Journal of the Korean Applied Science and Technology (한국응용과학기술학회지)

The Korean Society of Applied Science and Technology (한국응용과학기술학회)
권호 표지
DOI QR코드

DOI QR Code

Reuse of HPLC Guard Column by Ultrasonic Cleaning

  • Received : 2016.08.10
  • Accepted : 2016.09.12
  • Published : 2016.09.30
Download PDF
⟨ Previous Next ⟩

Abstract

This study investigated reusability of costly guard column by ultrasonic. It also investigated various effects that affect to guard column generation by ultrasonic. When investigated 30 KHz of frequency, area of ascorbic acid is 73.0% compared to unused guard column. As a result of investigation of effect of pH, guard column by ultrasonic is effective at alkali area. As a result of investigation of solvent effect, when ethanol is used, generation rate is 81.9% as of peak area compared to the case of analysis in un used column. From the result, it indicates that regenerated guard by ultrasonic is reusable.

Keywords

References

  1. N. Youngvises, T. Chaida, S. Khonyoung, N. Kuppithayanant, W. Tiyapongpattana, A. Itharat, and J. Jakmunee, Greener Liquid Chromatography using a Guard Column with Micellar Mobile Phase for Separation of Some Pharmaceuticals and Determination of Parabens, Talanta, 106, 350 (2013). https://doi.org/10.1016/j.talanta.2012.12.040
  2. M. Abu-Zaid, A Fouling Evaluation System for Industrial Heat Transfer Equipment Subject to Fouling, Int. Comm. Heat & Mass Trans., 27, 815 (2000). https://doi.org/10.1016/S0735-1933(00)00162-7
  3. X. Li, T. Liu, H. Wang, and X. Sun, Mixed Fouling Growth Process-Microbial and $CaCO_3$ Fouling in Water Systems, Chinese J. Chem. Eng., 53, 1247 (2002).
  4. Y. Jin, Y. Ju, H. Lee, and S. Hong, Fouling Potential Evaluation by Cake Fouling Index: Theoretical Development, Measurements, and Its Implications for Fouling Mechanisms, J. Membr. Sci., 490, 57 (2015). https://doi.org/10.1016/j.memsci.2015.04.049
  5. M. Hu, S. Zheng, and B. Mi, Organic Fouling of Graphene Oxide Membranes and Its Implications for Membrane Fouling Control in Engineered, Environ. Sci. & Technol., 50, 685 (2016). https://doi.org/10.1021/acs.est.5b03916
  6. G. Poppe, A. Roy, K. Majamaa, and W. Mickols, Novel Membrane Fouling Procedure to Compare Fouling-Resistant Membranes, Official Proc. the Inter. Wat. Confer., 71, 668 (2010).
  7. F. Smaili, D. K. Angadi, C. M. Hatch, and O. Herbert, Optimization of Scheduling of Cleaning in Heat Exchanger Networks Subject to Fouling: Sugar Industry Case Study, FOOD & BIOPRODUCTS PROCESSING, 77, 159 (1998).
  8. P. Bacchin and P. Aimar, Critical Fouling Conditions Induced by Colloidal Surface Interaction: From Causes to Consequences, Desalination, 175, 21 (2005). https://doi.org/10.1016/j.desal.2004.09.020
  9. B. Van der Bruggen, G. Cornelis, C. Vandecasteele, and I. Devreese, Fouling of Nanofiltration and Ultrafiltration Membranes Applied for Wastewater Regeneration in the Textile Industry, Desalination, 175, 111 (2005). https://doi.org/10.1016/j.desal.2004.09.025
  10. Y. C. Juang, D. J. Lee, and J. Y. Lai, Visualizing Fouling Layer in Membrane Bioreactor, Separ Sci. & Technol., 45, 962 (2010). https://doi.org/10.1080/01496391003666882
  11. K. Sasaki, M. Nishihira, and K. Imano, Precise Displacement Measurements Using Phase Information of 40 kHz Ultrasonic Waves in Pinhole-Based Air-Coupled Ultrasonic System, Separ Sci. & Technol., 46, 4545 (2007).
  12. D.-K. Lee, J.-H. Lee, and D.-S. Kim, UV Blocking Effect of $TiO_2/SiO_2$ Composite Powders Prepared by Ultrasonic Spray Pyrolysis, J. Korean Oil Chemists' Soc., 22, 281 (2005).
  13. H. Sunwoo and H.-S. Kim, Chemical Synthesis od Alkyl Polyglucoside Using Ultrasonic Emulsification, J. Korean Oil Chemists' Soc., 18, 127 (2001).
  14. http://www.glsciences.com/c-product/hplc/lc-columns/inertsil-ods-3/
  15. http://www.separations.us.tosohbioscience.com/Products/HPLCColumns/ReversedPhase/Silica/Monomeric80A/TSKgelODS-80Tm.htm