• Transactions on Electrical and Electronic Materials
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• v.11 no.5
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• pp.216-221
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• 2010

The microstructure, electrical properties, and DC-accelerated aging behavior of the Zn-Pr-Co-Cr-Y-Er (ZPCC-YE) varistors were investigated for different amounts of erbium oxide ($Er_2O_3$). The microstructure consisted of zinc oxide grain and an intergranular layer ($Pr_6O_{11}$, $Y_2O_3$, and $Er_2O_3$-rich phase) as a secondary phase. The increase of $Er_2O_3$ amount decreased the average grain size and increased the sintered density. As the $Er_2O_3$ amount increased, the breakdown field increased from 5094 V/cm to 6966 V/cm and the nonlinear coefficient increased from 27.8 to 45.1. The ZPCC-YE varistors added with 0.5 to 1.0 mol% $Er_2O_3$ are appropriate for high voltage, with high nonlinearity and stability against DC-accelerated aging stress.

• Journal of Korea Foundry Society
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• v.31 no.6
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• pp.366-370
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• 2011

The influence of aging treatment on the microstructure, mechanical and electrical properties of Cu-Be alloy for connector material applications was investigated. The properties of mechanical strength and electrical conductivity were found to increase with increasing aging temperature. By the way, SEM/EDS and TEM analysis exhibited that beryllides precipitation (CoBe and NiBe) with a size of 50 nm were distributed in grains. It was, therefore concluded that these beryllide precipitates improved the mechanical strength and also it was favor in increasing of electrical conductivity.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2001.11b
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• pp.255-257
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• 2001

In this paper, the silicon rubber insulator for transmission line was experimented for 1,000 hours aging test in salt-fog condition. To evaluate and examine the aging properties of silicon rubber insulator for test, the leakage current of surface was measured. Also hydrophobicity and scanning electron microscopy were compared with initial and aged sample respectively. Above results, we can confirm that the surface properties of silicon rubber insulator easily aged by salt-fog condition.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.11a
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• pp.479-482
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• 1999

Cured epoxy resins are extensively used for the electrical insulation in high-voltage equipments. The bisphenol A-based epoxy resins lured with azine show, especially, good thermal properties and mechanical resistances. For the technical and economic reasons, varing amount of inorganic fillers are added to endow the required special properties. In the large generators and motors of power plants, epoxy insulation is disclosed to the harsh conditions like the superheated steam and abrupt temperature variation. Hygrothermal aging at elevated temperatures tends to induce degradation in epoxy resins. To predict the effect of this degradation in DGEBA/MDA/SN/zeolite system, we proceeded the forced moisture absorption experiment using the autoclave. The thermal properties of the untreated and treated specimens were analyzed by DSC and TGA under the nitrogen flowing condition. The moisture absorption results showed a weight increase during hygrothermal aging at 1207. At the initial aging period, the system leaded to more or less postcuring but more prolonged environmental aging leaded the discoloration of specimen and lowering the T$_{g}$./.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.24 no.10
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• pp.803-806
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• 2011

1 mol% $Li_2O$ excess $0.9(Na_{0.52}K_{0.48})NbO_3-0.1LiTaO_3$ lead-free piezoelectric multilayer ceramic actuators were investigated to determine their aging properties. To reduce the thermal aging behavior, we applied a rectified unipolar electric field of 5 kV/mm to the specimen to accelerate the electric aging behavior. By employing a rectified unipolar electric field for the piezoelectric actuators, we could remove undesirable heating from the relaxation current in the motion of the ferroelectric domain. To accelerate the aging test, the applied electric fields had a frequency of 900 Hz. To have enough time for charging and discharging, we employed an accurate time constant to design the equivalent circuit model for the aging tester. To extract exact aging behavior, we measured the pseudo-piezoelectric coefficient before and after the aging process. We also measured the electro-mechanical coupling coefficient, the frequency-dependent dielectric permittivity, and the impedance to compare with fresh and aged specimen.

