• Nuclear Engineering and Technology
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• v.53 no.1
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• pp.172-177
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• 2021

The microstructure and texture of three 316L foils of 25 ㎛ thickness, which were subjected to different manufacturing process, were systematically characterized using advance analytical techniques. Then, the electrochemical property of the 316L foils in simulated pressurized water reactor (PWR) solution was analyzed using potentiodynamic polarization. The results showed that final rolling strain and annealing temperature had evident effect on grain size, fraction of recrystallization, grain boundary type and texture distribution. It was suggested that large final rolling strain could transfer Brass texture to Copper texture; low annealing temperature could limit the formation of preferable orientations in the rolling process to reduce anisotropy. Potentiodynamic polarization test showed that all samples exhibited good corrosion performance in the simulated primary PWR solution.

• Journal of Powder Materials
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• v.29 no.4
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• pp.309-313
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• 2022

In this study, additive manufacturing of a functionally graded material (FGM) as an alternative to joining dissimilar metals is investigated using directed energy deposition (DED). FGM consists of five different layers, which are mixtures of austenitic stainless steel (type 316 L) and low-alloy steel (LAS, ferritic steel) at ratios of 100:0 (A layer), 75:25 (B layer), 50:50 (C layer), 25:75 (D layer), and 0:100 (E layer), respectively, in each deposition layer. The FGM samples are successfully fabricated without cracks or delamination using the DED method, and specimens are characterized using optical and scanning electron microscopy to monitor their microstructures. In layers C and D of the sample, the tensile strength is determined to be very high owing to the formation of ferrite and martensite structures. However, the elongation is high in layers A and B, which contain a large fraction of austenite.

• Journal of Powder Materials
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• v.25 no.6
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• pp.475-481
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• 2018

Selective laser melting (SLM), a type of additive manufacturing (AM) technology, leads a global manufacturing trend by enabling the design of geometrically complex products with topology optimization for optimized performance. Using this method, three-dimensional (3D) computer-aided design (CAD) data components can be built up directly in a layer-by-layer fashion using a high-energy laser beam for the selective melting and rapid solidification of thin layers of metallic powders. Although there are considerable expectations that this novel process will overcome many traditional manufacturing process limits, some issues still exist in applying the SLM process to diverse metallic materials, particularly regarding the formation of porosity. This is a major processing-induced phenomenon, and frequently observed in almost all SLM-processed metallic components. In this study, we investigate the mechanical anisotropy of SLM-produced 316L stainless steel based on microstructural factors and highly-oriented porosity. Tensile tests are performed to investigate the microstructure and porosity effects on mechanical anisotropy in terms of both strength and ductility.

• Journal of the Korean Vacuum Society
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• v.19 no.6
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• pp.460-466
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• 2010

We measured the magnetic properties of stainless steels type 304 and 316L to see if those materials can be used for the applications where non-magnetic materials are required. The results show that the relative permeability of samples was greatly increased during manufacturing processes. After full solution annealing, however the permeability could be reduced to less than 1.02. Thus, the materials may be employed in the low-permeability applications.

• Corrosion Science and Technology
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• v.7 no.1
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• pp.45-49
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• 2008

The cyclic polarisation technique was applied to determine the corrosion, primary-passivation, transpassive, and protection potential of AISI 316L stainless steels immersed in 3550-ppm NaCl solution containing sulfate in the content up to 3000 ppm. The solutions were kept constant at $27^{\circ}C$ and saturated by laboratory air. The solution pH was varied from 3 to 11. Each type of potentials was plotted in function of pH and linked as lines to determine the different zones in the constructed potential-pH diagram. The predominant regimes of the immunity, general corrosion, perfect passivation, imperfect passivation, and pitting corrosion were determined based on those lines of potentials. Comparing to the potential-pH diagram of specimens immersed in the aerated and deaerated 3550-ppm NaCl solutions, the addition of 3000-ppm $Na_2SO_4$ to these solutions increased the overall, perfect and imperfect, passivation regime by shifting the transpassive-potential line to the noble direction. However, it also widened the imperfect passivation area. The addition of $Na_2SO_4$ did not significantly affect the corrosion potential. It was found that the dissolved oxygen tends to negatively shift the transpassive-potential and protection-potential lines at all studied pH. The considerable effect of dissolved oxygen on corrosion and primary-passivation potentials could not be observed.

