• Title/Summary/Keyword: Ultrasonic Irradiation

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Thermal Sensitivity of the Bean Curd by Ultrasonic Irradiation (초음파 조사에 의한 두부의 열 감도)

  • 조문재;윤용현;부유천;김용태
    • The Journal of the Acoustical Society of Korea
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    • v.23 no.7
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    • pp.503-513
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    • 2004
  • In this paper, the thermal sensitivity, i .e. the temperature rise per unit acoustic power, was newly defined and proposed as a performance parameter of a tissue mimicking material. Eatable tofu (bean curd) manufactured by a factory was selected as a sample material for the experiment. The temperature changes were measured not only with the variation of ultrasonic irradiation time, acoustic power, depth from the sample surface. and the distance from the source transducer while adjusting the frequency to 8 MHz but also with the variation of frequency while acoustic power. depth from the sample surface. and the distance from the source transducer keeping constant. As a result of a consideration for the transformation of the measured temperature changes to thermal sensitivities. the thermal sensitivity was found to be sufficient to use as a Performance parameter for tissue mimicking material. The tofu as a tissue mimicking material showed the maximum thermal sensitivity at 10 MHz, as is a significant result to imply the possibility that the thermal sensitivity of real human tissue strong1y depends on the frequency.

Reuse of HPLC Guard Column by Ultrasonic Cleaning

  • Lee, Byung-Dae
    • Journal of the Korean Applied Science and Technology
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    • v.33 no.3
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    • pp.459-465
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    • 2016
  • This study investigated reusability of costly guard column by ultrasonic. It also investigated various effects that affect to guard column generation by ultrasonic. When investigated 30 KHz of frequency, area of ascorbic acid is 73.0% compared to unused guard column. As a result of investigation of effect of pH, guard column by ultrasonic is effective at alkali area. As a result of investigation of solvent effect, when ethanol is used, generation rate is 81.9% as of peak area compared to the case of analysis in un used column. From the result, it indicates that regenerated guard by ultrasonic is reusable.

Ultrasonically enhancing flowability of cement grout for reinforcing rock joint in deep underground

  • Junho Moon;Inkook Yoon;Minjin Kim;Junsu Lee;Younguk Kim
    • Geomechanics and Engineering
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    • v.33 no.2
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    • pp.211-219
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    • 2023
  • This study analyzes the changes in the physical properties of grout by irradiating it with ultrasonic energy and assesses the injectability of the grout into deep rock fractures. The materials used in the research are OPC (Ordinary Portland Cement) and MC (Micro Cement), and are irradiated depending on the water/cement ratio. After irradiating the grout with ultrasonic energy, viscosity, compressive strength, and particle size are analyzed, and the results of the particle size analysis were applied to Nick Barton's theory to evaluate the injectability of the grout into deep rock fractures under those conditions. It was found that the viscosity of the grout decreased after ultrasonic wave irradiation, and the rate of viscosity reduction tended to decrease as the water/cement ratio increased. Additionally, an increase in compressive strength and a decrease in particle size were observed, indicating that the grout irradiated with ultrasonic energy was more effective for injection into rock fractures.

Mixing Augmentation of the Compressible Parallel Jets Using the Irradiation of Ultrasonic Waves (초음파 조사를 이용한 압축성 평행 제트의 활성화)

  • Chang Se-Myong;Shin Seong-Ryong;Lee Soogab
    • 한국전산유체공학회:학술대회논문집
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    • 2001.10a
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    • pp.138-143
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    • 2001
  • An experimental model to enhance the mixing of parallel supersonic-subsonic jet ($M_1$=1.78 and $M_2$=0.30) is simulated with a numerical technique by modeling the wall-mounted cavity to a boundary condition of oscillating pressure. The computed pilot pressure distributions along three representative cross sections show a good agreement with the equivalent experimental data. The irradiation of acoustic wave in the ultrasonic range causes the mixing augmentation of jet and wake due to the transfer of vibration energy between fluid particles.

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Preparation of the Copper Oxalate Powder by Ethanol Oxalic Acid Method (수산에타놀법을 이용한 수산동 분말의 합성)

  • Choi, H.L.;Lee, B.W.
    • Journal of Power System Engineering
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    • v.9 no.4
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    • pp.124-129
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    • 2005
  • Copper oxide, CuO, are very important components include of high temperature super- conductors, and widely used. The properties of sintered materials were affected by the size and shape of copper oxide with starting materials in the solid-phase reaction. A homogeneous and fine CuO powder was prepared by thermal decomposition of the copper oxalate precursor. Copper oxalate was precipitated by the addition of copper nitrate solution to an oxalic acid solution. The influence of various factors such as temperature, pH, concentration as well as ultrasonic irradiation in the solution were investigated.

