesion to silicon surface.

Simplified modeling of slide-fed curtain coating flow

  • Jung Hyun Wook;Lee Joo Sung;Hyun Jae Chun;Kim See Jo;Scriven L. E.
    • Korea-Australia Rheology Journal
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    • v.16 no.4
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    • pp.227-233
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    • 2004
  • Simplified model of slide-fed curtain coating flow has been developed and tested in this study. It rests on the sheet profile equations for curtain thickness in curtain flow and its trajectory derived by the integral momentum balance approach of Higgins and Scriven (1979) and Kistler (1983). It also draws on the film profile equation of film thickness variation in flow down a slide. The equations have been solved in finite difference approximation by Newton iteration with continuation. The results show that how inertia (Rey­nolds number), surface tension (capillary number), inclination angle of the slide, and air pressure difference across the curtain affect sheet trajectory and thickness profile. It has been revealed that approximate models can be useful to easily analyze coating flow dynamics without complex computations, giving qualitative agreement with full theory and with experiment.

Preparation of Barium Ferrite Thin Film by Sol-Gel Method (졸겔법을 이용한 바륨페라이트 박막 제조)

  • 변태봉;조원덕;김태옥
    • Journal of the Korean Ceramic Society
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    • v.34 no.1
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    • pp.37-44
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    • 1997
  • Barium ferrite thin films on the thermal oxidized Si substrate were prepared by using sol-gel method (dip coating) from the sol of composition ratio of 5.25, designated by mole ratio 2Fe/Ba. The gelation process was largely divided into 4 step, and the sol prepared by reaction for 90 minutes at 8$0^{\circ}C$ was the suit-able for coating. Needle shaped particles formed on the coating layer were placed parallel to substrate and the inclination was increased with film thickness. The easy-direction of magnetization of needle shaped par-ticles was long-axis direction.

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High-Precision Slot-Die Coating Machine for Thin Films of Flexible Display (플렉시블 디스플레이용 박막 도포를 위한 초정밀 슬롯다이 코팅장비)

  • Choi, Young-Man;Lee, Seung-Hyun;Jo, Jeongdai
    • Journal of the Korean Society for Precision Engineering
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    • v.31 no.6
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    • pp.491-495
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    • 2014
  • We developed a compact high-precision slot-die coating machine for thin-film deposition on a flexible substrate. For smooth and precise coating, air-bearing and linear motor system were employed to minimize velocity ripple. The gap control mechanism is specially designed to have repeatability of gap between nozzle and substrate under 1 ${\mu}m$. Due to extremely precise gap control, the machine can coat thin-films down to 50 nm with $200mm{\times}100mm$ size. A thin film of Ag nano-particle ink is coated for demonstration.