• Title/Summary/Keyword: calibration sensitivity

검색결과 383건 처리시간 0.023초

GC의 주입방식 차에 따른 고농도 악취황 성분의 검량오차 연구 : 주입부피의 고정방식 대비 주입농도의 고정방식 간 비교연구 (The Selection of Sample Injection Modes and Its Effect on the Calibration Bias in S Gas Detection by Gas Chromatography)

  • 김기현;최여진
    • 한국대기환경학회지
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    • 제21권2호
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    • pp.269-274
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    • 2005
  • In this work, analytical bias arising from the gas chromatographic determination of sulfur compounds was evaluated by the application of direct loop injection method to the GC/PFPD detection of four sulfur compounds including H$_{2}$S, CH$_{3}$SH, DMS, and DMDS. For the proper evaluation of analytical uncertainties involved in GC calibration, we employed two comparative techniques of calibration at fxed concentration injection (CFCI) vs calibration at fixed volume injection (CFVI) method. The results of our study indicate that CFCI method exhibits very poor sensitivity due to the matrix effect with varying injection volumes. On the other hand, as CFVI method overcomes such limitation, it can be used to obtain very accurate quantification of S compounds at their high concentration levels above a few to a few tens ppb.

가역원리에 의한 1인치 표준 컨덴서 마이크로폰의 정밀교정 (Precision Calibration of 1-Inch Standard Condenser Microphone by Reciprocity Technique)

  • 서상준;조문재
    • 한국음향학회지
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    • 제8권5호
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    • pp.23-32
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    • 1989
  • 표준 컨덴서 마이크로폰의 정밀 교정은 가역원리를 이용한 가역교정에 의해 이루어진다. 본 연구에서는 가역교정 중에서도 결합기를 이용하는 음압교정(pressure calibration)을 수행하여 세 개의 1인치 컨덴서 마이크로폰의 음압감도를 결정하였다. 마이크로본의 음압감도를 정밀하게 결정하기 위해서는 전압이나 결합기의 치수를 정밀하게 측정하여야 하며 결합기의 구조상 발생하는 제반 현상들에 대한 보정을 정확하게 해 주어야 한다. 이와같은 사항들을 정화하게 고려할 경우 가역교정에 의한 교정정밀도는 저주파와 중간 주파수 영역에서 0.05dB이며 10kHz 이상에서는 0.ldB가 된다.

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원자 현미경 탐침의 수평방향 힘 교정에 미치는 접촉 강성의 영향 (Effect of Contact Stiffness on Lateral Force Calibration of Atomic Force Microscopy Cantilever)

  • ;전기준;정구현
    • Tribology and Lubricants
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    • 제28권6호
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    • pp.289-296
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    • 2012
  • Atomic force microscopy (AFM) has been used for imaging surfaces and measuring surface forces at the nano-scale. Force calibration is important for the quantitative measurement of forces at the nano-scale using AFM. Normal force calibration is relatively straightforward, whereas the lateral force calibration is more complicated since the lateral stiffness of the cantilever is often comparable to the contact stiffness. In this work, the lateral force calibrations of the rectangular cantilever were performed using torsional Sader's method, thermal noise method, and wedge calibration method. The lateral optical lever sensitivity for the thermal noise method was determined from the friction loop under various normal forces as well. Experimental results showed that the discrepancies among the results of the different methods were as large as 30% due to the effect of the contact stiffness on the lateral force calibration of the cantilever used in this work. After correction for the effect of contact stiffness, all the calibration results agreed with each other, within experimental uncertainties.

Oxygen flooding에 의해 왜곡된 SIMS depth profile의 보정 (Correction of Secondary ion Mass Spectrometry depth profile distorted by oxygen flooding)

  • 이영진;정칠성;윤명노;이순영
    • 한국진공학회지
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    • 제10권2호
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    • pp.225-233
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    • 2001
  • Oxygen flooding을 이용한 Secondary ion Mass Spectrometry(SIMS) 분석에 있어서 표면에 산화막이 있을 때 발생하는 SIMS depth profile의 왜곡현상에 대한 원인을 분석하고 이를 보정하였다. 이러한 왜곡현상은 표면 산화막에서와 Si 매질에서의 sputter rate이 다른 데서 발생하는 깊이 보정 오류와 상대감도인자(relative sensitivity factor, RSF)가 다른 데서 발생하는 농도보정 오류로부터 발생됨이 밝혀졌다. 깊이보정 오류를 바로잡기 위하여 $N^a+$ 이온을 산화막과 Si 매질의 계면에 대한 marker로 사용하였으며 산화막 두께는 SEM 및 XPS로 측정하였다. 산화막과 Si 매질에서의 sputter rate 및 RSF의 차이는 주로 oxygen flooding이 유발한 산화막 형성시의 부피팽창에 의한 것으로 해석되었으며 이를 보정한 depth profile은 oxygen flooding없이 분석한 경우와 거의 동일한 결과를 보여주었다.

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헬멧형 뇌자도 장치의 센서 교정 (Sensor Calibration of a Helmet MEG System)

  • 권혁찬;김기웅;유권규;김진목;이용호
    • Progress in Superconductivity
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    • 제12권1호
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    • pp.57-61
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    • 2010
  • We have developed a whole-head MEG system for basic brain research and clinical application. The sensor system consists of a 152 SQUID gradiometer array oriented and located in a suitable way to cover a whole head of the human. The system measures magnetic fields generated by neuronal currents in the brain to get information on the brain activities. For this purpose, the field sensitivity determined by the position, orientation and geometry of the pickup coil as well as amplification factor of the electronic circuits should be known precisely. However, the position and orientation of the pickup coil might be changed from the designed specifications during cool down of the dewar and it is necessary to characterize the field sensitivity. In this study, we made calibration systems to determine the actual position and orientation of the 152 pickup coils and compared the localization results of the N100m source in the auditory cortex.

