• Title/Summary/Keyword: YIG

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YIG(Yttrium Iron Garnet) SingLe Crystal Growth by Floating Zone Method (Floating Zone법에 의한 YIG단결정 성장)

  • 신재혁;김범석;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.2 no.2
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    • pp.1-1
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    • 1992
  • YIG(Yttrium Iron Garnet) single crystals were grown by FZ(Floating Zone) method. Since YIG melts incongruently, TSFZ(Traveling Solvent Floating Zone) method which was modified FZ was applied to grow YIG single crystals. The optimum growth condition were growth rate Imm/hr, counter-rotation 30rpm and oxidized atmosphere was necessary to sintering and growth process. The quality of grown crystals depended on the degree of sintering. The voids were generated by the reaction of Fe ions with oxygen and the density of voids was increased with the growth rate increased. When the growth rate was more than 1.5mm/hr, the cellular growth occured and the density of dislocation was increased at the periphery of crystals. Also, secondary phases of orthoferrite(YFe$O_3$)compost ion were observed in the grown crystal.

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Ferromagnetic Resonance Study of an YIG Thin Film Grown by LPE Method (LPE법으로 제조한 YIG 박막에 대한 강자성공명 연구)

  • 이수형;염태호;윤달호;김약연;한기평;이상석
    • Journal of the Korean Magnetics Society
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    • v.9 no.2
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    • pp.85-90
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    • 1999
  • The ferromagnetic resonance study of the magnetostatic wave modes for an YIG thin film, grown by a liquid phase epitaxy method, was performed by an FMR spectrometer at room temperature. The magnetostatic surface wave and backward volume wave modes show periodic excitations in parallel configuration, whereas the complex spectra were observed in perpendicular configuration. The resonance spectra in parallel configuration can be well explained by the Walker and Damon-Eshbach theory. The peak-peak line width of uniform mode was 0.4 Oe. The saturation magnetization $M_s$ of the YIG thin film was calculated as 137 emu/㎤. In order to know the dependence of the magnetostatic modes as a function of the saturation magnetization and the thickness, the (1,1) and (3,1) modes of the magnetostatic backward volume wave were compared and theoretically calculated.

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Effect of Annealing for YIG Single Crystal Thick Films (YIG 단결정 후막의 열처리의 효과)

  • 김근영;윤석규;김용탁;이성문;윤대호
    • Journal of the Korean Ceramic Society
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    • v.40 no.9
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    • pp.855-858
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    • 2003
  • When the PbO-based flux system is used in the Liquid Phase Epitaxy (LPE) method for Yttrium Iron Garnet (YIG) thick film, the effect of Pb ions incorporated into the grown crystal; increase the lattice parameter, changed the uniaxial magnetic anisotropy constant (Ku) or conductance of grown film. It exerts a bad influence on physical property such as increasing optical absorption of grown film. The content of the Pb ion in crystal was decreased by volatilization of Pb ion after annealing; therefore, the lattice parameter of film was reduced on an average 0.0115 ${\AA}$ by the the Pb ion.

Thermal Decomposition and Synthesis of Yttrium Iron Garnet Powder by Homogeneous Precipitation Method (균일침전법에 의한 Yttrium Iron Garnet 분말의 합성 및 열분해특성)

  • An, Yeong-Su;Han, Mun-Hui;Kim, Jong-O
    • Korean Journal of Materials Research
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    • v.6 no.3
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    • pp.275-281
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    • 1996
  • YIG 전구체 분말은 요소의 열분해반응을 이용한 균일침전법에 의해서 질산염으로부터 제조하였다. 침전은 철이온이 먼저 침전한 후 이트륨이온이 침전하는 과정으로 이루어졌다. YGI전구체 분말은 철산화물과 비정질로 구성되어 있으며 그 분말의 대략적인 화학식은 2.5Fe2O3.Y3(OH)9-2x(CO3)x.nH2O로 되어있다. YIG 전구체 분말의 열분해과정은 dehydration, 철산화물의 recrystallization, yttrium carbonate 및 yttrium oxide의 형성과 고상반응등 여러단계로 구성되어 있다. 열처리온도가 증가함에 따라 Y2O3와 Fe2O3의 고상반응에 의해 YFeO3 intermediate을 경유해서 YIG상이 형성됨을 확인하였다. 단일상의 YIG는 120$0^{\circ}C$에서 6시간 공기중에서 소성함에 의해서 얻을 수 있었다.

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NSMM을 통한 Bi:YIG박막의 Bi농도에 따른 마이크로파 특성 연구

  • Lee, Han-Ju;Yun, Yeong-Un;Kim, Tae-Dong;Yu, Hyeong-Geun;Kim, Song-Hui;Balt, Erdene;Lee, Gi-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.142-142
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    • 2009
  • Bismuth-substituted yttrium iron garnet(Bi-YIG; $Bi_xY_{3-x}Fe_5O_{12}$, x=0, 0.5, 1.0, 1.5, 2.0) thin films were fabricated on glass substrates using a metal organic decomposition (MOD) method. The dielectric property was measured by NSMM(Near-field scanning microwave microscopy) system that operating frequency is 4 Ghz. The obtained reflection coefficient $S_{11}$ of the Bi:YIG thin films with different bismuth concentration was increased as the bismuth concentration increased due to the lattice mismatch and vacancy of ions because of a lager ionic radius of bismuth ion than yttrium ion.

