• 한국해양공학회지
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• 제25권1호
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• pp.67-72
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• 2011

Offshore structures, such as a platform, a buoy, or a floating vessel, are exposed to several dynamic loads, and viscoelastic damping material is used to reduce the vibration of offshore structures. It is important to know the properties of viscoelastic materials because loss factor and Young's modulus of the viscoelastic damping material are dependent on frequency and temperature. In this study, an advanced technique for obtaining accurate loss factor and Young's modulus of the viscoelastic damping material is introduced based on a multi degree of freedom curve-fitting method and the RKU (Ross-Kerwin-Ungar) equations. The technique is based on a modified experimental procedure from ASTM E 756-04. Loss factor and Young's modulus of the viscoelastic damping material are measured for different temperatures by performing the test in a temperature-controlled vibration measurement room where temperature varies from 5 to 45 degrees Celsius.

• Computers and Concrete
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• 제32권4호
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• pp.383-392
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• 2023

The mechanical properties of Recycled Aggregate Concrete (RAC) with 100 percent Recycled Coarse Aggregate (RCA) under loading rates were investigated in depth. The theoretical model was validated utilizing the RAC elastic modulus obtained from cylindrical specimens subjected to various strain rates. Viscoelastic theories have traditionally been used to describe creep and relaxation of viscoelastic materials at low strain rates. In this study, viscoelastic theories were extended to the time domain of high strain rates. The theory proposed was known as reversed viscoelastic theory. Normalized Dirichlet-Prony theory was used as an illustration, and its parameters were determined. Comparing the predicted results to the experimental data revealed a high level of concordance. This methodology demonstrated its ability to characterize the strain rate effect for viscoelastic materials, as well as its applicability for determining not only the elastic modulus for viscoelastic materials, but also their shear and bulk moduli.

• 대한기계학회논문집B
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• 제32권7호
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• pp.487-496
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• 2008

Quartz crystal oscillator is frequently used in measuring a very small amount of mass attached to or adsorbed on the surface of an electrode on the quartz plate. The physical principle is that the resonance frequency of the shear vibration of the quartz caused by an applied electric field is a function of the mass. Recently, effort has been tried to measure physical properties of viscoelastic fluids, such as viscosity and shear modulus. This paper presents useful formula that can be used in estimating the properties of viscoelastic fluids. Important finding in this analysis is that the formula can produce multiple values for the physical properties of the viscoelastic materials.

• Journal of Biosystems Engineering
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• 제16권3호
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• pp.263-271
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• 1991

When grains is subjected to oscillating load, the dynamic viscoelastic behavior of the material will be describe the complex modulus of the material. The complex modulus and therefore the storage modulus, the loss modulus, and the phase angle for the sample should be obtainable with a given static viscoelastic property of the material under static load. The complex relaxation moduli of the rough rice kernel were computed from the Burger's model describing creep behavior of the material which were obtained in the previous study. Also, the effects of cyclic load and moisture content of grain on the dynamic viscoelastic behavior of the samples were analized. The storage modulus of the rough rice kernel slightly increased with the frequency applied but at above the frequency of 0.1 Hz it was nearly constant with the frequency, and the loss modulus of the sample very rapidly decreased with increase in the frequency on those frequency ranges. It was shown that the storage modulus and the loss modulus of the sample increased with decrease in grain moisture content. Effect of grain moisture content on the storage modulus of the sample was highly significant than effect of the frequency applied, but effect of the frequency on the loss modulus of the sample was more significant than effect of grain moisture content.

• Journal of Pharmaceutical Investigation
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• 제36권1호
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• pp.31-38
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• 2006

