• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.07a
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• pp.593-596
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• 2003

A proposed way to prepare $YBa_2Cu_3O_y$ wires or tapes is that Ag is used as substrate and melting point of $YBa_2Cu_3O_y$ is decreased to lower than the melting point of silver ($961\;^{\circ}C$). Therefore after the deposition of $YBa_2Cu_3O_y$ film on Ag substrate, the heat treatment can be carried out below the Ag melting point. Silver (Ag) and Lead oxide(PbO) were selected to be additives for $YBa_2Cu_3O_y$. Different Ag and PbO contents were added in $YBa_2Cu_3O_y$, the melting points of which were measured by DTA. In order to guarantee that the superconductivity of $YBa_2Cu_3O_y$ was not reduced after Ag and PbO added into $YBa_2Cu_3O_y$, their superconductivities were measured. It is proved that as additives, both Ag and PbO can reduce the melting point of $YBa_2Cu_3O_y$. For Ag doped $YBa_2Cu_3O_y$, $T_c$ is about 93K and ${\Delta}Tc$ is $2{\sim}3K$. For PbO doped $YBa_2Cu_3O_y$, $T_c$ is $88K{\sim}92K$ and ${\Delta}T_c$ is $11{\sim}12K$. When 10 wt% of Ag and 10 wt% PbO were added in $YBa_2Cu_3O_y$, the melting point of the mixture of $YBa_2Cu_3O_y$ (80 wt%), Ag (10 wt%) and PbO (l0 wt%) is $943^{\circ}C$. The transition temperatures ($T_c$) of the sample is 91.8 K.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2006.06a
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• pp.346-347
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• 2006

기계적 품질계수(Qm)를 향상시키기 위해 $Y_2O_3$와 $MnO_2$를 첨가함에 따른 $SrBi_2Nb_2O_9$ 세라믹스의 강유전 특성을 알아보았다. 합성분말의 입도를 분석 한 결과 $SrBi_2Nb_2O_9$의 경우 781.27nm였고, $Y_2O_3$와 $MnO_2$를 첨가한 경우 각 각 830.4nm와 981.1nm로 particle size는 증가하였고, 소결 후 소결밀도는 차이가 거의 없었으며, grain size는 $SrBi_2Nb_2O_9$과 $Y_2O_3$를 첨가했을 경우 $1{\mu}m$이하이며 반면, $MnO_2$를 첨가하였을 때 결정립이 성장하여 $3{\sim}4{\mu}m$로 나타났다. 또한, 모두가 $450^{\circ}C$ 이상의 상전이온도를 갖았다.

• Nuclear industry
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• v.19 no.7 s.197
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• pp.31-34
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• 1999

99년 6월 21일 오전 11시. 울진 3호기의 모든 전산 설비의 날짜 및 시간이 2000년 00시 00분으로 변경되어 발전소의 모든 설비들은 2000년과 똑같은 상황하에서 운전되고 있었고 원자로 출력, 발전기 출력도 정상 상태를 유지하고 있었다. Y2K 종합 실증 실험은 50여분 동안 진행되었으며, 2000년 연도 전환 시험, 날짜 지정 시험, 윤년 인식 시험, 그리고 마지막으로 안전 설비 동작 시험순으로 시험이 진행되는 동안 아무런 설비의 이상 징후나 이상 상태 발생 없이 성공적으로 시험이 완료되었다. 지난 일년여 동안 Y2K 문제 해결을 위해 노력해온 모든 직원들의 노고가 한순간에 보상받는 순간이기도 했다. Y2K 종합 실증 실험이 끝나고 난후에 주제어실과 현장의 주요 설비들이 전보다 더 신뢰가 가고 튼튼해 보였던 것은 나만의 느낌이 아니었으리라 생각한다. 그 동안 수고한 모든 이들의 정성이 범국가적 아니 범세계적 핫이슈인 Y2K 문제를 원전의 울타리 밖으로 멀리 쫓아 버렸으며, 청정 에너지원인 원자력을 국민들로부터 더욱더 사랑받을 수 있도록 하는 계기가 되었다고 자평하고 싶다. 그 동안 울진 3호기 Y2K 종합 실증 시험을 마치기까지의 추진 경위와 Y2K 실증 시험 결과, 그리고 향후 대책 등에 대해서 간단히 소개하고자 한다.

• Journal of the Korean Ceramic Society
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• v.25 no.3
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• pp.225-230
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• 1988

The strength and thermal shock resistance of $Al_2O_3-ZrO_2$ composites have been studied. The tetragonal $ZrO_2$ powder containing 1 mol.% $Y_2O_3$ and monoclinic $ZrO_2$ powder were prepared by coprecipitation method and subsequently mixed with $Al_2O_3$ powder and granulated by sieving. Duplex composites were prepared by dry mixing matrix agglomerate with 15 to 30 vol.% of dispersion agglomerate, followed by pressing and sintering at 1$600^{\circ}C$ for1 hr. These $Al_2O_3-ZrO_2$ 2 composites having heterogeneous structure showed improved thermal shock behaviors because of the microcracking and pores in dispersed granules, and compressive stresses around dispersed granules resulting from $ZrO_2$ transformation.

