• 한국진공학회:학술대회논문집
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• 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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• pp.273.1-273.1
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• 2014

Graphene, a two dimensional plane structure of $sp^2$ bonding, has been promised for a new material in many scientific fields such as physics, chemistry, and so on due to the unique properties. Chemical vapor deposition (CVD) method using transitional metals as a catalyst can synthesize large scale graphene with high quality and transfer on other substrates. However, it is difficult to control the number of graphene layers. Therefore, it is important to manipulate the number of graphene layers. In this work, homogeneous solid solution of Cu and Ni was used to control the number of graphene layers. Each films with different thickness ratio of Cu and Ni were deposited on $SiO_2/Si$ substrate. After annealing, it was confirmed that the thickness ratio accords with the composition ratio by X-ray diffraction (XRD). The synthesized graphene from CVD was analyzed via raman spectroscopy, UV-vis spectroscopy, and 4-point probe to evaluate the properties. Therefore, the number of graphene layers at the same growth condition was controlled, and the correlation between mole fraction of Ni and the number of graphene layers was investigated.

• Water Engineering Research
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• 제1권3호
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• pp.209-222
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• 2000

A spectral formalism was applied to quantify the sampling errors due to spatial and/or temporal gaps in soil moisture measurements. The lack of temporal measurements of the two-dimensional soil moisture field makes it difficult to compute the spectra directly from observed records. Therefore, the space-time soil moisture spectra derived by stochastic models of rainfall and soil moisture was used in their record. Parameters for both models were tuned with Southern Great Plains Hydrology Experiment(SGP'97) data and the Oklahoma Mesonet data. The structure of soil moisture data is discrete in space and time. A design filter was developed to compute the sampling errors for discrete measurements in space and time. This filter has the advantage in its general form applicable for all kinds of sampling designs. Sampling errors of the soil moisture estimation during the SGP'97 Hydrology Experiment period were estimated. The sampling errors for various sampling designs such as satedlite over pass and point measurement ground probe were estimated under the climate condition between June and August 1997 and soil properties of the SGP'97 experimental area. The ground truth design was evaluated to 25km and 50km spatial gap and the temporal gap from zero to 5 days.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2010년도 제39회 하계학술대회 초록집
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• pp.85-85
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• 2010

Graphene, the building block of graphite, is one of the most promising materials due to their fascinating electronic transport properties. The pseudo-two-dimensional sp2 bonding in graphene layers yields one of the most effective solid lubricants. In this poster, we present the correlation between electrical and nanomechanical properties of graphene layer grown on Cu/Ni substrate with CVD (Chemical Vapor Deposition) method. The electrical (current and conductance) and nanomechanical (adhesion and friction) properties have been investigated by the combined apparatus of friction force microscopy/conductive probe atomic force microscopy (AFM). The experiment was carried out in a RHK AFM operating in ultrahigh vacuum using cantilevers with a conductive TiN coating. The current was measured as a function of the applied load between the AFM tip and the graphene layer. The contact area has been obtained with the continuum mechanical models. We will discuss the influence of mechanical deformation on the electrical transport mechanism on graphene layers.

• 대한구강악안면임플란트학회지
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• 제22권4호
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• pp.210-218
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• 2018

Purpose: The purpose of this study was to investigate the validity and reproducibility of a method based on cone-beam computed tomography (CBCT) technology for the visualization and measurement of gingival soft-tissue dimensions. Material and Methods: A total of 66 selected points in soft-tissue of the ex vivo head of an adult pig were investigated in this study. For the measurement of radiographic thickness (RT), wet soft-tissue surfaces were lightly covered with barium sulfate powder using a powder spray. CBCT was taken and DICOM files were assessed for soft-tissue thickness measurement at reference points. A periodontal probe and a rubber stop were used for the measurement of trans-gingival probing thickness (TPT). After flap elevation, actual thickness of soft-tissue (actual thickness, AT) was measured. Correlation analysis and intraclass correlation coefficients analysis (ICC) were performed for AT, TPT, and RT. Results: All variables were distributed normally. Strong significant correlations of AT with RT and TPT values were found. The two ICC values between TPT vs. AT and RT vs. AT differed significantly. Conclusion: Our results indicated that correlation of RT was stronger than that of TPT with AT. We concluded that soft tissue measurement with CBCT could be a reliable method, compared to the trans-gingival probing measurement method.