NGIS자료와 연계한 수질모의 결과의 자동보정 (Auto Calibration of Water Quality Modeling Using NGIS)

  • 한건연;이창희;김강모
    • 한국수자원학회:학술대회논문집
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    • 한국수자원학회 2004년도 학술발표회
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    • pp.1400-1403
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    • 2004
  • The current industrial development and the Increase of population along Nakdong River have produced a rapid Increase of wastewater discharge. This has resulted in problem of water quality control and management. Although many efforts have been carried out, water quality has not significantly improved. The goal of this study is to design a NGIS-based water quality management system for the scientific water quality control and management in the Nakdong River. For general water quality analysis, QULA2E model was applied to the Nakdong River. A sensitivity analysis was made to determine significant parameters and an optimization was made to estimate optimal values. The calibration and verification were performed by using observed water quality data for Nakdong River. A water qualify management system for Nakdong River was made by connecting the QUAL2E model to ArcView. It allows a Windows-based Graphic User Interface(GUI) to implement all operation with regard to water quality analysis. The modeling system in this study will be an efficient NGIS for planning of water quality management.

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실거리 파라미터 교정식 복합센서 기반 3차원 거리측정 시스템 (3D Depth Measurement System based on Parameter Calibration of the Mu1ti-Sensors)

  • 김종만;김원섭;황종선;김영민
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 영호남 합동 학술대회 및 춘계학술대회 논문집 센서 박막 기술교육
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    • pp.125-129
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    • 2006
  • The analysis of the depth measurement system with multi-sensors (laser, camera, mirror) has been done and the parameter calibration technique has been proposed. In the proposed depth measurement system, the laser beam is reflected to the object by the rotating mirror and again the position of the laser beam is observed through the same mirror by the camera. The depth of the object pointed by the laser beam is computed depending on the pixel position on the CCD. There involved several number of internal and external parameters such as inter-pixel distance, focal length, position and orientation of the system components in the depth measurement error. In this paper, it is shown through the error sensitivity analysis of the parameters that the most important parameters in the sense of error sources are the angle of the laser beam and the inter pixel distance.

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복합형 유역모델 STREAM의 개발(II): 모델의 시험 적용 (Development of a Hybrid Watershed Model STREAM: Test Application of the Model)

  • 조홍래;정의상;구본경
    • 한국물환경학회지
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    • 제31권5호
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    • pp.507-522
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    • 2015
  • In this study, some of the model verification results of STREAM (Spatio-Temporal River-basin Ecohydrology Analysis Model), a newly-developed hybrid watershed model, are presented for the runoff processes of nonpoint source pollution. For verification study of STREAM, the model was applied to a test watershed and a sensitivity analysis was also carried out for selected parameters. STREAM was applied to the Mankyung River Watershed to review the applicability of the model in the course of model calibration and validation against the stream flow discharge, suspended sediment discharge and some water quality items (TOC, TN, TP) measured at the watershed outlet. The model setup, simulation and data I/O modules worked as designed and both of the calibration and validation results showed good agreement between the simulated and the measured data sets: NSE over 0.7 and $R^2$ greater than 0.8. The simulation results also include the spatial distribution of runoff processes and watershed mass balance at the watershed scale. Additionally, the irrigation process of the model was examined in detail at reservoirs and paddy fields.

V 형상을 가지는 원자현미경 Cantilever의 정량적 마찰력 교정 (Quantitative Lateral Force Calibration of V-shaped AFM Cantilever)

  • 이희준;김광희;김현태;강보람;정구현
    • Tribology and Lubricants
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    • 제28권5호
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    • pp.203-211
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    • 2012
  • Atomic force microscopy (AFM) has been used as a tool, not only for imaging surfaces, but also for measuring surface forces and mechanical properties at the nano-scale. Force calibration is crucial for quantitatively measuring the forces that act between the AFM probe of a force sensing cantilever and a sample. In this work, the lateral force calibrations of a V-shaped cantilever were performed using the finite element method, multiple pivot loading, and thermal noise methods. As a result, it was shown that the multiple pivot loading method was appropriate for the lateral force calibration of a V-shaped cantilever. Further, through crosschecking of the abovementioned methods, it was concluded that the thermal noise method could be used for determining the lateral spring constants as long as the lateral deflection sensitivity was accurately determined. To obtain the lateral deflection sensitivity from the sticking portion of the friction loop, the contact stiffness should be taken into account.

지능형 자동 보정화 디지털 제어기 설계를 위한 퍼지 기법 (Fuzzy Methods for the design of Digital Controllers with Intelligent Calibration)

  • 나승유;박민상
    • 한국지능시스템학회:학술대회논문집
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    • 한국퍼지및지능시스템학회 1998년도 추계학술대회 학술발표 논문집
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    • pp.187-190
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    • 1998
  • The values of physical components of the plants and controllers as well as the relevant environmental conditions change in time, thus the output performance can be deteriorated during the operating span of the system. Naturally the duty of calibration or the prevention of performance deterioration due to excessive component sensitivity should be provided to the control system. The proposed controller, whenever necessary, measures the open-loop and close-loop characteristics, and then calculates the offset and sensor gain correction values based on the prepared standard measurements It is applied to the control of a flexible link system with the gain and offset calibration problems in the light sensor module for position to show the applicability. In this paper, we propose a digital controller which has the capability of calibration gain and offset adjustment using fuzzy methods.

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