• Title/Summary/Keyword: adhesive performance

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Evaluation of Shear Bond Strength and Microleakage of Self-adhesive Giomer

  • Gwangsuk Kim;Juhyun Lee;Haeni Kim;Howon Park
    • Journal of the korean academy of Pediatric Dentistry
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    • v.50 no.4
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    • pp.434-442
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    • 2023
  • This study was aimed to evaluate the bonding performance of a self-adhesive giomer and compare it to a conventional flowable composite resin with regard to shear bond strength and microleakage in enamel and dentin. Healthy human premolars extracted for orthodontic treatments were used in the study. For shear bond strength tests, enamel and dentin specimens were prepared for the study group with self-adhesive giomer and for the control group with conventional flowable composite resin with a 5th-generation adhesive system. A universal testing machine was used to measure the shear bond strength. For the microleakage tests, specimens were immersed in a 2% methylene blue solution for 24 hours, cut into sections, and evaluated with a stereomicroscope for the extent of dye penetration. The results of the study showed no statistically significant difference in shear bond strength between the self-adhesive giomer and the conventional flowable composite resin in enamel (p = 0.091). On the contrary, in dentin, the self-adhesive giomer showed significantly lower shear bond strength (p < 0.0001). The microleakage of the self-adhesive giomer was significantly higher than that of the conventional flowable composite resin (p = 0.002). Self-adhesive giomer is considered useful for restoring small cavities at the enamel level of pediatric patients by reducing chair time with the advantage of a simple bonding process. However, as the study was conducted in a laboratory setting, further research in a clinical environment is deemed necessary.

Shear Performance Evaluation of Composite Thermal Insulation with Quasi-Non-Combustible according to Adhesive Type (부착 유형에 따른 준불연 복합단열판 전단성능평가)

  • Choi, Ki-Sun;Oh, Keunyeong;Park, Keum-Sung;Ha, Soo-Kyung
    • Journal of the Korea Institute of Building Construction
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    • v.22 no.5
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    • pp.507-518
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    • 2022
  • The purpose of this research is to obtain experimental data for developing a structural design of an external insulation system by evaluating the shear performance of a composite insulation system according to the adhesive type. The shear performance of the composite insulation system was experimentally evaluated by considering a simultaneous placement method, full and spot/edge coverage using adhesive mortar. As a result of the test, the shear strength of simultaneous placement and full coverage method was almost similar, the spot/edge coverage method was about 80% of them. Also, the simultaneous placement method is considered to be constructively advantageous when applied as an external insulation system to a high-rise building compared to using an adhesive mortar.

Partial Purification of Mussel Adhesive Protein for Mytilus Edulis and Preparation of Mussel Protein Hydrolysates

  • Sun, Nam-Kyu;Song, Kyung-Bin
    • Preventive Nutrition and Food Science
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    • v.5 no.3
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    • pp.148-152
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    • 2000
  • Mussel adhesive protein (MAP) was extracted from Korean Mytilus edulis and then partially purified using Sephacryl S-300 gel permeation chromatography and reversed-phase high performance liquid chromatography. As an indicator of adhesiveness, is 3,4-dihydroxyphenylalanine (DOPA) content was determined. Its DOPA/protein ratio of 0.19 was higher than those of other reports, indicating a good adhesive. The partially purified MAP was confirmed by acid-urea polyacrylamide gel electrophoresis using cetylpiridinium bromide as a cationic detergent. Sea mussel hydrolysates were prepared using three commercial proteases to provide value-added functional materials and their angiotensin converting enzyme (ACE) inhibitory activities were determined. Among hydrolysates of sea mussel, Protamex was the best and further purification would improved ACE inhibitory activity.