• Applied Chemistry for Engineering
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• v.2 no.2
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• pp.165-174
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• 1991

The kinetics and the mechanism for the selective oxidation of ethylene on the supported monolithic silver catalyst were experimentally investigated in a fixed bed tubular reactor. The formation rates of ethylene oxide and carbon dioxide were measured at the atmospheric pressure with various combinations of partial pressures of ethylene and oxygen at temperature range of $225-300^{\circ}C$, conversion with 1.2-7.5 %, and then the mechanism of the selective oxidation of ethylene was verified. Their formation rates fitted with the Langmuir-Hinshelwood mechnism. The ethylene oxide and carbon dioxide are produced by reation of adsorbed ethylene with monoatomic oxygen adsorbed on the active sites of Ag-surface, and their formation rate equation are expressed as : $R_{EO}={\frac{k_1K_0{^{1/2}}K_EK_SP_{02}{^{3/2}}P_E}{(1+{\sqrt{K_0P_{02}}}+K_EP_E+K_PP_P)^2(1+{\sqrt{K_SP_{02}})^2}}$ $R_C={\frac{k_2K_0{^3}K_EK_S{^{7/2}}P_{02}{^{13/2}}P_E}{(1+{\sqrt{K_0P_{02}}}+K_EP_E+K_PP_P)^7(1+{\sqrt{K_SP_{02}})^7}}$ The activation energies of ethylene oxide and dioxide and carbon dioxide formations can be estimated to be 12.25 and 17.85 Kcal/mol, respectively.

• Applied Chemistry for Engineering
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• v.16 no.1
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• pp.45-51
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• 2005

$K^+-{\beta}^{{\prime}{\prime}}-Al_2O_3$ in the $K_2O-Li_2O-Al_2O_3$ ternary system was synthesized using aluminum nitrate solution as a starting material. For the synthesis of pure $K^+-{\beta}^{{\prime}{\prime}}-Al_2O_3$, raw materials with chemical composition of $0.84K_2O{\cdot}0.082Li_2O{\cdot}5.2Al_2O_3$ were mixed in solution state. The effects of dispersant and solution-pH were investigated in minimizing the particle size and on the synthesis of pure $K^+-{\beta}^{{\prime}{\prime}}-Al_2O_3$. Ethanol was used for a dispersant, and $NH_4OH$ solution and nitric acid were added for pH adjustment. The solution pH was increased from 1.0 to 7.5 by 0.5 increments. Each sample was calcined at $1200^{\circ}C$ for 2 h and characterized with X-ray diffraction and particle size analyzer. The pH of solution significantly effected both particle size and phase formation, while the addition of ethanol only effected particle size. The synthesis of pure $K^+-{\beta}^{{\prime}{\prime}}-Al_2O_3$ was favored by addition of nitric acid (for pH control).

• Fire Science and Engineering
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• v.32 no.5
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• pp.6-14
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• 2018

This study was carried out with respect to the heat release rate (HRR) properties of building wood. Heat release characteristics were measured using a cone calorimeter (ISO 5660-1) with four kinds of wood. The time to ignition measured after the combustion in $25kW/m^2$ external heat flux was 35 to 55 s. Time to ignition of both lauan and red pine was marked with the most delayed value in each of 54 s, 55 s. The maximum heat release rate ($HRR_{peak}$) was $156.87{\sim}235.1kW/m^2$, and the risk of early fire was highest in spruce. Total heat release of red pine was obtained in the highest value with $114.2MJ/m^2$. The mean effective heat of combustion of Japanese cedar was 19.1 MJ/kg and the highest among the samples. Fire risk of wood by FPI was orderly increased from lauan ($0.2468s{\cdot}m^2/kW$), red pine ($0.2339s{\cdot}m^2/kW$), spruce ($0.2308s{\cdot}m^2/kW$) to Japanese cedar ($0.2231s{\cdot}m^2/kW$). Fire risk of wood by FGI get increased from lauan ($0.5088kW/m^2{\cdot}s$), red pine ($0.5111kW/m^2{\cdot}s$), Japanese cedar ($2.8522kW/m^2{\cdot}s$) to spruce ($3.0662kW/m^2{\cdot}s$). Therefore, the risk of fire on the heat release characteristics of woods were found that spruce and Japanese cedar showed the high value compared with the other specimens.

• The Bulletin of The Korean Astronomical Society
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• v.32 no.2
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• pp.35.2-35.2
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• 2007

• Bulletin of the Korean Mathematical Society
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• v.36 no.2
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• pp.411-417
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• 1999

in this paper, we determine the jump number of the product of generalized crowns: s(${S_n}^k \times {S_m}^l$) = 2(m+1)(n+k)+2(m-2)(n-2)-1.

• Bulletin of the Korean Chemical Society
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• v.25 no.5
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• pp.629-633
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• 2004

A new PVC membrane electrode for $UO_2^{2+}$ ion based on 2,2'-[1,2-ethanediyl bis (nitriloethylidene)]bis(1-naphthalene) as a suitable ionophore was prepared. The electrode exhibites a Nernstian response for $UO_2^{2+}$ ion over a wide concentration range ($1.0{\times}10^{-1}-1.0{\times}10^{-7}$M) with a slope of 28.5 ${\pm}$ 0.8 mV/decade. The limit of detection is $7.0{\times}10^{-8}$M. The electrode has a response time of < 20 s and a useful working pH range of 3-4. The proposed membrane sensor shows good discriminating abilities towards $UO_2^{2+}$ ion with regard to several alkali, alkaline earth transition and heavy metal ions. It was successfully used to the recovery of uranyl ion from, tap water and, as an indicator electrode, in potentiometric titration of $UO_2^{2+}$ ion with Piroxycam.