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Ultrasound Energy Effect as Initiator of Polystyrene Latex Polymerization (Polystyrene Latex 제조공정에서 초음파 에너지의 개시효과)

  • Lee, Seung-Bum;Kim, Won-Il;Hong, In-Kwon
    • Elastomers and Composites
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    • v.31 no.3
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    • pp.175-182
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    • 1996
  • Polymer latices, prepared from the emulsion polymerization of vinyl monomer compounds, are widely used for many industrial applications. Included among these are uses in paints, adhesives, flocculants, and heavy-duty plastics as well as their original use in synthetic rubber compounds. The emulsion polymerization process with chemical initiator has chemical disadvantage such as removal of initiator which was left after polymerization. In this study, polystyrene latex was prepared by using ultrasonic irradiation which generate the free radical, and then it was analyzed by GPC. Reaction temperature hardly have an effect on average molecular weight. Average molecular weight is increased by increasing amount of surfactant, i.e. SDS, but polydispersity is decreased. After 90 minutes of reaction time, increase and decrease of average molecular weight Is repeated. It is proposed that monodisperse polymer is obtained by controlling ultrasonic irradiation time and surfactant concentration.

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Synthesis of Hybrid Fullerene Oxide[C60(O)n, (n≥1)] - Silver Nanoparticle Composites and Their Catalytic Activity for Reduction of 2-, 3-, 4-Nitroaniline

  • Park, Jeong Hoon;Ko, Jeong Won;Ko, Weon Bae
    • Elastomers and Composites
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    • v.54 no.3
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    • pp.252-256
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    • 2019
  • Fullerene oxide[$C_{60}(O)_n$, ($n{\geq}1$)] was synthesized by dissolving fullerene[$C_{60}$] and 3-chloroperoxybenzoic acid in toluene under refluxing condition for 5 h. Hybrid fullerene oxide-silver nanoparticle composites were synthesized by dissolving fullerene oxide and silver nitrate[$AgNO_3$] in diethylene glycol under ultrasonic irradiation for 3 h. The synthesized hybrid nanocomposites were characterized by X-ray diffraction, scanning electron microscopy, and ultraviolet-visible[UV-vis] spectroscopy. The catalytic activity for the reduction of various nitroanilines[NAs] was identified by UV-vis spectrophotometer. The efficiency of the catalytic reduction by the synthesized hybrid nanocomposites has an order of 4-NA > 2-NA > 3-NA.

Sonocatalytic Degradation of Rhodamine B in the Presence of TiO2 Nanoparticles by Loading WO3

  • Meng, Ze-Da;Sarkar, Sourav;Zhu, Lei;Ullah, Kefayat;Ye, Shu;Oh, Won-Chun
    • Korean Journal of Materials Research
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    • v.24 no.1
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    • pp.6-12
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    • 2014
  • In the present work, $WO_3$ and $WO_3-TiO_2$ were prepared by the chemical deposition method. Structural variations, surface state and elemental compositions were investigated for preparation of $WO_3-TiO_2$ sonocatalyst. X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and transmission electron microscopy (TEM) were employed for characterization of these new photocatalysts. A rhodamine B (Rh.B) solution under ultrasonic irradiation was used to determine the catalytic activity. Excellent catalytic degradation of an Rh.B solution was observed using the $WO_3-TiO_2$ composites under ultrasonic irradiation. Sonocatalytic degradation is a novel technology of treating wastewater. During the ultrasonic treatment of aqueous solutions sonoluminescence, cavitaties and "hot spot" occurred, leading to the dissociation of water molecules. In case of a $WO_3$ coupled system, a semiconductor coupled with two components has a beneficial role in improving charge separation and enhancing $TiO_2$ response to ultrasonic radiations. In case of the addition of $WO_3$ as new matter, the excited electrons from the $WO_3$ particles are quickly transferred to $TiO_2$ particle, as the conduction band of $WO_3$ is 0.74 eV which is -0.5 eV more than that of $TiO_2$. This transfer of charge should enhance the oxidation of the adsorbed organic substrate. The result shows that the photocatalytic performance of $TiO_2$ nanoparticles was improved by loading $WO_3$.

The Effect of Distance between Two Transducers on Sonochemical Reactions in Dual Irradiation Systems (이중 초음파 조사 시스템에서 진동부 사이의 거리가 초음파 화학 반응에 미치는 영향)

  • Kim, Eunkyung;Son, Younggyu
    • Journal of Soil and Groundwater Environment
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    • v.18 no.5
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    • pp.39-45
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    • 2013
  • Many researchers have studied the effectiveness of ultrasound in chemical and environmental engineering fields including material synthesis, pollutant removal, cleaning, extraction, and disinfection. Acoustic cavitation induced by ultrasound irradiation in aqueous phase can cause various sonophysical and sonochemical reactions without any chemicals. However most of the previous studies focused only on the relationships between ultrasonic conditions and the results of sonochemical reactions in lab-scale sonoreactors. As a results of this, only a few studies have been devoted to design and optimization of industrial scale sonoreactors. In this study, the effect of the distance between two opposite transducer modules on sonochemical reactions was investigated in single and dual irradiation systems (334 kHz) for four distances including 50, 100, 150, and 200 mm using KI dosimetry. It was found that the dual irradiation systems provided higher performance in terms of the zeroth reaction coefficient and the cavitation yield compared to the single irradiation systems. The sonochemiluminescence (SCL) images for the visualization of the cavitation field showed that cavitation active zone was larger and sonochemical reaction intensity was much higher in the dual irradiation system than in the single irradiation system.