Using a Rheometries Dynamic Analyzer (RDA II), the dynamic viscoelastic properties of a semi-solid ointment base (vaseline) in large amplitude oscillatory shear flow fields were measured over a temperature range of $25{\sim}45^{\circ}C$ and the linear viscoelastic behavior in small amplitude oscillatory shear flow fields was investigated over a wide range of angular frequencies. In this article, the nonlinear viscoelastic behavior was reported from the experimentally obtained data and the effect of temperature on this behavior was discussed in detail. In addition, the angular frequency and temperature dependencies of a linear viscoelastic behavior were explained. Finally, the applicability of a time-temperature superposition principle originally developed for polymeric materials was examined using a shift factor. Main results obtained from this study can be summarized as follows : (1) At very small strain amplitude region, vaseline shows a linear viscoelastic behavior independent of the imposed deformation magnitudes. Above a critical strain amplitude $({\gamma}_{0}=0.1{\sim}0.2%)$, however, vaseline exhibits a nonlinear viscoelastic behavior ; indicating that both the storage modulus and dynamic viscosity are sharply decreased with increasing deformation magnitude. (2) In large amplitude oscillatory shear flow fields, an elastic behavior (storage modulus) has a stronger strain amplitude dependence and begins to show a nonlinear behavior at a smaller strain amplitude region than does a viscous behavior (dynamic viscosity). (3) In small amplitude oscillatory shear flow fields, the storage modulus as well as the loss modulus are continuously increased as an increase in angular frequency and an elastic nature is always superior to a viscous behavior over a wide range of angular frequencies. (4) A time-temperature superposition principle can successfully be applicable to vaseline. This finding allows us to estimate the dynamic viscoelastic behavior of vaseline over an extraordinarily extended range (11 decades) of angular frequencies inaccessible from the experimentally measured range (4 decades).

• Journal of Pharmaceutical Investigation
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• 제39권3호
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• pp.185-199
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• 2009

Using a strain-controlled rheometer [Advanced Rheometric Expansion System (ARES)], the steady shear flow properties and the dynamic viscoelastic properties of $Antiphlamine-S^{(R)}$ lotion have been measured at $20^{\circ}C$ (storage temperature) and $37^{\circ}C$ (body temperature). In this article, the temperature dependence of the linear viscoelastic behavior was firstly reported from the experimental data obtained from a temperature-sweep test. The steady shear flow behavior was secondly reported and then the effect of shear rate on this behavior was discussed in detail. In addition, several inelastic-viscoplastic flow models including a yield stress parameter were employed to make a quantitative evaluation of the steady shear flow behavior, and then the applicability of these models was examined by calculating the various material parameters. The angular frequency dependence of the linear viscoelastic behavior was nextly explained and quantitatively predicted using a fractional derivative model. Finally, the strain amplitude dependence of the dynamic viscoelastic behavior was discussed in full to elucidate a nonlinear rheological behavior in large amplitude oscillatory shear flow fields. Main findings obtained from this study can be summarized as follows : (1) The linear viscoelastic behavior is almostly independent of temperature over a temperature range of $15{\sim}40^{circ}C$. (2) The steady shear viscosity is sharply decreased as an increase in shear rate, demonstrating a pronounced Non-Newtonian shear-thinning flow behavior. (3) The shear stress tends to approach a limiting constant value as a decrease in shear rate, exhibiting an existence of a yield stress. (4) The Herschel-Bulkley, Mizrahi-Berk and Heinz-Casson models are all applicable and have an equivalent validity to quantitatively describe the steady shear flow behavior of $Antiphlamine-S^{(R)}$ lotion whereas both the Bingham and Casson models do not give a good applicability. (5) In small amplitude oscillatory shear flow fields, the storage modulus is always greater than the loss modulus over an entire range of angular frequencies tested and both moduli show a slight dependence on angular frequency. This means that the linear viscoelastic behavior of $Antiphlamine-S^{(R)}$ lotion is dominated by an elastic nature rather than a viscous feature and that a gel-like structure is present in this system. (6) In large amplitude oscillatory shear flow fields, the storage modulus shows a nonlinear strain-thinning behavior at strain amplitude range larger than 10 % while the loss modulus exhibits a weak strain-overshoot behavior up to a strain amplitude of 50 % beyond which followed by a decrease in loss modulus with an increase in strain amplitude. (7) At sufficiently large strain amplitude range (${\gamma}_0$>100 %), the loss modulus is found to be greater than the storage modulus, indicating that a viscous property becomes superior to an elastic character in large shear deformations.

