• Tribology and Lubricants
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• 제29권3호
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• pp.160-166
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• 2013

There is an indispensable need for force calibration for quantitative nanoscale force measurement using atomic force microscopy. Calibrating the normal force is relatively straightforward, whereas doing so for the lateral force is often complicated because of the difficulty in determining the optical lever sensitivity. In particular, the lateral force calibration of a colloidal probe in a liquid environment often has a larger uncertainty as a result of the effects of the epoxy, the location of the colloidal particle on the cantilever, and a decrease in the quality factor. In this work, the lateral force of a colloidal probe using a reference cantilever with a known spring constant was calibrated in a liquid environment. By obtaining the spring constant and the lateral sensitivity at the equator of a spherical colloidal particle, the damage to the bottom surface of the colloidal particle could be eliminated. Further, it was shown that the effect of the contact stiffness on the determination of the lateral spring constant of the cantilever could be minimized. It was concluded that this method can be effectively used for the lateral force calibration of a colloidal probe in a liquid environment.

• 한국환경과학회지
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• 제4권1호
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• pp.91-103
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• 1995

The reaction rate, equilibrium, and flow injection analysis methods were fundamentally evaluated for the determination of aqueous ammonia. The selected indophenol blue method was based on the formation of indophenol blue in which ammonium ion reacted with hypochlorite and phenol in alkaline solution. In the optimized reaction condition, the reaction followed 1st order reaction kinetics and the final product was stable. The absorbance measurements before and after the equilibrium were utilized for the reaction rate and equilibrium methods. The reaction rate methods, based on the relative analytical signals for the possibility of eliminating interferents, were shown to have good linear calibration curves but the detection limit and the calibration sensitivity were poorer than those in the equilibrium method. The detection limits were 32-49 pub and 24 pub for the reaction rate and equilibrium methods, respectively In the flow injection analysis, the absorbance was measured before the equilibrium reached and thus resulted in 30% reduction of calibration sensitivity. However, the detection limit was 11 ppb, indicating that the peak-to-peak noise for the blank was remarkably improved. Compared to the manual methods, the optimized experimental condition in a closed reaction system reduced the blank absorbance and the inclusion of ammonia from the atmosphere was prevented. In addition, highly reproducible mixing of sample and reagents and analytical data extracted from continuous recording showed excellent reproducibility.

• 제어로봇시스템학회논문지
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• 제5권2호
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• pp.200-207
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• 1999

In this paper, a precise sensitivity measurement system of ultrasonic transducer in the frequency range from 1 MHz to 15 MHz, which can implement the reciprocity principle is constructed. All of the elements of this system such as the ultrasonic preamplifier, ultrasonic absorber, water tank, water degassing system, and four-axes translator and reflector are constructed. For the performance evaluation of the calibration system, a standard hydrophone precisely calibrated from PTB(Physikalisch Technische Bundesanstalt) in Germany are used. And the system parameters which affected the evaluation of the measurement accuracy and the reproducibility in various measuring conditions are considered. The measurement uncertainty of the calibration system is estimated within $\pm$ 2.0㏈.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 1998년도 추계종합학술대회 논문집
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• pp.413-416
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• 1998

Sensitivity and calibration considerations are most important in the design and implementation of real control systems. Ideally parameter changes due to various causes should not appreciably affect the system's performances. But all the values of physical components of the plants and controllers as well as the relevant environmental conditions change in time, thus the output performance can be deteriorated during the operating span of the system. Naturally the duty of calibration or the prevention of performance deterioration due to excessive component sensitivity should be provided to the control system. In this paper, we propose a digital controller which has the capability of calibration and gain adjustment as well as the execution of control law. Specifically the problems of gain adjustment and offset calibration in the light source and CdS sensor module for position measurement in a flexible link system are considerably resolved. The parameters of measurement module are prone to change due to environmental brightness conditions resulting in poor steady state performance of the overall control system. Thus a proper method is necessary to provide correction to the changed values of gain and offset in the position measurement module. The proposed controller, whenever necessary, measures the open-loop characteristics, andthen calculates the offset and sensor gain correction values based on the prepared standard measurements. It is applied to the control of a flexible link system with the gain and offset calibration porblems in the light sensor module for position to show the applicability.

• 한국군사과학기술학회지
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• 제12권4호
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• pp.491-499
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• 2009

The determination of response characteristics for pressure sensors is routinely limited to static calibration against a deadweight pressure standard. The strength of this method is that the deadweight device is a primary standard used to generate precise pressure. Its weakness lies in the assumption that the static and dynamic responses of the sensor in question are equivalent. Differences in sensor response to static and dynamic events, however, can lead to serious measurement errors. Dynamic techniques are required to calibrate pressure sensors measuring dynamic events in milliseconds. In this paper, a dynamic calibration using negative going dynamic pressure is proposed to determine dynamic pressure response for piezoelectric sensors. Sensitivity and linearity of sensor by the dynamic calibration were compared with those by the static calibration. The uncertainty of calibration results and the goodness of fit test of linear regression analysis were presented. The results show that the dynamic calibration is applicable to determine dynamic pressure response for piezoelectric sensors.

