• Title/Summary/Keyword: adhesion materials

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A Study on the Test Methods of Bond Strength in Waterproofing and Anti-corrosion Materials by Reversed Pressure (역수압 작용을 고려한 방수·방식재의 부착강도 시험방법에 관한 연구)

  • Kim, Meong-Ji;Choi, Su-Young;Choi, Sung-Min;Oh, Sung-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.05a
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    • pp.232-233
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    • 2014
  • Recently, water treatment facility is usually eastablished in underground, and waterproofing and anti-corrosion materials for concrete structures applied water treatment tank is developing in various ways. However, as the limit of research focused on durability improvement of top coating material, it is insufficient to study on the adhesion strength between the concrete surface and primer. Therefore, there is to confirm the adhesion of between concrete surface and the three primers used as anti-corrosion waterproofing materials, and to investigate the properties of adhesion strength according to the condition such as wet codition and water pressure condition of the concrete surface in this study.

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Thermal behavior of Flame Retardant Filled PLA-WF Bio-Composites

  • Choi, Seung-Woo;Lee, Byoung-Ho;Kim, Hyun-Joong;Kim, Hee-Soo
    • Journal of the Korean Wood Science and Technology
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    • v.37 no.2
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    • pp.155-163
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    • 2009
  • This study examined the thermal stability of PLA-WF bio-composites. Wood flour (WF)-filled PLA bio-composites were reinforced with the flame retardants, Melamine pyrophosphate (MPP), resorcinol bis (diphenyl phosphate) (RDP) and zinc borate (ZB). The flame retardant was compounded with PLA and natural biodegradable filler. The thermal properties of the biodegradable polymer and bio-composites reinforced with the flame retardant were measured and analyzed by DSC, DMA and TGA. The results showed that the flame retardant-reinforced biodegradable bio-composite exhibited improved thermal properties.

Nanotribological Behavior of Cu Oxide and Silicon Tip (Cu Oxide와 Silicon Tip 사이의 나노트라이볼러지 작용)

  • Kim, Tae-Gon;Kim, In-Kwon;Park, Jin-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.364-365
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    • 2005
  • This paper report nanotribological behavior between Si tip and Cu wafer surfaces which was treated various concentration of $H_2O_2$. This experimental approach has proven atomic level insight into Cu CMP. It has been used to study interfacial friction and adhesion force between Si tip and Cu wafer surfaces in air by atomic force microscopy (AFM). Adhesion force of Cu surfaces which was pre-cleaned in diluted HF solution was lager than Cu oxide surfaces. Adhesion force of Cu oxide surface was saturated around 7 nN. Slope of normal force vs lateral signal was increased as increasing concentration of $H_2O_2$ and it was saturated around 24. Friction force of Cu oxide was lager than Cu.

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Carboxylated Nitrile Elastomer/Filler Nanocomposite: Effect of Silica Nanofiller in Thermal, Dynamic Mechanical Behavior, and Interfacial Adhesion

  • Mahaling R. N.;Jana G. K.;Das C. K.;Jeong, H.;Ha C. S.
    • Macromolecular Research
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    • v.13 no.4
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    • pp.306-313
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    • 2005
  • Surface modified nanofillers are often used as curative-cum reinforcing agents for functional polymers. The polymer nanofiller interaction depends on the curative systems used. In the present study the carboxylic group of the carboxylated nitrile elastomer participated in the reaction with Zn-ion coated nanosilica filler producing a type of ionomeric elastomer. The interaction at the molecular level thus produced a high modulus vulcanizate. In this case, the S and MBT system, as curative, had an edge over the MDA and DPG curative system. Interfacial adhesion was enhanced in the presence of Zn-ion-coated nanosilica filler associated with dynamic mechanical behavior. The inferior properties obtained in the case of the MDA and DPG curative system were due to the decreased reactivity of the silica surface, thus reducing interfacial adhesion.