• Journal of Electrochemical Science and Technology
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• v.13 no.2
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• pp.237-253
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• 2022

The methyl 2-(1,3-dithietan -2- ylidene)-3-oxobutanoate (MDYO) and 2-(1,3-dithietan-2-ylidene) cyclohexane -1,3-dione (DYCD) were synthesized and tested at various concentrations as corrosion inhibitors for 316L stainless steel in 1 M HCl using weight loss, electrochemical impedance spectroscopy (EIS), potentiodynamic polarization (PDP), surface analysis techniques (SEM / EDX and Raman spectroscopy) and Functional Density Theory (DFT) was also used to calculate quantum parameters. The obtained results indicated that the inhibition efficiency of MDYO and DYCD increases with their concentration, and the highest value of corrosion inhibition efficiency was determined in the range of concentrations investigated (0.01 × 10^-3 - 10^-3 M). Polarization curves (Tafel extrapolation) showed that both compounds act as mixed-type inhibitors in 1M HCl solutions. Electrochemical impedance spectra (Nyquist plots) are characterized by a capacitive loop observed at high frequencies, and another small inductive loop near low frequencies. The thermodynamic data of adsorption of the two compounds on the stainless steel surface and the activation energies were determined and then discussed. Analysis of experimental results shows that MDYO and DYCD inhibitors adsorb to the metal surface according to the Langmuir model and the mechanism of adsorption of both inhibitors involves physisorption. SEM-EDX results confirm the existence of an inhibitor protective film on the stainless steel surface. The results derived from theoretical calculations supported the experimental observation.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.05a
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• pp.109-110
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• 2006

Various parametric methods, Larson-Miller (L-M), Orr-Sherby-Dorn (O-S-D), Manson-Haferd (M-H) parameters, and minimum commitment method (MCM), were used to predict longer rupture time from short-term creep data. A number of the creep data were collected through literature surveys and experimental data produced in KAERI for predicting the creep type of type 316LN SS. Polynomial equations for predicting the creep life were obtained by the time-temperature parameters (TTP) and the MCM. standard error (SE) and standard error or mean (SEM) values were compared for the each method with temperatures. The TTP methods were good in the creep-life prediction, but the MCM was much superior to the TTP ones at $700^{\circ}C\;and\;750^{\circ}C$. The MCM was found to be lower in the SE values compared to the TTP methods

• Journal of the Korean Society of Industry Convergence
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• v.22 no.2
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• pp.191-199
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• 2019

In this paper, dissimilar friction welding were produced using 15 mm diameter solid bar in chrome molybedenum steel(SCM440) to stainless steel(STS316L) to investigate their mechanical properties. Consequently, optimal welding conditions were n=2000 rpm, HP=70 MPa, UP=140 MPa, HT=10 sec and UT=10 sec when the metal loss(Mo) is 8.6 mm. In addition, an acoustic emission technique was applied to evaluate the optimal friction welding condition. AE parameters including the cumulative count, amplitude and energy showed a various changes according to the friction condition. A continuous type waveforms and low frequency spectrum was presented in friction time. On the other hand, a burst type waveform and high frequency spectrum was exhibited in pressing time.

• Journal of Advanced Marine Engineering and Technology
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• v.35 no.6
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• pp.802-808
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• 2011

One of the important mechanical properties of cryogenic temperature structure material is fracture toughness. Research on normalization of fracture toughness test method is becoming very important issue with development of cryogenic structural elements. Specially, mechanical properties estimation by each micro-structure of welding department is important because it can cause unstable fracture when use under cryogenic environment in case of welding department. In this study, fracture toughness estimation test was carried out to unloading compliance method and sensitization heat-tread minimized test specimen at liquid nitrogen (77K), liquid helium (4K), 293K temperature to STS-316L base metal and weld metal.

• Transactions of Materials Processing
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• v.29 no.2
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• pp.103-112
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• 2020

This study explores the effects of different pre-machining conditions on the deposition characteristics and mechanical properties of austenitic stainless steel samples repaired using direct energy deposition (DED). In the DED repair process, defects such as pores and cracks can occur at the interface between the substrate and deposited material. In this study, we varied the shape of the pre-machined zone for repair in order to prevent cracks from occurring at the slope surface. After repairs by the DED process, macro-scale cracks were observed in samples that had been pre-machined with elliptic and trapezoidal grooves. In addition, it was not possible to completely prevent micro-crack generation on the sloped interfaces, even in the capsule-type grooved sample. From observation of the fracture surfaces, it was found that the cracks around the inclined interface were due to a lack of fusion between the substrate and the powder material, which led to low tensile properties. The specimen with the capsule-type groove provided the highest tensile strength and elongation (respective of 46% and 571% compared to the trapezoidal grooved specimen). However, the tensile properties were degraded compared to the non-repaired specimen (as-hot rolled material). The fracture characteristics of the repaired specimens were determined by the cracks at the sloped interfaces. These cracks grew and coalesced with each other to form macro-cracks, they then coalesced with other cracks and propagated to the substrate, causing final fracture.