• Advanced Composite Materials
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• 제17권3호
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• pp.235-246
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• 2008

This paper is concerned with geotextiles bonded chemically with geogrid to form a geocomposite. Geotextiles, thermally bonded and non-woven, play an important role as a separator. Also, this study investigates the resistance to the application environment of geotextile composites. Here, numerous tests have been performed and it was revealed from experimental results that thermally bonded geotextile in geosynthetic composites showed superior characteristics to that manufactured from needle punched non-woven method in terms of tensile strength, tensile strain and high separation performance. It was noted from experiments that the geotextile prepared for separation purpose and manufactured in a thermal bonding method showed relatively low permittivity so that it could be used as a smooth separator. In addition, PVA geotextile/HDPE geomembrane composites were designed and manufactured to investigate the waste landfill related properties. Numerous experiments have been performed and experimental results were summarized to evaluate practical applicability of PVA geotextile/HDPE geomembrane composites. Among the properties of proposed geomembrane composites, evaluation has been focused on the investigation of mechanical properties, AOS (apparent opening size), permittivity and ultraviolet stability.

• 한국재료학회지
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• 제26권10호
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• pp.542-548
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• 2016

The influence of NiCrAlY bond coating on the adhesion properties of an Fe thermal coating sprayed on an Al substrate was investigated. By applying a bond coat, an adhesion strength of 21MPa was obtained, which was higher than the 15.5MPa strength of the coating without the bond coat. Formation of cracks at the interface of the bond coat and the Al substrate was suppressed by applying the bond coat. Microstructural analysis of the coating interface using EBSD and TEM indicated that the dominant bonding mechanism was mechanical interlocking. Mechanical interlocking without crack defects in the coating interface may improve the adhesion strength of the coating. In conclusion, the use of an NiCrAlY bond coat is an effective method of improving the adhesion properties of thermal sprayed Fe coatings on Al substrates.

• Bulletin of the Korean Chemical Society
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• 제34권12호
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• pp.3559-3564
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• 2013

Alumina particles were grafted onto the surface of manganese oxide particles via the coprecipitation process using surfactant and cosurfactant. The phase of Mn/Al salts (Phase I) and the phase of precipitation agent (Phase II) were prepared in aqueous surfactant solution, separately. Phase II was added into Phase I and the reaction was performed to form the precursors of composites through hydrogen bonding between $Mn(OH)_2$ and $Al(OH)_3$ prepared by the reaction of Mn/Al salts with the precipitation agent. The alumina-grafted manganese oxide particles were obtained as a final product after calcination. The concentrations of Al salt and surfactant were varied to investigate their effects on the formation and the crystallinity of composites. In addition, the crystal structure of products could be controlled by changing the calcination temperature. Through thermal analyses, it was found that the thermal stability of manganese oxide was improved by the introduction of alumina on its surface.

• The Journal of Advanced Prosthodontics
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• 제7권2호
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• pp.108-114
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• 2015

PURPOSE. The aim of this study was to evaluate effect of different surface treatment methods on the bond strength between aged composite-resin core and luting agent. MATERIALS AND METHODS. Seventy-five resin composites and also seventy-five zirconia ceramic discs were prepared. 60 composite samples were exposed to thermal aging (10,000 cycles, 5 to $55^{\circ}C$) and different surface treatment. All specimens were separated into 5 groups (n=15): 1) Intact specimens 2) Thermal aging-air polishing 3) Thermal aging- Er:YAG laser irradiation 4) Thermal aging- acid etching 5) Thermal-aging. All specimens were bonded to the zirconia discs with resin cement and fixed to universal testing machine and bond strength testing loaded to failure with a crosshead speed of 0.5 mm/min. The fractured surface was classified as adhesive failure, cohesive failure and adhesive-cohesive failure. The bond strength data was statistically compared by the Kruskal-Wallis method complemented by the Bonferroni correction Mann-Whitney U test. The probability level for statistical significance was set at ${\alpha}$=.05. RESULTS. Thermal aging and different surface treatment methods have significant effect on the bond strength between composite-resin cores and luting-agent (P<.05). The mean baseline bond strength values ranged between $7.07{\pm}2.11$ and $26.05{\pm}6.53$ N. The highest bond strength of $26.05{\pm}6.53$ N was obtained with Group 3. Group 5 showed the lowest value of bond strength. CONCLUSION. Appropriate surface treatment method should be applied to aged composite resin cores or aged-composites restorations should be replaced for the optimal bond strength and the clinical success.

• 한국진공학회지
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• 제8권2호
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• pp.136-140
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• 1999

The stability and response time of $WO_3$ thin films for EC device are critical problems being solved. Those are affected by the species of electrolyte, preparation conditions and fabricating methods of specimen. In this paper, we compared the stabilities of three kinds of tungsten oxide film in electrolyte. Each of three films was prepared by different manufacturing conditions, that is, one is a thermal oxidation film of tungsten metal deposited on pure glass substrate, another is a $WO_3$ film made on ITO glass directly, the other is a thermally oxidized film on tungsten plate. It was observed that thermally oxidized $WO_3$ films has a remarkable stability (the lifetime was above $10^6$ cycle). From these results, we found that the stability was closely related to the stoichiometric bonding between tungsten and oxygen atoms in addition to crystallinity and density of film.