Brazing Adhesion Properties of Ag Coated W-Ag Electric Contact on the Cu Substrate (Ag 코팅한 W-Ag 전기접점/Cu 모재간의 브레이징 접합 특성)

  • Kang Hyun-Goo;Kang Yun-Sung;Lee Jai-Sung
    • Journal of Powder Materials
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    • v.13 no.1 s.54
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    • pp.18-24
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    • 2006
  • The brazing adhesion properties of Ag coated W-Ag electric contact on the Cu substrate have been investigated in therms of microstructure, phase equilibrium and adhesion strength. Precoating of Ag layer ($3{\mu}m$ in thickness) on the $W-40\%Ag$ contact material was done by electro-plating method. Subsequently the brazing treatment was conducted by inserting BCuP-5 filler metal (Ag-Cu-P alloy) layer between Ag coated W-Ag and Cu substrate and annealing at $710^{\circ}C$ in $H_2$ atmosphere. The optimum brazing temperature of $710^{\circ}C$ was semi-empirically calculated on the basis of the Cu atomic diffusion profile in Ag layer of commercial electric contact produced by the same brazing process. As a mechanical test of the electric contact after brazing treatment the adhesion strength between the electric contact and Cu substrate was measured using Instron. The microstructure and phase equilibrium study revealed that the sound interlayer structure was formed by relatively low brazing treatment at $710^{\circ}C$. Thin Ag electro-plated layer precoated on the electric contact ($3{\mu}m$ in thickness) is thought to be enough for high adhesion strength arid sound microstructure in interface layer.

The evaluation for adhesion and compatibility properties of polyurethane and silicone sealant for window installation (창호 시공용 폴리우레탄 및 실리콘 실란트 접착성 및 상응성 평가)

  • Ahn, Myung-Su;Jung, Jin-young;Seo, YeonWon;Kim, Sung Hyun;Bae, Keesun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.75-77
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    • 2014
  • Using sealant for window installation is sealing the gap between the window frame and outer wall (such as concrete). A sealant serves to prevent external environmental impacts such as moisture, rain, sand, and dust entering inside of the building and make the building durable. In order to fulfill basic jointing function of sealing, at least 6 mm joint gap between two bonding surfaces are required. Also, adhesion performance between sealant and surfaces and the compatibility with other building materials are required to check before installation. In general, 2 part polyurethane sealant and 1 part silicone sealant are most common materials for sealing the joint of window. In this study, adhesion performances of those two generic sealants reflecting actual application conditions and the compatibility evaluations with other building materials are conducted to propose proper window installation procedures.

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A Study on Adhesion and Electro-optical Properties of ITO Films Deposited on Flexible PET Substrates with Deposition of SiO2 Buffer Layers (PET 기판 위에 SiO2 버퍼층 증착에 따른 ITO 박막의 부착 및 전기적 광학적 특성 연구)

  • Kang, Ja-Youn;Kim, Dong-Won;Cho, Kyu-Il;Woo, Byung-Il;Yun, Hwan-Jun
    • Journal of Surface Science and Engineering
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    • v.42 no.1
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    • pp.21-25
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    • 2009
  • Using an evaporation system, $SiO_2$ was deposited as a buffer layer between a PET substrate and a ITO layer and then ITO/$SiO_2$/PET layers were annealed for 1.5 hours at the temperature of $180^{\circ}C$. Adhesion and electro-optical properties of ITO films were studied with thickness variance of a $SiO_2$ buffer layer. As a result of introduction of the $SiO_2$ buffer layer, sheet resistance and resistivity increased and a ITO film with optimum sheet resistance ($529.3{\Omega}/square$) for an upper ITO film of resistive type touch panel could be obtained when $SiO_2$ of $50{\AA}$ was deposited. And it was found that ITO films with $SiO_2$ buffer layer have higher transmittance of $88{\sim}90%$ at 550 nm wavelength than ITO films with no buffer layers and the transmittance was enhanced as $SiO_2$ thickness increased from $50{\AA}$ to $100{\AA}$. Adhesion property of ITO films with $SiO_2$ buffer layers became better than ITO films with no buffer layers and this property was independent of $SiO_2$ thickness variance ($50{\sim}100{\AA}$). By depositing a $SiO_2$ buffer layer of $50{\AA}$ on the PET substrate and sputtering a ITO thin film on the layer, a ITO film with enhanced adhesion, electro-optical properties could be obtained.

