• YAKHAK HOEJI
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• v.21 no.2
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• pp.101-109
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• 1977

The effect of humidity on the aging process of hydrous aluminum oxide prepared by the reaction of aluminum chloride and sodium bicarbonate solution at pH 7.8, which was then kept in various atmosphere under relative humidity at 37.deg. was observed by the measurements of acid consuming capacity, X-ray diffraction and IR absorption. The humidity was one of the important factors influencing the aging process of hydrous aluminum oxide during storage. The higer the humidity, the more was accelerated age, crystalize and loss in acid reactivity. Depending on the humidity, the aging product was different, especially, in the case of up to the relative humidity of 72%, it forming bayerite. On the other hand, the hydrous aluminum oxide aged below the relative humidity of 50% was still amorphous even after 120 days storage. When hydrous aluminum oxide was aged under higher humidity, definite IR absorption bands develop as the hydroxys become part of an ordered structure, and it showed their characteristic absorption band around 1630 and 1060 cm$^{-1}$.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.60 no.2
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• pp.338-343
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• 2011

In this paper, the FT-IR, conductivity and flow electrification phenomena of Vegetable oils were discussed. Vegetable oil has high flash point and eco-friendly properties compared to conventional mineral oil. Accelerated aging transformer oil samples produced in the oven at 140[$^{\circ}C$] for 500 hours, 1000 hours, 1500 hours, 2000 hours. Serial device to measure the flow electrification phenomena was designed and fabricated. Pico ammeter and the Labview data measurements were utilized. The effects of Temperature and antistatic agent on fluid flow electrification were investigated. Both Mineral and vegetable oil showed similar trends for temperature change. The polarity reversal occurred in mineral oil with antistatic agent above 10 ~ 30[ppm] and in vegetable oil with antistatic agent above 5[ppm].

• Journal of the Korea Academia-Industrial cooperation Society
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• v.6 no.4
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• pp.285-290
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• 2005

Mechanical properties of rubber mat are influenced by many factors such as compounding ingredients and states of cure, process of rubber, and fillers. Our study aim is to investigate influence of N-isopropyl-N'-chloro-P-phenylene diamine antioxidant on the thermal aging and ozone cracking. In this work, the degradation of antiblastic rubber mat was studied and suggested mechanism to involve two-types of degradation, thermal-aging and ozone-cracking both of which can be contained antioxidant or non-antioxidant.

• Elastomers and Composites
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• v.57 no.4
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• pp.165-174
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• 2022

The effect of fumed silica loading on the thermal stability and mechanical properties of fluorosilicone (FVMQ) rubber was investigated. The distribution of fumed silica inside FVMQ was characterized using scanning electron microscopy, and the thermal stability of composites was evaluated using thermogravimetric analysis and by the changes in mechanical performance during thermo-oxidative aging. The function mechanism of fumed silica was studied by Fourier transform infrared spectroscopy. The results show that with increasing silica content, the crosslink density of composites, the modulus at 100%, and tensile strength also increased, whereas the elongation at break decreased. Furthermore, increasing the silica content of composites increased the initial decomposition temperature (T_d) and residual weight of the composite after exposure to nitrogen. In addition, the thermal oxidative aging experiment demonstrated improved aging resistance of the FVMQ composites, including lower change in tensile strength, elongation at break, and modulus at 100%.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2023.11a
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• pp.91-92
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• 2023

In this study, the chemical composition of converter slag according to CO₂ nanobubble promotion aging time was examined. The CO₂ nanobubble water immersion time was 0, 12, 24, 36, 48 hours, and then dried and pulverized to perform XRD analysis. As a result, the longer the sample was immersed in CO₂ nanobubble water, the higher the amount of calcite produced, and the change after 36 hours was minimal.

• Proceedings of the Korea Concrete Institute Conference
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• 1998.10c
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• pp.72-75
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• 1998

In this study, we investigate the difference of concrete between natural aggregate and electric are furnace(EAF) slag one in oder to use EAF slag aggregate as coarse aggregate in concrete. We find the physical and chemical properties of EAF slag aggregate for the aging process. We consider the properties od the concrete made with EAF slag aggregate which are compressive strength, splitting tensile strength and modulus of elasticity.

• Proceedings of the Korea Concrete Institute Conference
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• 1991.10a
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• pp.1-4
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• 1991

Relationship between againg and characteristic change of asphalt is not well known through asphalt rheolopy. Therefore, this study was conducted to evaluate characteristic change of asphalt cement due to againg based on experimental results of chromatogram and selected physical properties. Currently, three virgin asphalt cements were tested for physical properties and chromatograms before and after artificially conditioning for againg. Results in the current study showed that againg caused significant changes of physical properties and increase of larger size molecules and approximately corresponding reduction of smaller size molecule in asphalt cement molecular size distribution.

• Elastomers and Composites
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• v.6 no.2
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• pp.73-79
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• 1971

As a series of the studies of EPDM-Polymer blends, the experiments are concentrated to the investigation of the physical properties of the EPDM-SBR blends. The results are shown as follows: 1. Tensile strength decreased with increase in EPDM contents and the decreasing value was good results than NR blending. 2. It was found that the aging were much improved after blending and experiments data was good results than NR blending.

• The Korean Journal of Food And Nutrition
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• v.22 no.4
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• pp.548-553
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• 2009

Qualitative properties- polyphenol compounds(total phenolics, anthocyanin, flavonoids, tannins), color parameters and antioxidant activities- of wild grape wine having different aging periods were studied. The contents of total phenolics and anthocyanin decreased significantly in accordance with aging terms(p<0.05). The total phenolics and anthocyanin of the oldest wine(WG3) represented only 43% and 45% of it's related compound in the wine aged for one year(WG1), respectively. The contents and the degree of polymerization of tannins, including condensed tannins, also decreased but not showed statistically significant. However, The contents of flavonoids of the 2 year old wine(WG2) decreased significantly related to that of WG1, remaining, then, almost constant at that levels during aging. The L* values, b(yellow) values and the hue (hab) values were increased in long aged wines(WG2, WG3), while the intensity of color(CI) and, the a(red) parameter value decreased. The antiradical activity of wild grape wines was shown to be high(87 EDA%) in WG1. The corresponding coefficient of tannin concentrations with antiradical activity($r^2$=0.9189) suggests that the tannin content may be strongly related to the antioxidant properties of wild grape wines.

• Journal of the Korean Institute of Gas
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• v.16 no.6
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• pp.115-122
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• 2012

Polyurethane foams were synthesized with different contents and kinds of catalysts to know change of properties under various NCO index. UTM(universal testing machine), DSC(differential scanning calorimetry), SEM(scanning electron microscope) and FT-IR(Fourier transform spectroscopy) were used for studying the PUF's physical properties change. Compressive strength of PUF increased with increasing contents of catalyst. Glass transition temperature(Tg) and compressive strength of PUF using PC-8 and 33LV catalyst, increased with increasing NCO index at the aging. According to the results of Infrared spectral analysis, reduction of NCO peak was found in gelling catalyst, because unreacted NCO reacted with polyurethane. Although Tg and compressive strength of PUF using TMR-2, unchanged with increasing NCO index at the aging, because trimerization of isocyanate.