• 한국전기전자재료학회논문지
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• 제36권1호
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• pp.29-35
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• 2023

Herein we investigated the effect of the conductive agent on the electrochemical performance of the SiOx anode. SiOx anodes have a relatively low volume expansion (~160%) compared to Pure-silicon, but have a problem in that they have a poor electrical conductivity characteristic. In this study, physical and electrochemical measurements were performed using two 0-dimensional amorphous carbon conductive agents with different crystallinity and surface area. The crystal structure of the conductive agents and the local graphitization degree were analyzed through XRD and Raman, and the surface area of the particles was observed through BET. In addition, the electrical performance according to the graphitization degree of the conductive agents was confirmed through a 4-point probe. As a result of the electrochemical cycle and rate performance, it was confirmed that the performance of SiOx using a conductive agent having a low graphitization degree and a high surface area was improved. The results in this study suggest that the graphitization degree and surface area of the amorphous carbon conductive agent may play an important role in the SiOx electrode.

• 대한조선학회지
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• 제12권2호
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• pp.59-66
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• 1975

Recently, as the dimensions of energy carriers increase, especially in draft, a reliable prediction of the ship motions at finite depths of water becomes necessary. The purpose of this paper is to probe the effect of finite water depth on the hydrodynamic forces and ship motions, particularly heave and pitch, in longitudinal regular head waves, by comparing the experimental value of Freakes and Keay with the author's theoretical value obtained by applying the modified strip theory to the Mariner class ship. It is confirmed that generally the hydrodynamic coefficients in the equations of motion increase with decreasing water depth, and the wave exciting forces and moments decrease with decreasing water depth. Amplitudes of heave and pitch in longitudinal regular head waves decrease as the water depth in the range where the length of the incident wave is comparatively long. The effects of Froude Number on the hydrodynamic coefficients increase with decreasing water depth and is more noticeable in the case of heave than pitch. In heave, generally the discrepancy between the experimental value and the theoretical value is relatively small in the case of $F_n=O$, but it is very large in the case of $F_n=0.2$. It is considered that the trend stems from the ignorance of the three dimensional effect and the other effects due to shallowness of water on the hydrodynamic coefficients in the theoretical calculation. An extension of methods for calculating the two dimensional hydrodynamic forces to included the effect of forward speed should be recommended. It is required that more experimental works in finite water depths will be carried out for correlation studies between the theoretical calculation, according tp modified strip theory, and model experiments.

• Journal of Plant Biology
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• 제34권2호
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• pp.121-127
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• 1991

유도된 해녀콩(Canavalia lineata)의 뿌리혹을 발달 단계별로 구분하여 수용성 단백질을 추출하고 SDS-PAGE 및 2차원 전기영동(2-D) 방법으로 뿌리의 수용성 단백질과 비교 분석하였다. SDS-PAGE에 의해 뿌리혹에서만 나타나는 13개의 뿌리혹 특이 단백질 밴드를 검색하였고, 20D 방법으로 분석한 결과 30개의 뿌리혹 특이 단백질 spot을 확인하였다. 이들 단백질은 뿌리혹 발달 단계에 따라 질적 및 양적 차이를 보여, leghemoglobin(Lb) 유사 단백질의 경우 I 단계(b<2mm)에서는 3개, II 단계(d=4-5mm)부터는 5개의 단위체가 차등적으로 검출되었다. 이들은 콩의 경우에 비해 좁은 pI 범위(4.4-5.0)를 갖고 있으나 분자량면에서는 15.7 kd으로 더 크게 나타났다. 또한 콩의 lb 유전자를 탐침으로한 뿌리혹과 뿌리의 전체 RNA에 대한 northern 혼성화반응을 수행한 결과 해녀콩의 lb 유전자는 뿌리혹에서만 조지 특이적으로 발현되고 있음이 확인되었다.

• 한국정밀공학회지
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• 제23권8호
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• pp.72-79
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• 2006

We measured grating pitch standards using optical diffractometry and analyzed measurement uncertainty. Grating pitch standards have been used widely as a magnification standard for a scanning electron microscope (SEM) and a scanning probe microscope (SPM). Thus, to establish the meter-traceability in nano-metrology using SPM and SEM, it is important to certify grating pitch standards accurately. The optical diffractometer consists of two laser sources, argon ion laser (488 nm) and He-Cd laser (325 nm), optics to make an incident beam, a precision rotary table and a quadrant photo-diode to detect the position of diffraction beam. The precision rotary table incorporates a calibrated angle encoder, enabling the precise and accurate measurement of diffraction angle. Applying the measured diffraction angle to the grating equation, the mean pitch of grating specimen can be obtained very accurately. The pitch and orthogonality of two-dimensional grating pitch standards were measured, and the measurement uncertainty was analyzed according to the Guide to the Expression of Uncertainty in Measurement. The expanded uncertainties (k = 2) in pitch measurement were less than 0.015 nm and 0.03 nm for the specimen with the nominal pitch of 300 nm and 1000 nm. In the case of orthogonality measurement, the expanded uncertainties were less than $0.006^{\circ}$. In the pitch measurement, the main uncertainty source was the variation of measured pitch values according to the diffraction order. The measurement results show that the optical diffractometry can be used as an effective calibration tool for grating pitch standards.