• Nuclear Engineering and Technology
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• 제42권2호
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• pp.219-230
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• 2010

In nuclear power plants (NPPs), periodic sensor calibrations are required to assure that sensors are operating correctly. By checking the sensor's operating status at every fuel outage, faulty sensors may remain undetected for periods of up to 24 months. Moreover, typically, only a few faulty sensors are found to be calibrated. For the safe operation of NPP and the reduction of unnecessary calibration, on-line instrument calibration monitoring is needed. In this study, principal component-based auto-associative support vector regression (PCSVR) using response surface methodology (RSM) is proposed for the sensor signal validation of NPPs. This paper describes the design of a PCSVR-based sensor validation system for a power generation system. RSM is employed to determine the optimal values of SVR hyperparameters and is compared to the genetic algorithm (GA). The proposed PCSVR model is confirmed with the actual plant data of Kori Nuclear Power Plant Unit 3 and is compared with the Auto-Associative support vector regression (AASVR) and the auto-associative neural network (AANN) model. The auto-sensitivity of AASVR is improved by around six times by using a PCA, resulting in good detection of sensor drift. Compared to AANN, accuracy and cross-sensitivity are better while the auto-sensitivity is almost the same. Meanwhile, the proposed RSM for the optimization of the PCSVR algorithm performs even better in terms of accuracy, auto-sensitivity, and averaged maximum error, except in averaged RMS error, and this method is much more time efficient compared to the conventional GA method.

• 유체기계공업학회:학술대회논문집
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• 유체기계공업학회 2000년도 유체기계 연구개발 발표회 논문집
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• pp.193-199
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• 2000

The effects of Reynolds number on the non-nulling calibration of a cone-type five-hole probe in low-speed flows have been investigated at the Reynolds numbers of $2.04{\times}10^3,\;4.09{\times}10^3$, and $6.13{\times}10^3$. The calibration is conducted at the pitch and yaw angles in ranges between -35 degrees and 35 degrees with an angle interval of 5 degrees. The result shows that each calibration coefficient, in general, is a function of the pitch and yaw angles, so that the pre-existing calibration data in a nulling mode are not enough in accounting for the full non-nulling calibration characteristics. Due to the interference of the probe stem, the calibration coefficients have more Reynolds number sensitivity at positive pitch angles than at negative ones.

• 한국정밀공학회지
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• 제32권2호
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• pp.185-190
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• 2015

This paper presents a new method to determine sensitivity coefficients of temperature and humidity of torque transducers by using a natural and seasonal variation of ambient conditions at the laboratory. We had measured the sensitivities of the torque transducers over almost one year using the KRISS 2 kN m torque standard machine. The sensitivity data acquired at various ambient conditions were processed using our measurement model to extract the sensitivity coefficients of temperature and humidity simultaneously with high precision. A comparison with a previous method using an environmental control chamber was carried out to test the feasibility of using our new method. Two results agreed within the uncertainty. We revealed that the torque measuring errors could be 8 times higher than the measurement and calibration capability of KRISS torque standard machine if the sensitivity changes due to the temperature and humidity are not properly corrected during a calibration.

• 한국진공학회지
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• 제16권2호
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• pp.91-98
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• 2007

한국표준과학연구원 진공기술센터에서 잔류기체분석기 교정장치를 개발하였으며, 이 장치를 이용하여 서로 다른 구조를 가진 두개의 사중극 질량분석기 (quadrupole mass spectrometer)의 질소, 아르곤, 헬륨에 대한 기체감도를 측정하였다. 그 결과 기체감도는 QMS 구조와 상관없이 기체의 질량이 클수록 높게 나타났고 압력에 따라서도 다른 특성을 보였으므로 정확한 사용을 위해서는 기체감도를 꼭 보정해야 함을 알 수 있었다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 춘계학술대회
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• pp.1364-1369
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• 2004

New method for the design, fabrication, and calibration of micro-machined heat flux sensor has been developed. Two types of micro-machined heat flux sensor having different thicknesses of the thermal-resistance layer are fabricated using the MEMS technique. Photo-resist patterning using a chrome mask, bulk-etching and copper-nickel sputtering using a shadow mask are applied to make heat flux sensors, which are calibrated in the convection-type heat flux calibration facility. The sensitivity of the device varies with thermal-resistance layer, and hence can be used to measure the heat flux in heat-transfer phenomena.