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Ashpalt 2 Component Adhesive Leakage Repair Sealant Evaluation (아스팔트 2액형 점착재의 누수보수 평가에 관한 연구)

  • Cho, Il-Kyu;Kim, Keun-Hur;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.140-141
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    • 2017
  • This study is based on the evaluation of a single component injection type adhesive repair material and a new 2 component type used in leakage of underground concrete structures. The studies showed that based on different mix ratio of the 2 component type adhesive sealant comprised of an asphalt main and latex mixture agent the viscosity of the material compound differed significantly. Based on a permeability testing, injection and economic efficiency, and performance, the appropriate ratio was determined to be 6:1 and was proceeded to the KS F 4935 evaluation method. The 2 component type adhesive sealant uses a static mixer and a cartridge type container for the injection procedure and was able to satisfy the evaluation criteria outlined in the KS F 4935 standard.

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Improvement of Re-adhesion Control Performance on Railway Electric Vehicle using Estimation of Maximum Adhesive Effort (최대점착력 추정을 이용한 철도차량의 재점착 제어 성능 개선)

  • Kim, U-Seok;Kim, Yong-Seok;Gang, Jun-Gu;Seol, Seung-Gi
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.49 no.1
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    • pp.32-39
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    • 2000
  • In this paper, an improved re-adhesion control scheme is proposed for 1C4M railway traction system. It is well known that the coefficient of adhesion between wheel and rail has a maximum value at a certain slip velocity. In the proposed scheme, adhesive effort is estimated by a full-order observer and the driving torque of motor is controlled to get maximum adhesive effort. The-adhesion control simulator is designed to verify the proposed re-adhesion control algorithm. The simulation results and experimental results are presented.

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Effects of Spangle Size on the Mechanical Properties of Galvanized Steel Sheets (용융아연도금강판 코팅층 접합강도에 미치는 스팽글 크기의 영향)

  • Hong, Moon-Hi;Lee, Ju-Youn;Paik, Doo-Jin
    • Korean Journal of Metals and Materials
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    • v.49 no.11
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    • pp.831-838
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    • 2011
  • Effects of spangle size and crystallographic characteristics on the surface appearance, galling properties, and adhesive strength of hot-dip galvanized steel sheets have been investigated. Both spangle size and crystallographic orientation measured by optical microscopy, scanning electron microscopy, and X-ray diffraction were identified as critical factors influencing the galvanized coating performance. By decreasing the spangle size, surface appearance and galling properties related to the friction coefficient were significantly improved. However, low temperature adhesive-strength with small spangle galvanized steel sheets showed lower values compared to commercially used galvanized coating. The variation of adhesive strength in terms of spangle size has been clarified.

Effects of endodontic tri-antibiotic paste on bond strengths of dentin adhesives to coronal dentin

  • Mirzakoucheki, Parvin;Walter, Ricardo;Khalighinejad, Navid;Jahromi, Maryam Zare;Mirsattari, Sanaz;Akbarzadeh, Navid
    • Restorative Dentistry and Endodontics
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    • v.40 no.2
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    • pp.136-142
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    • 2015
  • Objectives: The aim of this study was to evaluate the effects of tri-antibiotic paste (TAP) on microtensile bond strengths (MTBS) of dental adhesives to dentin. Materials and Methods: Sixty extracted molars had their occlusal surfaces flattened to expose dentin. They were divided into two groups, i.e., control group with no dentin treatment and experimental group with dentin treatment with TAP. After 10 days, specimens were bonded using self-etch (Filtek P90 adhesive) or etch-and-rinse (Adper Single Bond Plus) adhesives and restored with composite resin. Teeth were sectioned into beams, and the specimens were subjected to MTBS test. Data were analyzed using two-way ANOVA and post hoc Tukey tests. Results: There was a statistically significant interaction between dentin treatment and adhesive on MTBS to coronal dentin (p = 0.003). Despite a trend towards worse MTBS being noticed in the experimental groups, TAP application showed no significant effect on MTBS (p = 0.064). Conclusions: The etch-and-rinse adhesive Adper Single Bond Plus presented higher mean bond strengths than the self-etch adhesive Filtek P90, irrespective of the group. The superior bond performance for Adper Single Bond when compared to Filtek P90 adhesive was confirmed by a fewer number of adhesive failures. The influence of TAP in bond strength is insignificant.