• 대한기계학회논문집A
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• 제33권5호
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• pp.489-495
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• 2009

A novel technique to measuret of viscoelastic properties of polymers is proposed to investigate complex Poisson's ratio as a function of frequency. The forced vibration responses for the samples under the normal and the shear deformation are to be measured with varying load masses. The measured data were used to obtain the viscoelastic properties of the material based on an accurate 2D numerical deformation model of the sample. The 2D model enabled us to exclude data correction by the empirical form factor used in 1D model. Comprehensive measurements of viscoelastic properties of two slightly varied silicone RTV rubber ($Silastic^{(R)}$ S2) compositions were performed. Standard composition (90% PDMS polymer + 10% catalyst) and modified composition (92.5% polymer + 7.5% catalyst) were tested in temperature range from $30^{\circ}C$ to $70^{\circ}C$. Shear modulus, modulus of elasticity, loss factor, and both the real and the imaginary parts of the Poisson's ratio were determined for frequencies from 50 to 400Hz in the linear deformation regime (at relative deformations $10^{-4}{\sim}10^{-3}$).

• 한국소음진동공학회논문집
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• 제16권4호
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• pp.372-379
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• 2006

Little attention has been paid to static-strain-dependence of dynamic complex modulus of viscolelastic materials in computational analysisso far. Current commercial Finite Element Method (FEM) codes do not take such characteristics into consideration in constitutive equations of viscoelastic materials. Recent experimental observations that static-strain-dependence of dynamic complex modulus of viscolelastic materials, especially filled rubbers, are significant, however, require that solutions somehow are necessary. In this study, a simple technique of using a commercial FEM code, ABAQUS, is introduced, which seems to be far more cost/time saving than development of a new software with such capabilities. A static-strain-dependent correction factor is used to reflect the influence of static-strains in Merman model, which is currently the base of the ABAQUS. The proposed technique is applied to viscoelastic components of rather complicated shape to predict the dynamic stiffness under static-strain and the predictions are compared with experimental results.

• Korea-Australia Rheology Journal
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• 제18권2호
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• pp.67-81
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• 2006

Using a strain-controlled rheometer, the dynamic viscoelastic properties of aqueous xanthan gum solutions with different concentrations were measured over a wide range of strain amplitudes and then the linear viscoelastic behavior in small amplitude oscillatory shear flow fields was investigated over a broad range of angular frequencies. In this article, both the strain amplitude and concentration dependencies of dynamic viscoelastic behavior were reported at full length from the experimental data obtained from strain-sweep tests. In addition, the linear viscoelastic behavior was explained in detail and the effects of angular frequency and concentration on this behavior were discussed using the well-known power-law type equations. Finally, a fractional derivative model originally developed by Ma and Barbosa-Canovas (1996) was employed to make a quantitative description of a linear viscoelastic behavior and then the applicability of this model was examined with a brief comment on its limitations. Main findings obtained from this study can be summarized as follows: (1) At strain amplitude range larger than 10%, the storage modulus shows a nonlinear strain-thinning behavior, indicating a decrease in storage modulus as an increase in strain amplitude. (2) At strain amplitude range larger than 80%, the loss modulus exhibits an exceptional nonlinear strain-overshoot behavior, indicating that the loss modulus is first increased up to a certain strain amplitude(${\gamma}_0{\approx}150%$) beyond which followed by a decrease in loss modulus with an increase in strain amplitude. (3) At sufficiently large strain amplitude range (${\gamma}_0>200%$), a viscous behavior becomes superior to an elastic behavior. (4) An ability to flow without fracture at large strain amplitudes is one of the most important differences between typical strong gel systems and concentrated xanthan gum solutions. (5) The linear viscoelastic behavior of concentrated xanthan gum solutions is dominated by an elastic nature rather than a viscous nature and a gel-like structure is present in these systems. (6) As the polymer concentration is increased, xanthan gum solutions become more elastic and can be characterized by a slower relaxation mechanism. (7) Concentrated xanthan gum solutions do not form a chemically cross-linked stable (strong) gel but exhibit a weak gel-like behavior. (8) A fractional derivative model may be an attractive means for predicting a linear viscoelastic behavior of concentrated xanthan gum solutions but classified as a semi-empirical relationship because there exists no real physical meaning for the model parameters.

• Journal of Mechanical Science and Technology
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• 제18권1호
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• pp.12-19
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• 2004

Using LSM (laser scanning method) , the radius of curvature due to thermal deformation in polyimide film coated on Si substrate is measured. Since the polyimide film shows viscoelastic behavior, i.e., the modulus and deformation of the film vary with time and temperature, we estimate the relaxation modulus and the residual stresses of the polyimide film by measuring the radius of curvature and subsequently by performing viscoelastic analysis. The residual stresses relax by an amount of 10％ at 100$^{\circ}C$ and 20% at 150$^{\circ}C$ for two hours.