• 한국자기학회:학술대회 개요집
• /
• 한국자기학회 2002년도 춘계연구발표회 논문개요집
• /
• pp.102-102
• /
• 2002

• 열처리공학회지
• /
• 제30권3호
• /
• pp.106-112
• /
• 2017

In this study dual-phase steels with different ferrite grain size and martensite fraction were fabricated by varying micro-alloying elements and intercritical anneling temperatures, and then the tensile properties were investigated in terms of yield and tensile strengths, elongation, and yield ratio. The addition of micro-alloying elements reduced ferrite grain size, and the increased intercritial transformation tempeature increased the martensite fracton. The tensile test results showed that yield and tensile strengths of all the steel specimens increased with increasing the martensite fraction. However, the elongation and yield ratio were differently changed according to variations in the morphology and carbon content of martensite, ferrite grain size, and precipitates resulting from the addition of micro-alloying elements and intercritical annealing.

• 한국분말재료학회지
• /
• 제18권6호
• /
• pp.496-501
• /
• 2011

In this study, the effect of milling time on the microstructure and phase transformation behaviors of Ni-12 wt.%B powders was investigated using vibratory ball milling process. X-ray diffraction patterns showed that the phase transformation of mixed Ni-B elemental powder occurred after 50 hours of milling, with a formation of nickel boride phases. Through the study of microstructures in mechanical alloying process, it was considered that ball milling strongly accelerates solid-state diffusions of the Ni and B atoms during mechanical alloying process. The results of X-ray photoelectron spectroscopy showed that most of B atoms in the powder were linked to Ni with a formation of nickel boride phases after 200 hours of milling. It was finally concluded that mechanical alloying using ball milling process is feasible to synthesize fine and uniform nickel boride powders.

• 한국주조공학회지
• /
• 제18권6호
• /
• pp.563-569
• /
• 1998

A Study on microstructure and elevated temperature strength of 18Cr-2Mo ferritic stainless steel castings strengthened by alloying small amounts of titanium and carbon, has been conducted. The morphology of titanium carbides showed spherical in shape and their distribution depended on the amount of alloying elements. Maximum density ($7{\times}10^5/cm^2$) of titanium carbides has been formed in the alloy containing 2.0 wt.% titanium and 0.5 wt.% carbon as alloying elements and the size of carbide particles is in the range of 0.5 to $3.0\;{\mu}m$. High temperature tensile and fatigue strength of this alloy were the highest among the alloys tested in this research. The fracture mode of the alloys containing alloying elements less that 2.0 wt.% titanium and 0.5 wt.% carbon showed intercrystalline fracture at room temperature, while the alloys containing higher amounts of alloying elements showed transcrystalline fracture. All of the alloys showed creep or ductile rupture mode at elevated temperature.

• 한국재료학회지
• /
• 제26권10호
• /
• pp.535-541
• /
• 2016

The present study deals with the effects of micro-alloying elements such as Ni, V, and Ti on the recrystallization behavior of carbon steels at different strain rates. Eight steel specimens were fabricated by varying the chemical composition and reheating temperature; then, a high-temperature compressive deformation test was conducted in order to investigate the relationship of the microstructure and the recrystallization behavior. The specimens containing micro-alloying elements had smaller prior austenite grain sizes than those of the other specimens, presumably due to the pinning effect of the formation of carbonitrides and AlN precipitates at the austenite grain boundaries. The high-temperature compressive deformation test results indicate that dynamic recrystallization behavior was suppressed in the specimens with micro-alloying elements, particularly at increased strain rate, because of the pinning effect of precipitates, grain boundary dragging and lattice misfit effects of solute atoms, although the strength increased with increasing strain rate.

• 동력기계공학회지
• /
• 제15권2호
• /
• pp.42-48
• /
• 2011

440A martensitic stainless steels which were modified with reduced carbon content(~0.5%) and addition of small amount of nickel, vanadium, tungsten and molybdenum were manufactured. Effects of alloying elements and tempering temperatures on the uniform corrosion in the solution of lN H2S04 were investigated through the electrochemical polarization test. When tempering temperature is constant, corrosion current density in active-passive transition point, Icorr, decreased a little with an increase of austenitizing temperature. In addition to this, when austenitizing temperature is constant, longer holding time showed a little lower Icorr and Ipass, passive current density. And when austenitized at $1050^{\circ}C$ and tempered in a range of $350{\sim}750^{\circ}C$, best anti-corrosion properties were obtained at $350^{\circ}C$ tempering temperature while worst at $450^{\circ}C$ or $550^{\circ}C$. The specimens tempered at below $450^{\circ}C$ and above $550^{\circ}C$, similar and good anti-corrosion characteristics were obtained regardless of alloying elements added, showing anti-corrosion characteristics are influenced more by tempering temperature than by alloying elements.