• Journal of the Korean Society for Heat Treatment
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• v.4 no.1
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• pp.30-36
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• 1991

Effects of aging treatment on the mechanical properties of a 18 Ni maraging steel were investigated by considering the reverted austenite. Specimens were heat treated by austenitizing at $840^{\circ}C$ for 1 hr and then aged for various times at $480^{\circ}C$ and $520^{\circ}C$. The main results obtained are as follows : 1) The amounts of reverted austenite are increased up to about 4% at $480^{\circ}C$ and about 22% at $520^{\circ}C$ with 1 to 48 hrs aging time. 2) Decreasing tendencies of impact energy and fracture toughness with increasing aging time are diminished after aging for 2 hrs at two aging temperatures of $480^{\circ}C$ and $520^{\circ}C$. 3) Peak hardness and yield strength are obtained after aging for 4 hrs at $480^{\circ}C$ and 2 hrs at $520^{\circ}C$ respectively. From the above results, it was concluded that the optimum aging condition with which showed good strength and toughness combination are given to be $480^{\circ}C$ for 4 hrs and $520^{\circ}C$ for 2 hrs.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.16 no.12
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• pp.1136-1141
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• 2003

The primary insulation materials used in an oil filled transformer are kraft paper, wood, porcelain and oil. Modern transformers use chemically treated paper to improve its tensile strength and resistance to aging caused by immersion in oil. But these insulation papers are mainly aged by thermal stress. Over the life time of the insulation paper and oil, it is exposed to high temperatures, oxygen and water. Its interaction with the steel of the tank and core plus the copper and aluminium of the windings will eventually cause the chemical properties of the oil to decay. High temperature have an effect on mechanical strength of cellulous paper used in the layer insulation. We made two aging cells in which insulation papers and mineral oil are conducted to test thermal properties. It is measured dielectric strength, number of acid, moisture, etc. of insulation paper and oil aged in the aging cells.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.5
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• pp.1372-1381
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• 1996

As recieved boiler tuve steel was aged artificially at $650^{\circ}C$ and$690^{\circ}C$ for various time duration to simulate the material deterioration which could be occurred during the operation of fossiol power plants. And the tensile tests, the microhardness tests and the characterization of carbides formed in the aging process were performed to asses the relationship between the mechanical properties and the effect of thermal aging. Furthernore, the amout of Mo-rich carbide were investigated by ondestructive method by noticing the fact that formation of Mo-rich carbide were investigated by ondestructive melthod by noticing the fact that formation of Mo-rich carbides($Mo_6C$) which stabilizes lastly affects the mechanical properties. It was known that the microhardness results of service exposed materials were similar to the ones which are aged at $650^{\circ}C$. The room temperature measurement showed small variation in the yield points and ultimate strength in materials aged at $650^{\circ}C$. Those properties at $540^{\circ}C$ showed the abrupt decrease compared with as received material even if short aging time. And it was found that $650^{\circ}C$ $690^{\circ}C$ aging cause different effects on mechanical properties, although the temperature time parameters(LMP;Larson-Miller parameter) are same. And it was concluded that the aigng at $650^{\circ}C$ is more appropriate to simulate the service exposed condition. Finally, the relationship between high temperature tensile properties and Ip values were established, which offers a potential way of reliability tests onthe power plant components.

• Journal of the Korean Society of Propulsion Engineers
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• v.22 no.1
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• pp.66-71
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• 2018

The evaluation of the shelf-life of energetic materials is important. However, there are several difficulties associated with the evaluation. First, aging experiments require a considerable amount of time. Second, treating highly energetic materials is dangerous. For these reasons, many evaluation methods have been developed. Because most energetic materials decompose with the evolution of heat, it is important to analyze the thermal properties of energetic materials in order to understand decomposition and aging properties. In this paper, we describe the estimation of thermal aging properties and develop a kinetic model from spot data set of mechanical properties and estimate aging properties for mechanical results.

• Korean Journal of Materials Research
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• v.34 no.3
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• pp.175-183
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• 2024

Geopolymer, also known as alkali aluminum silicate, is used as a substitute for Portland cement, and it is also used as a binder because of its good adhesive properties and heat resistance. Since Davidovits developed Geopolymer matrix composites (GMCs) based on the binder properties of geopolymer, they have been utilized as flame exhaust ducts and aircraft fire protection materials. Geopolymer structures are formed through hydrolysis and dehydration reactions, and their physical properties can be influenced by reaction conditions such as concentration, reaction time, and temperature. The aim of this study is to examine the effects of silica size and aging time on the mechanical properties of composites. Commercial water glass and kaolin were used to synthesize geopolymers, and two types of silica powder were added to increase the silicon content. Using carbon fiber mats, a fiber-reinforced composite material was fabricated using the hand lay-up method. Spectroscopy was used to confirm polymerization, aging effects, and heat treatment, and composite materials were used to measure flexural strength. As a result, it was confirmed that the longer time aging and use of nano-sized silica particles were helpful in improving the mechanical properties of the geopolymer matrix composite.