Hydrophobicity and Adhesion Evaluation of MWCNT/Teflon-polyurethane Topcoat for Aircraft with Different MWCNT Coating Times (탄소나노튜브 코팅횟수에 따른 항공기용 탄소나노튜브/테프론-폴리우레탄 탑코트의 표면소수성 및 부착력 평가)

  • Lee, Jae-Hyuk;Kim, Jong-Hyun;Park, Joung-Man
    • Composites Research
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    • v.35 no.2
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    • pp.80-85
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    • 2022
  • This work presents an experiment study to evaluate the nanoparticle adhesion and surface hydrophobicity characteristics of Teflon-polyurethane top coat depending on the number of multi-wall carbon nanotube (MWCNT) coatings, which is a carbon-based hydrophobic particle. In order to measure the adhesion between the nanoparticles and the top coat, adhesion pull-off test was performed with different MWCNT oxidation times. Static contact angle and roughness measurements were carried out to characterize the surface hydrophobic behavior. Through the roughness evaluation, it was confirmed that the carbon nanotubes were wetted in the Teflon-polyurethane top coat, and the degree carbon nanotube wetting was confirmed through a USB-microscope. As a result, it was found that the larger the degree of wetting, the better the adhesion. From the experimental results, as the hydrophobicity of Teflon-polyurethane increased, the adhesive propertydecreased with the number of coatings. It was possible to improve the adhesive force and determine the number of coatings of carbon nanotubes with optimized hydrophobicity.

Historical Trends of Micromechanical Testing Methods for Structural Fiber Reinforced Composites to Evaluate the Interfacial Adhesion (구조용 섬유강화복합재료의 계면접착 특성 평가를 위한 미세역학시험법의 연구동향 고찰)

  • Park, Joung-Man;Kim, Jong-Hyun;Kim, Dong-Uk;Kwon, Dong-Jun
    • Journal of Adhesion and Interface
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    • v.23 no.3
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    • pp.59-69
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    • 2022
  • In composite materials, the adhesion and interfacial properties were the most important factors to obtain high performance of mechanical properties. This review paper had been focused on the micromechanical evaluation methods for the interfacial property historically. The interfacial property of fiber-reinforced composites (FRC) could be evaluated using only a single fiber and matrix via various micromechanical testing methods. Self-sensing due to the fracture behavior of FRC could be determined and discussed more critically and clearly using electro-micromechanical evaluation. In this paper, the research trends for micro-mechanical evaluation of composites was summarized, and their practical applications would be suggested in the future.

Preparation and Adhesion of One Part Room Temperature Curable Alkoxy Type Silicone Sealant (일액형 알코올형 실리콘 실란트의 제조 및 접착 물성)

  • Kim, Dae-Jun;Park, Young-Jun;Kim, Hyun-Joong;Lee, Bong Woo;Han, Jae Chul
    • Journal of Adhesion and Interface
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    • v.2 no.4
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    • pp.1-9
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    • 2001
  • Silicone sealants are composed of polymer, plasticizer, crosslinker, catalyst and filler. Types and compositions of components are effected on sealant performances. In recent, use of alkoxy type silicone sealant increased due to environmental advantage. In this study, we investigated effects of component types and ratios on one-part room temperature curable alkoxy type silicone sealant preparation and adhesion properties. Alkoxy type silicone sealants were prepared with various PDMS (polydimethylsiloxane) viscosities. In addition, the effect of plasticizer, crosslinkers, and catalyst on sealant obtained from by mixture of PDMS viscosities of 20000 and 80000 was investigated. Reaction temperature on change of mixing time was observed, and then proper crosslinking systems were found. Adhesion (properties) of silicone sealants were measured. In the sealants preparation, stable reaction was achieved by adjusting composition variance ratio in the sealant mixture temperature below $40^{\circ}C$. The adhesion properties of sealant differ from substrate composition. The order of adhesion strength was glass/glass > glass/aluminum > aluminum/aluminum system. The elongation of sealant was increased as polymer viscosity and plasticizer content increased. The strength was increased as crosslinker and plasticizer decreased, while catalyst increased.

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