• 한국표면공학회:학술대회논문집
• /
• 한국표면공학회 1998년도 춘계학술발표회 초록집
• /
• pp.158-159
• /
• 1998

• 한국세라믹학회:학술대회논문집
• /
• 한국세라믹학회 2002년도 추계총회 및 연구발표회 초록집
• /
• pp.46.2-46
• /
• 2002

• 한국재료학회지
• /
• 제9권8호
• /
• pp.768-774
• /
• 1999

세리아 안정화 지르코니아 성형체내에 이트리아를 침적법으로 도핑시켜 미세구조를 관철하였다. 도핑된 이트리아의 양과 열처리 조건을 제어하여 입계가 변형된 불규칙 입자형상의 미세구조를 형성시켰으며, 이때 입자형상의 불규칙 정도는 첨가된 이트리아의 양에 비례하였다. 0.2M 농도의 Y(NO$_3$)$_3$.6$H_2O$의 수용액에 재침적하여 1$650^{\circ}C$에서 2시간 열처리한 시편의 미세구조는 표면부와 내부 모두에서 불규칙 입자형상을 나타내었으며, 입자의 불규칙도도 가장 큰 것으로 나타났다. 가압소결을 행한 결과 입계가 불규칙하게 변화된 미세구조가 창출됨과 동시에 평균입자 크기가 0.3$\mu\textrm{m}$ 가량인 미세한 소결체를 제조할 수 있었으며, 상분석 결과 대부분 정방정상을 유지하고 있었다. 불규칙 입자형상의 미세구조를 가진 시편의 파괴인성값은, 정상적인 입자형상을 갖는 시편에서의 압흔 균열 크기로부터 비교 유추한 결과 17.6MPa.m(sup)1/2 이상인 것으로 나타났다.

• 한국세라믹학회지
• /
• 제35권12호
• /
• pp.1294-1300
• /
• 1998

Yttria-stabilized zirconia ceramics with irregular grain shapes and curved grain boundaries was prepared by ceria doping. The amount of ceria doped into zirconia compacts by a dipping method were at range of 2 to 20 mol% Irregular grain shapes and curved grain boundaries were formed only inspecimens doped with more than 8mol% cerial. Ceria-doped specimens showed large grain size and low sintered density compared with pure yttria-stabilized zirconia which was due to the increase in the contents of stabilizer and cubic phase. The amount of doped ceria was larger on the surface than the inside regions and therefore mi-crostructure and phase on the surface were different from those in the inside regions. Transgranular frac-ture mode was observed ion ceria doped specimens due to irregular large grain sizes.

• 한국세라믹학회지
• /
• 제53권3호
• /
• pp.332-337
• /
• 2016

As a case study on yttria stabilized zirconia ceramics, the sintering characteristics of submicron powders and the granulation prepared by two-fluid spray drying of submicron particles were investigated. As-received powders of yttria stabilized zirconia particles were reduced to a uniform size of less than about 200 nm by repeated milling. Granulation size obtained by the two-fluid spray drying was affected by the organic matter and the primary particle size. Sintering behavior such as porosity, water absorption ratio, density, and transparency was influenced by processing conditions of the powder, and the discontinuous interfaces in a green body were reduced.

• 한국생산제조학회지
• /
• 제19권1호
• /
• pp.7-14
• /
• 2010

AE(acoustic emission) sensor has been used for a state monitoring and observation during a ultra-precision machining because AE signal, which has high frequency range, is sensitive enough. In case of ceramic fabrication, a monitoring of machining state is important because of its hard and brittle nature. A machining characteristic of ceramic is susceptibly different in accordance with variable machining conditions. In this study, Yttria($Y_2O_3$) ceramic was fabricated using the ultra-precision lapping process with in-process electrolytic dressing(IED) method. And the surface machining characteristic and AE sensor signal were compared and analyzed.

• 한국전기전자재료학회논문지
• /
• 제11권10호
• /
• pp.842-848
• /
• 1998

The stability of paraseodymium-based zinc oxide varistor consisting of Zn-Pr-Co-Cr-Y oxide was investigated according to yttria additives under different stress conditons, such as 0.8V\ulcorner\ulcorner/373K/12h and 0.85V\ulcorner\ulcorner/393K/12h. Wholly, all varistor after the stress showed nearly symmetric and stable I-V characteristics. Particularly, in the case of 2.0mol% and 4.0mol% yttria-added varistor showing a good I-V characteristics, the varation rate of varistor voltage were less 1% and that of nonlinear coefficient were about degree of 5%, and what is remarkable, leakage current with increasing stress time during the applied stress was almost constant. It the light of these facts, it is estimated that varistor constituents having 2.0mol% and 4.0mol% yittria, respectively, will be utilized to various application fields.

• 한국재료학회지
• /
• 제34권2호
• /
• pp.79-84
• /
• 2024

Thin films of yttria-stabilized zirconia (YSZ) nanoparticles were prepared using a low-temperature deposition and crystallization process involving successive ionic layer adsorption and reaction (SILAR) or SILAR-Air spray Plus (SILAR-A+) methods, coupled with hydrothermal (175 ℃) and furnace (500 ℃) post-annealing. The annealed YSZ films resulted in crystalline products, and their phases of monoclinic, tetragonal, and cubic were categorized through X-ray diffraction analysis. The morphologies of the as-prepared films, fabricated by SILAR and SILAR-A+ processes, including hydrothermal dehydration and annealing, were characterized by the degree of surface cracking using scanning electron microscopy images. Additionally, the thicknesses of the YSZ thin films were compared by removing diffusion layers such as spectator anions and water accumulated during the air spray plus process. Crack-free YSZ thin films were successfully fabricated on glass substrates using the SILAR-A+ method, followed by hydrothermal and furnace annealing, making them suitable for application in solid oxide fuel cells.

• 한국세라믹학회지
• /
• 제35권7호
• /
• pp.691-698
• /
• 1998

• 한국결정성장학회지
• /
• 제19권5호
• /
• pp.237-241
• /
• 2009

Dislocation dipoles were formed in the early stage of deformation of Y-CSZ single crystal at high temperatures. And the dipoles were pinched off to break into dipoles loops by dislocation climb. Dislocation loop annealing was peformed in Y-CSZ single crystal to evaluate the diffusivity of cation which was the rate-controlling ion.