• 한국자기공명학회논문지
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• 제12권1호
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• pp.14-25
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• 2008

To investigate the 3-bond connectivity of human brain metabolites by scalar coupling interaction through 2D-correlation spectroscopy (COSY) techniques using high field NMR spectroscopy. All NMR experiments were performed at 298K on Unity Inova 500 or 600 (Varian Inc.) equipped with a triple resonance probe head with z-shield gradient. Human brain metabolites were prepared with 10% $D_2O$. Two dimensional 2D COSY spectra were acquired with 4096 complex data points in $t_2$ and 128 or 256 increments in $t_1$ dimension. The spectral width was 9615.4 Hz and solvent suppression was achieved using presaturation using low power irradiation of the water resonance during 2s of relaxation delay. NMR data were processed using VNMRJ (Varian Instrument) software and all the chemical shifts were referenced to the methyl resonance of N-acetyl aspartate (NAA) peak at 2.0 ppm. Total 10 metabolites such as N-acetyl aspartate (NAA), creatine (Cr), choline (Cho), glutamine (Gln), glutamate (Glu), myo-inositol (Ins), lactate (Lac), taurine (Tau), ${\gamma}$-aminobutyricacid (GABA), alanine (Ala) were included for major target metabolites. Symmetrical 2D-COSY spectra were successfully acquired. Total 14 COSY cross peaks were observed even though there were parallel/orthogonal noisy peaks induced by water suppression. Except for Cr, all of human brain metabolites produced COSY cross peaks. The spectra of NAA methyl proton at 2.02 ppm and Glu methylene proton ($CH_2(3)$) at 2.11 ppm and Gln methylene proton ($CH_2(3)$) at 2.14 ppm were overlapped in the similar resonance frequency between 2.00 ppm and 2.15 ppm. The present study demonstrated that in vitro 2D-COSY represented the 3-bond connectivity of human brain metabolites by scalar coupling interaction. This study could aid in better understanding the interactions between human brain metabolites in vivo 2D-COSY study. Also it would be helpful to determine the molecular stereochemistry in vivo by using two-dimensional MR spectroscopy.

• 자원환경지질
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• 제35권5호
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• pp.465-478
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• 2002

JERS-1 L-밴드 SAR 위성에서 얻어진 5개의 interferogram을 이용하여 1996년 5월 2일부터 1998년 2월 21일 사이 연안매립지인 녹산 국가산업단지의 공단조성과정에서 발생한 지반침하량을 계산하였다. 약 16 m의 공간해상도를 갖는 레이더 관측결과는 현장측정 자료로부터 관측되기 어려운 세밀한 침하 양상을 잘 반영하였다. 정확도 검증을 위해 2-pass DInSAR로 구한 침하량을 Magnetic Probe Extensometer(측정정밀도:${\pm}$1 mm)를 사용하여 총 42개소에 서 측정된 현장자료와 비교하였다. 5개의 쌍으로부터 추정된 DInSAR침하량과 실측침하량의 평균 상관계수는 0.77 이다. 추정된 DInSAR 침하량 중 0.5 이상의 긴밀도를 갖는 점들만을 이용하여 계산한 경우 상관계수는 0.87이며, RMSE는 1.44 cm로 더욱 좋은 결과를 나타낸다. 또한 추정된 회귀선의 기울기는 1.04로 실측값과 DInSAR 추정값이 기울기 1에 가까운 선형관계를 잘 만족하고 있음을 보여준다. 즉 DInSAR 결과 긴밀도 0.5 이상의 지점을 이용하면 효과적으로 연안매립지의 침하량을 관측할 수 있다. DInSAR를 이용하여 계산된 녹산 국가산업단지에서 발생한 최대 누적침하량은 약 60 cm 정도이며, 연구지역의 북쪽과 남서쪽에서는 약 20 cm 이하의 침하가 관측되었다. 이러한 결과는 자연적인 지표변위 관측뿐만 아니라 지반공학적 응용분야에서도 DInSAR 기술이 매우 중요한 역할을 맡을 수 있음을 보여준다.