• 한국분말재료학회지
• /
• 제12권3호
• /
• pp.179-185
• /
• 2005

As the electrodes of secondary battery are made with sulfur compounds, excellent electrode system of environmental non-toxicity, high specific energy density and low material cost can be obtained. In this study, the $FeS_2$ fine compound powders for active material in the battery were synthesized by mechanical alloying. Fine Fe-53.5 wt.%S powders of 450 nm of mean size were fabricated by mechanical alloying for 60 hours at the horizontal attritor. As the mechanical alloying time increases, particle size of Fe-53.5 wt.%S was decreased and steady state of Fe-53.5 wt.%S compound powders was obtained at 30 hours. Fe-53.5 wt.%S cathode shows the excellent discharge capacity (1011 mAh/g).

• 한국분말재료학회지
• /
• 제12권1호
• /
• pp.70-78
• /
• 2005

Mechanical alloying using high-energy ball mill and subsequent spark plasma sintering (SPS) process was applied to understand mechanical alloying processing of Al-Fe alloy system. The thermal stability of mechanically alloyed Al-Fe alloy was intended to be enhanced by SPS process. Various analytical techniques including particle size analysis, density measurement, micro-Vickers hardness test, SEM, TEM, and X-ray diffractometry were adopted to find optimum processing conditions for mechanical alloying and subsequent SPS and to estimate thermal stability of the prepared alloy. It was found from the treatment of mechanically alloyed Al-8wt.%Fe powder mixture that needle-shaped $Al_3Fe$ precipitates was formed in the Al-Fe matrix, and the alloy compact showed enhanced densification and reached its full density with little loss of its fine microstructure. After heat treatment at $500^{\circC}$, it was also shown that the thermal stability of Al-8wt.%Fe alloy fabricated in the present study was enhanced, which was due to its fine microstructure developed by fast densification of SPS.

• 한국주조공학회지
• /
• 제28권6호
• /
• pp.273-281
• /
• 2008

Effects of alloying elements on the mechanical properties of hardened and austempered 3.60wt%C - 2.50wt%C ductile cast iron were investigated. Strength and hardness were increased and ductility was decreased as the amount of alloying element increased. The increasing effect of copper addition on the strength was the most pronounced. The strength and hardness were greatly increased and ductility was decreased by hardening. The effect of alloying element on the mechanical properties of the hardened ductile cast iron was not so pronounced due to the high contents of C and Si. The strength and hardness of austempered ductile cast iron were greatly increased, meanwhile the difference of strength from that of hardened one was not so big. The ductility of the former was higher than that of the latter. The strength and ductility of austempered ductile cast iron with 0.25%Mn were the maximum of all Mn added ones. The maximum strength of that was obtained with the addition of 0.80wt%Cu or 2.00wt%Ni along with this amount of Mn added.

• 한국수소및신에너지학회논문집
• /
• 제16권4호
• /
• pp.372-378
• /
• 2005

Ni/YSZ ($Y_2O_3$-stabilized $ZrO_2$) composite powder for a cathode material in high temperature electrolysis(HTE) was synthesized by a mechanical alloying method with Ni and YSZ powder. Microstructure of the composite and cell thickness for HTE reaction has been analyzed with various techniques of XRD, SEM to investigate effects of fabrication conditions. Employing the composite material, furthermore, the unit cell for HTE has been studied to evolve hydrogen from water. XRD patterns showed that the composites after wet mechanical alloying were composed of respective nano-sized crystalline Ni and YSZ. While ethanol as additive for mechanical alloying increased to $20\;{\mu}m$ of average particle size of the composites, alpha-terpineol effectively decreased to sub-micro size of that. This study has been found out the evolution of hydrogen by HTE reaction employing the fabricated cathode material, showing 1.4 ml/min of $H_2$ generation rate as increasing $20\;{\mu}m$ of cathode thickness.