• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2001년도 춘계학술대회 논문집
• /
• pp.827-832
• /
• 2001

A lot of investigations have been made in recent years on the equal channel angular pressing(ECAP) which produces ultra-fine grains(UFG). Among many process parameters such as channel angles, frictions, die deformations and materials employed, the effects of material properties on the deformation behavior have been investigated. The finite element method(FEM) has been used to investigate this issue.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2003년도 The 8th Asian Symposium on Precision Forging ASPF
• /
• pp.189-192
• /
• 2003

The Electro-thermal Explosion Coating (EEC) technique is a new surface treatment technology emerged in recent years. It uses an electrical discharge (with very high voltage from 5 to 30 kV or more) to produce a pulse current with large density inside the material to be deposited, the metal wire undergo the heating, melting, vaporization, ionization and explosion processes in a very short time (from tens ns to several hundreds ${\mu}s$), and the melted droplets shoot at the substrate with a very high velocity (3000 - 4500 m/s), so that the coating materials can be deposited on the surface of the substrate. Coatings with nano-size grains or ultra- fine grains can be formed because of rapid solidification (cooling rate up to $10^6-10^9\;k/s$). Surface of the substrate (about $1-5{\mu}m$ in depth) can be melted rapidly and coatings with very high bonding strength can be obtained.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2004년도 춘계학술대회 논문집
• /
• pp.228-230
• /
• 2004

Samples of the aluminum alloy 3103 sheets were repeatedly deformed by ECAR up to twelve passes. Shear textures developed after the first passage of ECAR. However, the intensity of shear texture components decreased with increasing number of ECAR passages. Observations by TEM and EBSD revealed that the degree of misorientations within the deformed grains increased with increasing number of ECAR passes. Changes in textures and microstructures were hardly observed during recrystallization anneal. Upon subsequent annealing, the samples deformed by a large number of ECAR passes displayed a continuous grain growth. A higher deformation by ECAR resulted in a slower softening, which reflects the stability of ultra-fine grains against the grain growth.

• 한국생산제조학회지
• /
• 제7권2호
• /
• pp.100-107
• /
• 1998

Diamond wheels with fine grains and multi-porous structures are newely trial developed for smoothing and mirror finishing materials. Grinding wheel must have performed both to remove tool marks efficienitly and to contact elastically with curved surfaces, that are employed for ultra precision and high performance grinding of difficult-to materials such as tungsten carbide alloy using tool and die materials, Diamond grains are bonded by a melamine resin to prevent the decrease of machining efficiency due to grain sinking within the bond materials. Also, highly foamed structures are developed to increase the flexibility of the grinding wheel, and to induce self-sharpening by increasing contact pressure between the grinding wheel and workpiece surfaces. In this paper, melamine-bonded diamond wheels try to manufacture, then the forming method of grinding wheel are suggested, and the grinding characteristics of melamine-bonded diamond grinding wheel are also illustrated.

• 한국재료학회지
• /
• 제9권4호
• /
• pp.341-344
• /
• 1999

We reported compositional separation(CS) into Co-enriched and Cri-enriched components inside the grains of Co-Cr based thin films prepared by rf sputtering. CS strongly depends on the sputtering conditions of substrate temperature and target composition. Tuning the microstructure of the Co-Cr films is important in order to employ the CS for high-density magnetic recording. We investigated the origin of CS from thermodynamic viewpoint. We employ a spinodal decomposition-like model to describe the origin of the CS in Co-Cr films. We consider the total free energy of the Co-Cr films as the sum of several free energies of; 1) thermodynamic mixing entropy of a binary solid solution, 2) magnetic ordering interaction(MOI) energy below the Curie temperature, and 3) excess interaction energy(XS) caused by the sputtering process as a function of temperature and composition. Those energies distorted the total free energy like the spinodal decomposition and caused the compositionally separated fine microstructure inside the grains. If the second derivative of the total free energy with respect to Cr composition becomes negative at a given substrate temperature, we may observe a metastable compositional separation inside the Co-Cr alloy films. We expect to exploit the microstructure of CS for ultra-high density magnetic recording.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2005년도 추계학술대회 논문집
• /
• pp.381-383
• /
• 2005

극저온 압연중인 알루미늄 합금의 미세조직의 변화 - 집합조직의 발전과 결정립 크기 및 형상 변화 -를 예측할 수 있는 오일러리안 유한요소 해석을 수행하였다. 패스 당 압하율 $30\%$ 인 연속 세 패스의 압연공정을 시뮬레이션 하여 얻은 결과는 실험에서 관측된 것과 비슷한 경향을 보여, 본 연구의 해석모델의 타당성을 입증하였다.

• 한국표면공학회지
• /
• 제34권6호
• /
• pp.531-536
• /
• 2001

Co-22 %Cr alloy films are promising for high-density perpendicular magnetic recording media with their perpendicular anisotropy and large coercivity of 3000 Oe. We observed that a self organized nano structure (SONS) of fine ferromagnetic Co-enriched phase and paramagnetic Cr-enriched phase appears inside the grain of Co-Cr magnetic alloy thin films at the elevated substrate temperature after do-sputtering. The periodic fine Co-enriched phase and Cr-enriched phase is the plate shape of 80 (equation omitted)-wide and 1000 (equation omitted)-long. Cr-enriched phases are located at the center of grains. We prepared 5000 (equation omitted) -thick Co-22 %Cr films on polyimide substrate with varying substrate temperature of $ 30^{\circ}C$, $ 150^{\circ}C$ ,200 $^{\circ}C$, $300^{\circ}C$, and $400^{\circ}C$, respectively. A transmission electron microscope equipped with energy dispersive X-ray analyzer is employed to observe the microstructure of each samples after Co-enri-ched phase are etched selectively. The self organized nano structure of Co-enriched and Cr-enriched lamellar is observed above the substrate temperture of $150^{\circ}C$. No compositional change is observed with substrate temperature. The compositional phase separation in self organized structure becomes clear as the substrate temperature increases. Our results implies that the self organized nano structure in Co-22 %Cr film is ideal for ultra high density recording media by recording selectively on Co-enri-ohed phase.

• 대한기계학회논문집A
• /
• 제30권7호
• /
• pp.765-772
• /
• 2006

Much research efforts have been made on the equal channel angular pressing (ECAP) which produces ultra-fine grains. Along with the experiments, the finite element method has been widely employed to investigate the deformation behavior of specimen during ECAP and the effect of process parameters of ECAP. In this paper, sectional shape change has been investigated during ECAP with the pure-Zr, Zr-702 by using three-dimensional finite element analysis. The results have been compared with experimental results.

• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2002년도 춘계학술대회 논문집
• /
• pp.661-665
• /
• 2002

A lot of investigations have been made in recent years on the equal channel angular pressing (ECAP) which produces ultra-fine grains. The finite element method has been used to investigate this issue. In this paper, pure-Zirconium is considered far ECAP process by three dimensional finite element analysis. The effects of fiction on the deformation behavior have been investigated and compared with two dimensional finite element analysis.

• 한국정밀공학회지
• /
• 제19권8호
• /
• pp.187-193
• /
• 2002

Much research efforts have been made on the equal channel angular pressing (ECAP) which produces ultra-fine grains. Among many process parameters such as channel angles, frictions, die deformations and materials employed, the effects of material properties on the deformation behavior have been investigated. The finite element method has been used to investigate this issue.