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Study of Temperature stabilization for Isolator using YIG ferrite (YIG 페라이트를 이용한 아이솔레이터의 온도안정화 연구)

  • 전동석;이홍열;김동영;한진우;이상석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.78-81
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    • 2002
  • This paper describes on the design structure and development temperature stable strip-line junction isolator operating in above resonance mode. Temperature characteristics of isolator depend on magnet, YIG(Yttium Iron Garnet) ferrite, and conductor etc. These require temperature stability and possible methods of compensation for the temperature dependent effects. In this paper, the analysis and measurement of the temperature characteristics were carried out for the material isolator prototype. The bandwidth of isolator was expended and the center frequency shift was reduced in temperature range of -20∼8O$^{\circ}C$.

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Suppression of the abnormal grain growth in the sintering of YIG (YIG 소결시 나타나는 비정상입성 장 현상과 그의 억제)

  • 김동영;한진우;전동석;이상석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.466-469
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    • 2002
  • In the sintering of YIG, abnormal grain growth phenomena was observed. This abnormal grain growth is related to the sintering temperature in this experiment. In the sintering below 145$0^{\circ}C$., the sintered body showed narrow size distribution. However, in the sintering at 145$0^{\circ}C$, a few grains grew rapidly with respect to other grains, and bimodal size distribution was appeared. Liquid phase was not observed far from the abnormally grown large grains, but only near the large grains. This means that the abnormal grain growth was caused by the nonuniform distribution of liquid phase which promote the grains growth. This nonuniform distribution of liquid phase was thought to be due to the nonuniform mixing of the starting materials. This abnormal grain growth was suppressed by enhance the compositional uniformity by multiple calcination.

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Study of Temperature Stabilization for Isolator using YIG ferrite (YIG 페라이트를 이용한 아이솔레이터의 온도안정화 연구)

  • 전동석;이홍열;김동영;한진우;이상석
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.12
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    • pp.1075-1078
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    • 2002
  • This paper describes on the design structure and development of temperature stable strip-line function isolator operating In above resonance mode. Temperature characteristics of isolator depend on magnet, YIG(Yttium Iron Garnet) ferrite, and conductor etc. These require temperature stability and possible methods of compensation for the temperature dependent effects. In this paper, the analysis and measurement of the temperature characteristics were carried out for the material isolator prototype. The bandwidth of isolator was expended and the frequency shift at center was reduced in the temperature range of -20∼80$\^{C}$.

The Study on the Microstructure and Magnetic Properties of Polycrystalline $Y_3Fe_5O_{12}$ (다결정 $Y_3Fe_5O_{12}$의 미세구조와 자기적 특성 연구)

  • 이재동;김성재;이승호;김태옥
    • Journal of the Korean Ceramic Society
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    • v.30 no.12
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    • pp.1015-1022
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    • 1993
  • The formation process of polycrystalline YIG(Y3Fe5O12) prepared by conventional method in Fe2O3-Y2O3 system was investigated. Effect of the microstructure of sintered body on electromagnetic properties was also investigated. Orthoferrite (YFeO3) was formed between 900 and 110$0^{\circ}C$. Formation of YIG phase begin at 110$0^{\circ}C$ with sharp increased saturation magnetization simultaneously. YIG phase is identified as single phase above 120$0^{\circ}C$. The microstructures and electromagnetic properties of sintered bodies are varied due to calcination condition of starting materials. The sintered YIG of calcined sample at 110$0^{\circ}C$ has such magnetic properties as Bs=1580G, BHC=1.89Oe, Tc=570K, ΔH(9.3GHz)=78Oe.

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Dependence of Microstructure of Sintered $Y_3$Fe$_5$O$_{12}$ in Addition of CuO (CuO 첨가에 따른 $Y_3$Fe$_5$O$_{12}$ 소결체의 미세구조 변화)

  • 이재동;김광석;김성재;김태옥
    • Journal of the Korean Ceramic Society
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    • v.35 no.10
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    • pp.1014-1019
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    • 1998
  • As results of the study on the sinterbility of YIG at the low temperature using CuO as additive CuO com-pound which contain {{{{ { {Fe }_{2 }O }_{3 } }} was shown liquid in sintering process. YIG crystal dissolved into CuO compound liquid phase and then Y element which is considered no solubility in solid CuO compound moved to the grain during cooling. The abnormal grain growth up to 150${\mu}{\textrm}{m}$ at CuO 8.6mole% was shown due to shape accomdation reaction and local liquid distribution. The apparent density of YIG shows minimum at CuO 8.6 mole% due to abnormal grain growth and the saturation magnetization decrease dramatically at 32.5mole% due to orthoferrite formation.

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