• 제목/요약/키워드: Uncertainty in Measurement

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공작기계 주축회전체 진동 측정에서의 불확도 추정 방법 (Estimation of Measurement Uncertainty for Vibration Tests in the Machine Tool Main Spindle)

  • 이정훈;윤상환;;박민원
    • 한국정밀공학회지
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    • 제28권4호
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    • pp.404-409
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    • 2011
  • Report on the notion of uncertainty is important. The reason is that the measured value includes a lot of uncertain factors. Reliable results can't be derived without the notion of uncertainty. The mathematical model to evaluate uncertainty considering the quality of vibration is important to evaluate uncertainty, and it must contain the every quantity which contributes significantly to uncertainty in the measured results. In this paper, the evaluation of uncertainty analysis about rotor vibration measurements of machine tools is presented to evaluate the most important factors of uncertainty.

GC/MS를 이용한 모발 중 메스암페타민 및 암페타민 분석의 측정불확도 평가 (Uncertainty Evaluation of the Analysis of Methamphetamine and Amphetamine in Human Hair by GC/MS)

  • 김진영;김종상;김민경;이재일;서용준;인문교
    • 약학회지
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    • 제51권3호
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    • pp.206-213
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    • 2007
  • Recently estimating the uncertainty of an analytical result has become an essential part of quantitative analysis. This study describes the uncertainty of the measurement for the determination of methamphetamine and its major metabolite amphetamine in human hair, The method consists of washing, drying, weighing, incubation and extraction with methanolic HCI solution, clean-up, trifluoroacetyl derivatization, and qualification/quantification of residues by gas chromatography/mass spectrometry (GC/MS). Traceability of measurement was established through traceable standards and calibrated volumetric equipment and measuring instruments. Measurement uncertainty associated with each analyte in real samples was estimated using quality control (QC) data. The main source of combined standard uncertainty comprised two components, which are uncertainties associated with calibration linearity and variations in QC, while those associated with preparation of analytical standards and sample weighing were not so important considering the degree of contribution. Relative combined standard uncertainties associated with the described method ranged for individual analytes from 4.99 to5.03%.

담배 연기 중 휘발성 유기물질 분석에 대한 측정 불확도 산출 (Measurement Uncertainty for Analysis of Volatile Organic Compound in Cigarette Mainstream Smoke)

  • 가미현;조성일;김미주;이철희;지상운;정종수;김용하;민영근
    • 한국연초학회지
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    • 제28권2호
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    • pp.144-151
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    • 2006
  • A measurement uncertainty for analysis of volatile organic compound (benzene) in cigarette mainstream smoke was carried out. In this study one point re-calibration method was used to estimate uncertainty for benzene. The measurement uncertainty was calculated based on the uncertainty sources of each analysis step, quality appraisal sources, drift and repeatability. As a result, the concentration and expanded uncertainty of benzene in cigarette mainstream smoke were measured as $38.08{\pm}4.36{\mu}g/cig$. Relative uncertainty of drift and repeatability obtained were 5% and 3%, respectively.

농업용트랙터 ROPS 시험의 신뢰성 향상을 위한 측정불확도 추정 (Measurement Uncertainty calculation for improving test reliability of Agricultural tractor ROPS Test)

  • 임류갑;강영선;김택진
    • 드라이브 ㆍ 컨트롤
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    • 제20권1호
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    • pp.34-40
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    • 2023
  • The agricultural tractor ROPS test method according to OECD code 4 is a test to assess whether the driver's safety area can be secured when a tractor overturns, and reliability should be ensured. In this study, a model formula and procedure for calculating measurement uncertainty expressing reliability in the field of agricultural machinery testing were established according to the ISO/IEC Guide 98-3:2008. The characteristics of the ROPS test device were assessed and repeated tests were performed, and the were used as factors to calculate the measurement uncertainty. As a result of repeated tests, the accuracy was higher than 1.9 % in all load directions; thus, they were, applied to calculate the type A standard uncertainty. The final expanded uncertainty was calculated within the range of less than ± 7.76 kN of force and ± 6.96 mm of deformation in all load directions.