• 대한기계학회논문집 C: 기술과 교육
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• 제3권4호
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• pp.265-271
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• 2015

스마트폰을 비롯한 고성능 모바일 전자기기의 발전에 따라서 경박단소한 전자부품의 요구가 커지고 있으며 이를 위해서 새로운 패키징 방법이 탄생하고 있다. 이러한 새로운 패키징 공정에서 웨이퍼 본딩 공정이 많이 요구되고 있다. 웨이퍼 본딩에서 많이 활용되는 방법이 열 압착 방법으로 가열된 헤드로 웨이퍼에 압력을 가하여 본딩하는 방법이다. 열 압착 방법에서 요구되는 공정조건은 온도 균일성과 Uniform Press이다. 온도 균일성은 마이크로 히터와 열 해석을 통한 설계로 비교적 쉽게 요구조건을 만족 시킬 수 있지만 Uniform Press를 가공과 조립으로만 요구조건을 만족시키기 위해서는 매우 높은 정밀도가 요구된다. 열 압착 방법은 고온에서 동작되므로 열 변형에 대한 기계적인 오차를 고려하여 설계, 가공, 조립이 진행되어야하므로 많은 어려움이 따른다. 본 연구에서는 Air 스프링과 Metal Form의 자가 보정장치를 이용하여 가공, 조립, 열 변형으로 발생하는 기계적 오차를 보상하여 성능과 신뢰성을 향상시켰다.

• International Journal of Safety
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• 제9권1호
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• pp.43-46
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• 2010

In the recycle process of organic solvent, the atmospheric oxygen can cause autoxidation and product peroxide. The time-saving method to evaluate the hazards has been required. In this study, oxygen pressure monitoring experiment was proposed as a new method to evaluate autoxidative resistances of solvents. Some of organic solvents were pressurized by oxygen and kept under isothermal condition. At the same time, the pressure in the vessel tracked. Iodometrical titration, thermal analysis and spectroscopic analysis were performed to measure peroxide concentration, the heat of reaction and chemical bonding change. From the results that THF has larger oxygen consumption rate than CPME, it is considered that autoxidative resistance of THF is lower than that of CPME. This method enables to obtain results in shorter time than other methods. These experimental results were consistent with the previous research with longer test durations [1-2].

• 한국건축시공학회지
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• 제7권3호
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• pp.107-113
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• 2007

This study is to investigate adhesive properties depending on the temperature, humidity, and freeze-thraw of the Steel plate adhesive strengthening method by the epoxy resin. The results are summarized as following. For the temperature variation, the debonding failure appear only after 1 cycle of temperature varoation because the coefficient of thermal expansion of the epoxy resin is comparatively large, and the bonding strength is decreased. The deformation properties and ultrasonic pulse velocity on each materials are similar until 4 cycles on the dry and moisture test. As the freeze-thraw test, the epoxy resin is degraded easily subjected to freeze-thaw cycle, comparatively easy, so the debonding failure may occur in short term because of the freeze-thaw repeatition.p

• 전산구조공학
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• 제8권1호
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• pp.173-186
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• 1995

2가지 이상의 재질로 결합된 구조물이 온도 변화를 받으면 열응력이 발생한다. 이러한 응력은 재질간의 열팽창계수가 서로 상이하여 생긴다. 본 논문에서는 균일한 온도변화를 받는 복합 재료로 이루어진 축대칭 원판(disk)에 대한 응력상태를 구하는 공식을 유도하였다. 먼저, 재료역학원리를 이용하여 근사해를 구한 후, Eigenfunction series를 전개하여 탄성학적인 정확해(Exact Solution)를 구하였다. 또한 정확해는 유한요소법으로 구한 해와 비교하였다. 상기 근사해로는 연계면에서의 응력분포를 예측하는 데 어려움이 있었으나, 정확해는 유한요소법으로 구한 결과와 대체로 일치하고 있어 응력분포를 충분히 예측할 수 있었다. 따라서, 본 논문에서 구한 정확해(Exact Solution) 공식은 복합재료로 구성된 구조물의 연계면에서의 응력분포를 결정하는 데 유용하다.

• 한국의류산업학회지
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• 제16권2호
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• pp.319-325
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• 2014

This article describes a method for producing chitosan non-woven fabrics by just hot pressing without the use of a binder. A study has been made of the wet spinning of chitosan fiber. The fibers were rinsed thoroughly in running water and chopped wet into staples of with a length of approximately 5-10 mm. The chopped chitosan staples were dispersed uniformly in water and fabricated using a non-woven making machine. This study examined the formation and the characteristics of chitosan non-woven fabrics manufactured by hot pressing without the use of a binder. The effects of the non-woven fabrication conditions on the thermal, morphological, structural, and physical properties of chitosan non-woven fabric with and without water as a plasticizer were studied. The temperature of the exothermic peak, decomposition of chitosan fibers increased with increasing heating rate. Water in the chitosan fiber effectively plasticized the chitosan fiber. The thermal bonded structure of the wet chitosan fiber with water as a plasticizer was clearly found in many parts of the non-woven fabric at a fabrication temperature of $200^{\circ}C$. The intensity and profile of the (100) plane($2{\theta}=10.2^{\circ}$) and (040) plane($2{\theta}=20.9^{\circ}$) in the chitosan non-woven fabric decreases and became smooth in the non-woven fabric formation by melting.