Research on Flame Retardant Formaldehyde-Free Plywood Glued by Aqueous Polymer Isocyanate Adhesive

  • WEN, Ming-Yu;ZHU, Jia-Zhi;ZHU, Meng;SUN, Yao-Xing;PARK, Hee-Jun;SHI, Junyou
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.5
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    • pp.755-764
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    • 2020
  • Due to pronounced mechanical performance and being environmental friendly, aqueous polymer isocyanate adhesive (API) has been widely applied in the production of formaldehyde-free wood products. In this study, flame retardant formaldehyde-free plywood was prepared by incorporation of flame retardants into the API adhesive. Partially phosphorylated poly (vinyl alcohol) (PPVA) which was prepared by reacting poly (vinyl alcohol) with phosphoric acid was used to replace PVA in API formula. In addition, Mg-Al layered double hydroxides (LDH) was chosen as additive flame retardant, replacing traditional filler CaCO3 in API adhesive formula. And then, the flame retardant API adhesive with main agent (PPVA replacing PVA70wt.%, SBR emulsion 30wt.%), curing agent 10wt.% (accounts for of the main agent), and 20wt.% LDHs (accounts of the main agent) was used to prepare flame retardant plywood. The effect of application of PPVA and Mg-Al LDH on bonding strength of plywood was investigated. The flammability characteristics of the plywood were determined by cone calorimeter test (CCT). The results revealed that compared with the plywood prepared with API adhesive, the use of PPVA and LDH enhanced the flame retardancy of plywood without negatively affecting bonding strength. The CCT tests indicated that the heat release and smoke production flame retardant API plywood were lower than those of the ordinary API glued plywood. Promising developments for flame retardant API adhesive were expected in future applications of flame retardant formaldehyde-free plywood.

A Mechanical Experimental Study for Waterproofing Performance Evaluation of Self Adhesive Sheet Combined Polymer Resin and Poly-Iso Butylene (폴리머수지와 폴리이소부틸렌을 복합한 자착식시트의 방수성능평가를 위한 역학적 실험연구)

  • Min, Inki;Tae, Ghi-Ho
    • Journal of the Korean Society of Safety
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    • v.27 no.5
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    • pp.126-134
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    • 2012
  • The purpose of this study is to investigate waterproofing performance of self adhesive sheet combined polymer resin and poly-iso butylene. For the performance estimation of external waterproofing of concrete underground structures, there can be required various properties such as adhesion strength, hair crack resistance, repeat low and high temperature test, and so on. In this study, there engineering properties of composite system using polymer resin and poly-iso butylene were examined and could be confirmed to satisfy the guidelines of KS. Especially, it was turn out that the adhesion properties was excellent and high crack-resistance up to 1.49mm will be perform.

A Study on the Measurement of the Elastic Moduli and Characteristics for Space Adhesives (우주용 접착제의 탄성계수 측정 및 특성 규명에 관한 연구)

  • Kim, Hyun-Jung;Seo, Yu-Deok;Park, Sang-Hoon;Kim, Ji-Yeon;Uhm, Tae-Kyoung;Lee, Sang-Ryool;Lee, Seung-Hoon;Lee, Deog-Gyu;Lee, Eung-Shik;Jang, Hong-Sul;Jung, Dae-Jun;Youn, Sung-Kie
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.35 no.2
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    • pp.101-106
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    • 2007
  • The optical performance of the mirror for satellite camera is highly dependent on the adhesive properties between the mirror and its support. Therefore, in order to design a mirror with high optical performance, the mechanical properties of adhesives should be well defined. In this paper, the mechanical properties of three kinds of space adhesives are studied. Elastic moduli of the adhesives are determined by tensile tests. Stress-strain relation is obtained by using exponential curve fitting for the adhesive which shows non-linear behavior. In case of the linear behavior material, elastic modulus is calculated through linear curve fitting. For the tensile tests, several points have been selected in the operating temperature range of the adhesive. The elastic modulus of each adhesive is expressed as a function of temperature. Characteristics of the adhesives are discussed regarding their temperature sensitivity.