몬테카를로 시뮬레이션을 이용한 시운전 선속-동력 성능에 대한 불확실성 해석 (Uncertainty Analysis for Speed and Power Performance in Sea Trial using Monte Carlo Simulation)

  • 서대원;김민수;김상엽
    • 대한조선학회논문집
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    • 제56권3호
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    • pp.242-250
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    • 2019
  • The speed and power performance of a ship is not only a guarantee issue between the ship owner and the ship-yard, but also is related with the Energy Efficiency Design Index (EEDI) regulation. Recently, International Organization for Standardization (ISO) published the procedure of the measurement and assessment for ship speed and power at sea trial. The results of speed and power performance measured in actual sea condition must inevitably include various uncertainty factors. In this study, the influence for systematic error of shaft power measurement system was examined using the Monte Carlo simulation. It is found that the expanded uncertainty of speed and power performance is approximately ${\pm}1.2%$ at the 95% confidence level(k=2) and most of the uncertainty factor is attributed to shaft torque measurement system.

측정이론에 관한 중학교 1학년 학생의 선개념 조사 (Investigation on the Seventh Grade Student's Preconceptions about Measurement Theory)

  • 서정아
    • 한국과학교육학회지
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    • 제22권3호
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    • pp.455-465
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    • 2002
  • 본 연구는 중학교 1학년 학생 30명을 대상으로 반복 측정, 대푯값 선정, 오차, 측정의 불확실성에 대한 신개념을 관찰 및 면담을 통하여 조사하였다. 조사 결과 50%의 학생들이 단 두 번만 측정하였고, 5번 이상 측정한 학생은 없었다. 반복 측정 후에 77%의 학생들은 자신의 느낌에 의거하여 측정값 중에서 대푯값을 선택하였고, 13%의 학생만 평균값을 계산하여 대푯값으로 정하였다. 60%의 학생은 측정 오차의 원인을 환경이나 측정 도구보다는 자신의 과실 때문이라고 하였다. 또한 대부분의 학생들은 다른 사람들에 의한 측정값이나 사간차를 둔 측정값이 달라지는 원인을 인간 때문이라고 생각하였다. 측정의 불확실성에 대하여 묻는 질문에 대하여 완전히 정확한 측정이 가능하다고 응답한 학생이 40%, 측정은 불확실하다고 응답한 학생이 33% 이었다. 학생들은 이에 대한 판단 근거로 주로 인간의 한계를 생각하였다. 결론적으로 과반수 이상의 학생들이 반복 측정 및 대푯값 선정에 대하여 이해하지 못하였고 측정 오차의 원인을 자신의 과실로 생각하였다. 또한 대부분의 학생들은 측정 결과가 다르거나, 측정이 불확실한 원인을 인간으로 생각하였다.

미터 소급성을 갖는 원자간력 현미경을 이용한 1차원 격자 피치 측정과 불확도 평가 (Pitch Measurement of One-dimensional Gratings Using a Metrological Atomic Force Microscope and Uncertainty Evaluation)

  • 김종안;김재완;박병천;엄태봉;강주식
    • 한국정밀공학회지
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    • 제22권4호
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    • pp.84-91
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    • 2005
  • We measured the pitch of one-dimensional (ID) grating specimens using a metrological atomic force microscope (M-AFM). The ID grating specimens a.e often used as a magnification standard in nano-metrology, such as scanning probe microscopy (SPM) and scanning electron microscopy (SEM). Thus, we need to certify the pitch of grating specimens fur the meter-traceability in nano-metrology. To this end, an M-AFM was setup at KRISS. The M-AFM consists of a commercial AFM head module, a two-axis flexure hinge type nanoscanner with built-in capacitive sensors, and a two-axis heterodyne interferometer to establish the meter-traceability directly. Two kinds of ID grating specimens, each with the nominal pitch of 288 nm and 700 nm, were measured. The uncertainty in pitch measurement was evaluated according to Guide to the Expression of Uncertainty in Measurement. The pitch was calculated from 9 line scan profiles obtained at different positions with 100 ㎛ scan range. The expanded uncertainties (k = 2) in pitch measurement were 0.10 nm and 0.30 nm for the specimens with the nominal pitch of 288 nm and 700 nm. The measured pitch values were compared with those obtained using an optical diffractometer, and agreed within the range of the expanded uncertainty of pitch measurement. We also discussed the effect of averaging in the measurement of mean pitch using M-AFM and main components of uncertainty.

부가저항 실험의 불확실성 연구 (Uncertainty Study of Added Resistance Experiment)

  • 박동민;이재훈;김용환
    • 대한조선학회논문집
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    • 제51권5호
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    • pp.396-408
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    • 2014
  • In this study, uncertainty analysis based on ITTC(International Towing Tank Conference) Recommended Procedures is carried out in the towing-tank experiment for motion responses and added resistance. The experiment was conducted for KVLCC2 model in head sea condition. The heave, pitch and added resistance were measured in different wave conditions, and the measurement was repeated up to maximum 15 times in each wave condition in order to observe the uncertainty of measured data. The uncertainty analysis was carried out by adopting the ISO-GUM(International Organization for Standardization, Guide to the Expression of Uncertainty in Measurements) method recommended by ITTC. This paper describes the details about the analysis method, uncertainty and the measured uncertainty for each source. The uncertainty analysis results are summarized as a tabular form. To validate the accuracy of the present measurement, the experimental results are compared with the results of numerical computation and other experiment. From the present uncertainty analysis, the main sources of uncertainty are identified, which can be very useful to improve the accuracy for added resistance experiment.

장기 안정성을 고려한 경질유 유량표준장치 불확도 평가 (Long Term Stability of Uncertainty Analysis of Light Oil Elow Standard System)

  • 임기원;최종오
    • 대한기계학회논문집B
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    • 제29권10호
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    • pp.1130-1138
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    • 2005
  • A national standard system for the petroleum field has been developed to calibrate and test the oil flow meters in Korea. The operating system and the uncertainty of the system were evaluated by the peer reviewers of foreign national metrology institutes in 2002. Since the characteristics of the system might be changed by time, the uncertainty of the system is reevaluated with the consideration of the long term stability of the system. It is found that the system has a relative expanded uncertainty of 0.048 $\%$ in the range of $15\~120\;m^3/h$. According to the uncertainty budget, the uncertainties of the fluid density and the final mass measurement, which are temperature dependent, contribute about $94\%$ of the total uncertainty in the oil flow standard system

길이 소급성을 갖는 AFM을 이용한 150nm 피치 측정 (150 nm Pitch Measurement using Metrological AFM)

  • 진종한
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2003년도 춘계학술대회 논문집
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    • pp.264-267
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    • 2003
  • Pitch measurements of 150 nm pitch one-dimensional grating standards were carried out using an contact mode atomic force microscopy(C-AFM) with a high resolution three-axis laser interferometer. It was called as 'Nano-metrological AFM' In Nano-metrological AFM, Three laser interferometers were aligned well to the end of AFM tip. Laser sources of the three-axis laser interferometer in the nano-metrological AFM were calibrated with an I$_2$-stablilzed He-Ne laser at a wavelength of 633 nm. So, the Abbe error was minimized and the result of the pitch measurement using the nano-metrological AFM has a traceability to the length standard directly. The uncertainty in the pitch measurement was estimated in accordance with the Guide to the Expression of Uncertainty in Measurement(GUM). The Primary source of uncertainty in the pitch-measurements was derived from repeatability of pitch-measurement, and its value was approx 0.186 nm. Expanded uncertainty(k=2) of less than 5.23 nm was obtained. It is suggested that the metrological AFM is a useful tool for the nano-metrological standard calibration.

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